#------------------------------------------------------------------------------
#$Date: 2017-03-04 15:27:23 +0200 (Sat, 04 Mar 2017) $
#$Revision: 193464 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/12/53/4125392.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4125392
loop_
_publ_author_name
'Yang, Huayan'
'Yan, Juanzhu'
'Wang, Yu'
'Su, Haifeng'
'Gell, Lars'
'Zhao, Xiaojing'
'Xu, Chaofa'
'Teo, Boon K.'
'Häkkinen, Hannu'
'Zheng, Nanfeng'
_publ_section_title
;
 Embryonic Growth of Face-Center-Cubic Silver Nanoclusters Shaped in
 Nearly Perfect Half-Cubes and Cubes.
;
_journal_issue                   1
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              31
_journal_page_last               34
_journal_paper_doi               10.1021/jacs.6b10053
_journal_volume                  139
_journal_year                    2017
_chemical_formula_moiety
'0.5(Ag63 C312 F72 P8 S36), 0.5(Ag63 C318 F72 P8 S36), 1(Br)'
_chemical_formula_sum            'C315 Ag63 Br F72 P8 S36'
_chemical_formula_weight         13428.79
_space_group_crystal_system      trigonal
_space_group_IT_number           148
_space_group_name_Hall           '-R 3'
_space_group_name_H-M_alt        'R -3'
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_atom_sites_solution_primary     iterative
_audit_creation_date             2016-09-23
_audit_creation_method
;
Olex2 1.2
(compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155)
;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            6
_cell_length_a                   25.2879(4)
_cell_length_b                   25.2879(4)
_cell_length_c                   114.758(2)
_cell_measurement_reflns_used    20509
_cell_measurement_temperature    100.01(10)
_cell_measurement_theta_max      61.0150
_cell_measurement_theta_min      4.0650
_cell_volume                     63553.5(18)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb  1 2013,16:14:44)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb  1 2013,16:14:44)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb  1 2013,16:14:44)
;
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution
;
Superflip (Palatinus & Chapuis, 2007;Palatinus & van der Lee, 2008;
Palatinus et al., 2012)
;
_diffrn_ambient_temperature      100.01(10)
_diffrn_detector_area_resol_mean 10.3415
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_details
;
#__ type_ start__ end____ width___ exp.time_
  1 omega  -91.00   -1.40   0.7000   15.0000
omega____ theta____ kappa____ phi______ frames
    -      -40.9924  125.0000  150.0000 128

#__ type_ start__ end____ width___ exp.time_
  2 omega  -95.00  -67.70   0.7000   15.0000
omega____ theta____ kappa____ phi______ frames
    -      -40.9924  125.0000 -150.0000 39

#__ type_ start__ end____ width___ exp.time_
  3 omega  -47.00  -19.00   0.7000   15.0000
omega____ theta____ kappa____ phi______ frames
    -      -40.9924  125.0000 -150.0000 40

#__ type_ start__ end____ width___ exp.time_
  4 omega -113.00  -16.40   0.7000   15.0000
omega____ theta____ kappa____ phi______ frames
    -      -40.9924  -38.0000  -60.0000 138

#__ type_ start__ end____ width___ exp.time_
  5 omega -118.00   -7.40   0.7000   15.0000
omega____ theta____ kappa____ phi______ frames
    -      -40.9924  -77.0000   90.0000 158

#__ type_ start__ end____ width___ exp.time_
  6 omega  -48.00   -0.40   0.7000   30.0000
omega____ theta____ kappa____ phi______ frames
    -      -61.5000   45.0000   90.0000 68

#__ type_ start__ end____ width___ exp.time_
  7 omega   36.00  105.30   0.7000   30.0000
omega____ theta____ kappa____ phi______ frames
    -      108.1940  -94.0000   60.0000 99

#__ type_ start__ end____ width___ exp.time_
  8 omega   30.00   70.60   0.7000   30.0000
omega____ theta____ kappa____ phi______ frames
    -      108.1940  -30.0000   30.0000 58

