Crystallography Open Database

Information card for entry 8107445

Preview

Coordinates	8107445.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	bis[(<i>N,N</i>-dimethylformamide-κ<i>O</i>) (pyridine-2-carboxylato-κ^2^<i>N,O</i>) (μ~2~-pyridine-2-carboxylato-κ^2^<i>N,O</i>)-dinickel(II)
Formula	C30 H30 N6 Ni2 O10
Calculated formula	C30 H30 N6 Ni2 O10
Title of publication	Crystal structure of bis(N,N-dimethylformamide-κO)-bis(pyridine-2-carboxylato-κ 2 N,O)-bis(μ 2-pyridine-2-carboxylato-κ 2 N,O)-dinickel(II), C30H30N6Ni2O10
Authors of publication	Ha, Kwang
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2023
Journal volume	238
Journal issue	2
Pages of publication	373 - 375
a	9.1314 ± 0.0005 Å
b	9.412 ± 0.0005 Å
c	10.8608 ± 0.0005 Å
α	68.1912 ± 0.0016°
β	70.7776 ± 0.0017°
γ	86.8173 ± 0.0018°
Cell volume	815.93 ± 0.07 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0219
Residual factor for significantly intense reflections	0.0207
Weighted residual factors for significantly intense reflections	0.0518
Weighted residual factors for all reflections included in the refinement	0.0528
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
285111 (current)	2023-07-10	cif/ Adding structures of 8107445 via cif-deposit CGI script.	8107445.cif