#__ type_ start__ end____ width___ exp.time_
  9 omega   79.00  177.00   0.7000   30.0000
omega____ theta____ kappa____ phi______ frames
    -      108.1940   30.0000  -30.0000 140

#__ type_ start__ end____ width___ exp.time_
 10 omega   36.00   84.30   0.7000   30.0000
omega____ theta____ kappa____ phi______ frames
    -      108.1940  -30.0000   60.0000 69

#__ type_ start__ end____ width___ exp.time_
 11 omega   48.00  135.50   0.7000   30.0000
omega____ theta____ kappa____ phi______ frames
    -      108.1940  -61.0000 -120.0000 125

#__ type_ start__ end____ width___ exp.time_
 12 omega   78.00  150.10   0.7000   30.0000
omega____ theta____ kappa____ phi______ frames
    -      108.1940   30.0000   60.0000 103
;
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_UB_11      0.0077987000
_diffrn_orient_matrix_UB_12      -0.0492855000
_diffrn_orient_matrix_UB_13      -0.0063753000
_diffrn_orient_matrix_UB_21      -0.0303735000
_diffrn_orient_matrix_UB_22      0.0084811000
_diffrn_orient_matrix_UB_23      -0.0109313000
_diffrn_orient_matrix_UB_31      0.0629616000
_diffrn_orient_matrix_UB_32      0.0494715000
_diffrn_orient_matrix_UB_33      -0.0044784000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0617
_diffrn_reflns_av_unetI/netI     0.0449
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       28
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_k_max       28
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       130
_diffrn_reflns_limit_l_min       -130
_diffrn_reflns_number            87736
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        61.150
_diffrn_reflns_theta_max         61.150
_diffrn_reflns_theta_min         3.368
_diffrn_source                   'SuperNova (Cu) X-ray Source'
_exptl_absorpt_coefficient_mu    25.420
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.36499
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb  1 2013,16:14:44)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.105
_exptl_crystal_description       block
_exptl_crystal_F_000             37380
_exptl_crystal_size_max          0.1
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.08
_refine_diff_density_max         5.142
_refine_diff_density_min         -3.086
_refine_diff_density_rms         0.422
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.090
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1399
_refine_ls_number_reflns         21696
_refine_ls_number_restraints     54
_refine_ls_restrained_S_all      1.089
_refine_ls_R_factor_all          0.1520
_refine_ls_R_factor_gt           0.1246
_refine_ls_shift/su_max          0.081
_refine_ls_shift/su_mean         0.004
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1549P)²+22635.4551P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3893
_refine_ls_wR_factor_ref         0.4101
_reflns_Friedel_coverage         0.000
_reflns_number_gt                15656
_reflns_number_total             21696
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ja6b10053_si_005.cif
_cod_data_source_block           '[Ag63(SPhF2)36(PnBu3)8]Br'
_cod_depositor_comments
'Adding full bibliography for 4125391--4125393.cif.'
_cod_original_cell_volume        63554(3)
_cod_database_code               4125392
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_reflns_odcompleteness_completeness 85.97
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     66.97
_olex2_refinement_description
;
1. Restrained distances
 C52-S7
 2.8 with sigma of 0.02
 C68-S7
 2.8 with sigma of 0.02
 S7-C55
 1.8 with sigma of 0.02
 C121-C0AA = C184-C121 = C184-C13 = C177-C13
 1.5 with sigma of 0.02
 C198-C141 = C141-C140 = C174-C140
 1.5 with sigma of 0.02
 C294-C113
 1.5 with sigma of 0.02
 C193-C125
 1.5 with sigma of 0.02
 C184-C0AA
 2.5 with sigma of 0.04
 C121-C13
 2.5 with sigma of 0.04
 C184-C177
 2.5 with sigma of 0.04
 C294-C154
 2.5 with sigma of 0.04
 C193-C82
 2.5 with sigma of 0.04
 C183-C125
 2.5 with sigma of 0.04
2. Uiso/Uaniso restraints and constraints
Uanis(C99) \\sim Ueq, Uanis(C108) \\sim Ueq, Uanis(C177) \\sim Ueq, Uanis(C36)
\\sim Ueq, Uanis(C160) \\sim Ueq, Uanis(C57) \\sim Ueq: with sigma of 0.1 and
sigma for terminal atoms of 0.2
3. Others
 Fixed Sof: Br29(0.33333)
4.a Fitted hexagon refined as free rotating group:
 C3(C18,C58,C79,C78,C90), C6(C27,C66,C80,C104,C122), C16(C23,C31,C65,C115,
 C136), C43(C34,C63,C98,C95,C84), C52(C55,C68,C134,C160,C77), C149(C112,C57,C45,
 C110,C114), C179(C14,C47,C119,C129,C38)
;
_shelx_shelxl_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Ag1 Ag 0.33007(3) 0.73074(3) 0.62572(2) 0.0293(2) Uani 1 1 d . . .
Ag2 Ag 0.20289(3) 0.53579(3) 0.64603(2) 0.02704(19) Uani 1 1 d . . .
Ag3 Ag 0.3333 0.6667 0.59369(2) 0.0456(4) Uani 1 3 d S T P
Ag4 Ag 0.26752(3) 0.53445(3) 0.66654(2) 0.02176(18) Uani 1 1 d . . .
Ag5 Ag 0.26631(2) 0.66523(3) 0.64624(2) 0.02149(17) Uani 1 1 d . . .
Ag6 Ag 0.27340(3) 0.47178(3) 0.64517(2) 0.0346(2) Uani 1 1 d . . .
Ag7 Ag 0.13701(3) 0.66845(3) 0.66668(2) 0.0343(2) Uani 1 1 d . . .
Ag8 Ag 0.32563(4) 0.52492(3) 0.62260(2) 0.0440(2) Uani 1 1 d . . .
Ag9 Ag 0.12841(3) 0.59349(3) 0.64701(2) 0.0364(2) Uani 1 1 d . . .
Ag10 Ag 0.0000 0.0000 0.42720(2) 0.0522(4) Uani 1 3 d S T P
Ag11 Ag 0.07081(3) 0.01197(3) 0.45913(2) 0.0386(2) Uani 1 1 d . . .
Ag12 Ag 0.13131(3) 0.07979(3) 0.49990(2) 0.0291(2) Uani 1 1 d . . .
Ag13 Ag 0.06034(3) 0.07094(3) 0.47964(2) 0.0283(2) Uani 1 1 d . . .
Ag14 Ag 0.13910(3) 0.01904(3) 0.47936(2) 0.0364(2) Uani 1 1 d . . .
Ag15 Ag 0.3333 0.6667 0.6667 0.0184(4) Uani 1 6 d S T P
Ag16 Ag 0.11104(4) 0.20775(3) 0.48037(2) 0.0413(2) Uani 1 1 d . . .
Ag17 Ag 0.33983(5) 0.36084(4) 0.64309(2) 0.0661(3) Uani 1 1 d . . .
Ag18 Ag 0.20926(3) 0.02600(3) 0.49989(2) 0.0407(2) Uani 1 1 d . . .
Ag19 Ag 0.28214(5) 0.33102(4) 0.47634(2) 0.0655(4) Uani 1 1 d . . .
Ag20 Ag 0.18809(3) 0.15223(4) 0.47869(2) 0.0412(2) Uani 1 1 d . . .
Ag21 Ag 0.19949(4) 0.38980(4) 0.66652(2) 0.0494(3) Uani 1 1 d . . .
Ag22 Ag 0.0000 0.0000 0.5000 0.0237(4) Uani 1 6 d S T P
Ag23 Ag 0.13218(5) 0.14289(4) 0.45616(2) 0.0570(3) Uani 1 1 d . . .
Ag24 Ag 0.27406(4) 0.17052(4) 0.49984(2) 0.0571(3) Uani 1 1 d . . .
S1 S 0.29176(12) 0.56706(11) 0.60619(2) 0.0378(8) Uani 1 1 d . . .
S2 S 0.43928(12) 0.59101(11) 0.62729(2) 0.0383(8) Uani 1 1 d . . .
S3 S 0.09768(14) 0.06706(14) 0.43970(3) 0.0499(10) Uani 1 1 d . . .
S4 S 0.30340(13) 0.42075(11) 0.62934(3) 0.0445(8) Uani 1 1 d . . .
S5 S 0.15561(13) 0.41750(11) 0.64911(3) 0.0477(9) Uani 1 1 d . . .
S6 S 0.05657(16) 0.17875(12) 0.46085(3) 0.0546(11) Uani 1 1 d . . .
S7 S 0.12019(13) 0.34880(11) 0.68246(3) 0.0514(10) Uani 1 1 d D . .
S8 S 0.32359(12) 0.14094(14) 0.51548(3) 0.0542(10) Uani 1 1 d . . .
S9 S 0.29491(14) 0.27547(15) 0.49432(3) 0.0582(11) Uani 1 1 d . . .
S10 S 0.27342(15) 0.35618(12) 0.66088(3) 0.0543(10) Uani 1 1 d . . .
S11 S 0.25468(12) 0.10034(13) 0.48235(3) 0.0511(10) Uani 1 1 d . . .
S12 S 0.23227(16) 0.23285(14) 0.46269(3) 0.0601(11) Uani 1 1 d . . .
P13 P 0.3333 0.6667 0.57258(6) 0.072(2) Uani 1 3 d S T P
P14 P 0.3404(2) 0.27459(15) 0.63446(5) 0.0915(16) Uani 1 1 d . . .
P15 P 0.3632(2) 0.4217(2) 0.46756(6) 0.109(2) Uani 1 1 d . . .
P16 P 0.0000 0.0000 0.40609(7) 0.143(5) Uani 1 3 d S T P
C3 C 0.4810(3) 0.5749(3) 0.61705(6) 0.051(4) Uani 1 1 d . . .
C18 C 0.5425(3) 0.5943(5) 0.61864(9) 0.080(6) Uani 1 1 d G . .
C58 C 0.5743(5) 0.5818(8) 0.61021(12) 0.150(10) Uani 1 1 d G . .
C79 C 0.5445(7) 0.5500(8) 0.60018(11) 0.102(7) Uani 1 1 d G . .
C78 C 0.4829(7) 0.5307(6) 0.59859(8) 0.104(7) Uani 1 1 d G . .
C90 C 0.4512(4) 0.5431(4) 0.60702(7) 0.109(7) Uani 1 1 d G . .
F4 F 0.3015(5) 0.0435(6) 0.42109(11) 0.142(5) Uani 1 1 d . . .
C6 C 0.4206(3) 0.2562(3) 0.51567(8) 0.080(6) Uani 1 1 d . . .
C27 C 0.3799(4) 0.2068(4) 0.52242(9) 0.068(5) Uani 1 1 d G . .
C66 C 0.3880(6) 0.2078(5) 0.53441(9) 0.105(8) Uani 1 1 d G . .
C80 C 0.4368(6) 0.2581(7) 0.53965(8) 0.097(7) Uani 1 1 d G . .
C104 C 0.4775(5) 0.3075(6) 0.53290(10) 0.139(12) Uani 1 1 d G . .
C122 C 0.4694(4) 0.3065(4) 0.52091(10) 0.145(12) Uani 1 1 d G . .
F8 F 0.4863(4) 0.1458(7) 0.46185(12) 0.166(6) Uani 1 1 d . . .
C9 C 0.3288(6) 0.1060(7) 0.46473(12) 0.074(6) Uani 1 1 d . . .
C10 C 0.2215(5) 0.5120(5) 0.60058(11) 0.047(4) Uani 1 1 d . . .
C11 C 0.0955(5) 0.3477(5) 0.64259(13) 0.058(5) Uani 1 1 d . . .
F12 F 0.1057(6) 0.3724(4) 0.42701(9) 0.130(5) Uani 1 1 d . . .
F13 F -0.0358(6) 0.1903(4) 0.62768(11) 0.149(6) Uani 1 1 d . . .
F14 F 0.0592(4) 0.3851(6) 0.58541(10) 0.135(6) Uani 1 1 d . . .
C15 C 0.0693(6) 0.2361(6) 0.45054(11) 0.062(5) Uani 1 1 d . . .
C16 C 0.2746(3) 0.2849(3) 0.69265(7) 0.090(6) Uani 1 1 d . . .
C23 C 0.2692(5) 0.3204(4) 0.68401(8) 0.070(6) Uani 1 1 d G . .
C31 C 0.2839(6) 0.3155(5) 0.67254(7) 0.062(4) Uani 1 1 d G . .
C65 C 0.3041(6) 0.2751(6) 0.66972(7) 0.137(10) Uani 1 1 d G . .
C115 C 0.3095(7) 0.2396(6) 0.67836(9) 0.158(10) Uani 1 1 d G . .
C136 C 0.2948(5) 0.2445(4) 0.68983(8) 0.126(10) Uani 1 1 d G . .
C17 C 0.0870(7) 0.3483(6) 0.63041(12) 0.074(6) Uani 1 1 d . . .
F19 F 0.5215(5) 0.3553(6) 0.53829(15) 0.155(7) Uani 1 1 d . . .
F24 F 0.2993(6) 0.2076(4) 0.69733(12) 0.179(5) Uani 1 1 d . . .
F25 F 0.5785(5) 0.5393(5) 0.59304(10) 0.157(4) Uani 1 1 d . . .
C26 C 0.0410(7) 0.2960(8) 0.62562(15) 0.089(6) Uani 1 1 d . . .
C28 C 0.2658(6) 0.0882(7) 0.43445(16) 0.083(6) Uani 1 1 d . . .
C29 C 0.1580(5) 0.0581(5) 0.43431(13) 0.056(4) Uani 1 1 d . . .
C32 C 0.3833(6) 0.1170(8) 0.45939(19) 0.109(6) Uani 1 1 d . . .
C33 C 0.0449(7) 0.2750(7) 0.45188(16) 0.092(5) Uani 1 1 d . . .
F35 F 0.4784(6) 0.1534(9) 0.48535(16) 0.195(9) Uani 1 1 d . . .
C36 C 0.0635(7) 0.2975(6) 0.65001(15) 0.081(6) Uani 1 1 d . U .
C39 C 0.2542(7) 0.0487(8) 0.42588(15) 0.087(6) Uani 1 1 d . . .
C40 C 0.1877(8) 0.4503(7) 0.60588(18) 0.099(8) Uani 1 1 d . . .
C41 C 0.3407(7) 0.5003(6) 0.48162(19) 0.085(7) Uani 1 1 d . . .
C42 C 0.0174(10) 0.2446(9) 0.64440(18) 0.145(11) Uani 1 1 d . . .
C43 C 0.3289(3) 0.3051(3) 0.51696(8) 0.090(6) Uani 1 1 d . . .
C34 C 0.3356(5) 0.3254(4) 0.50550(8) 0.087(7) Uani 1 1 d G . .
C63 C 0.3787(7) 0.3853(5) 0.50276(11) 0.087(6) Uani 1 1 d G . .
C98 C 0.4151(6) 0.4250(4) 0.51147(14) 0.138(11) Uani 1 1 d G . .
C95 C 0.4084(5) 0.4048(4) 0.52293(13) 0.136(10) Uani 1 1 d G . .
C84 C 0.3653(5) 0.3449(4) 0.52567(9) 0.23(2) Uani 1 1 d G . .
F44 F -0.0176(10) 0.1959(6) 0.6508(2) 0.248(12) Uani 1 1 d . . .
C46 C 0.2190(7) 0.0911(7) 0.43995(19) 0.093(7) Uani 1 1 d . . .
F49 F 0.4449(7) 0.2607(8) 0.55072(14) 0.185(8) Uani 1 1 d . . .
C51 C 0.1295(12) 0.3930(11) 0.6016(2) 0.169(11) Uani 1 1 d . . .
C52 C 0.1251(3) 0.2422(2) 0.68510(6) 0.150(10) Uani 1 1 d D . .
C55 C 0.1216(5) 0.2889(3) 0.69076(7) 0.112(8) Uani 1 1 d DG . .
C68 C 0.1156(6) 0.2878(4) 0.70281(7) 0.136(9) Uani 1 1 d DG . .
C134 C 0.1132(6) 0.2399(4) 0.70920(6) 0.264(11) Uani 1 1 d G . .
C160 C 0.1167(6) 0.1932(4) 0.70354(7) 0.261(12) Uani 1 1 d G U .
C77 C 0.1227(5) 0.1943(3) 0.69149(7) 0.265(15) Uani 1 1 d G . .
C54 C 0.3745(6) 0.1354(10) 0.48304(14) 0.104(8) Uani 1 1 d . . .
C56 C 0.3270(5) 0.1149(8) 0.47583(15) 0.081(6) Uani 1 1 d . . .
F59 F 0.4393(8) 0.4534(8) 0.53009(14) 0.258(11) Uani 1 1 d . . .
C60 C 0.0984(8) 0.3295(7) 0.43413(14) 0.099(6) Uani 1 1 d . . .
F61 F 0.1919(6) -0.0154(7) 0.41134(12) 0.222(6) Uani 1 1 d . . .
F62 F 0.1210(8) 0.4896(11) 0.57705(14) 0.244(13) Uani 1 1 d . . .
C67 C 0.1509(6) 0.0236(7) 0.42519(17) 0.084(6) Uani 1 1 d . . .
C69 C 0.0084(8) 0.2451(9) 0.6324(2) 0.112(9) Uani 1 1 d . . .
F72 F 0.0312(7) 0.3497(6) 0.44431(18) 0.219(8) Uani 1 1 d . . .
C73 C 0.3672(8) 0.3238(6) 0.61228(16) 0.095(6) Uani 1 1 d . . .
C74 C 0.1069(9) 0.2468(7) 0.44110(17) 0.124(7) Uani 1 1 d . . .
C75 C 0.1969(8) 0.5252(8) 0.59109(15) 0.095(7) Uani 1 1 d . . .
F76 F 0.4652(6) 0.2675(8) 0.44429(18) 0.260(9) Uani 1 1 d . . .
C81 C 0.3193(9) 0.2604(8) 0.61909(17) 0.102(8) Uani 1 1 d . . .
C82 C 0.2571(5) 0.6441(6) 0.56615(16) 0.093(6) Uani 1 1 d D . .
C83 C 0.4318(7) 0.1361(9) 0.46659(17) 0.109(7) Uani 1 1 d . . .
C85 C 0.0544(8) 0.3171(6) 0.4444(2) 0.115(7) Uani 1 1 d . . .
C87 C 0.1170(11) 0.2905(8) 0.43257(19) 0.117(9) Uani 1 1 d . . .
C88 C 0.1987(7) 0.0179(8) 0.42122(17) 0.102(7) Uani 1 1 d . . .
C91 C 0.3471(15) 0.3081(11) 0.59928(19) 0.162(16) Uani 1 1 d . . .
F92 F 0.4554(12) 0.4795(8) 0.5087(2) 0.289(16) Uani 1 1 d . . .
C93 C 0.3062(9) 0.5619(10) 0.4936(2) 0.122(10) Uani 1 1 d . . .
F94 F 0.4436(9) 0.2561(16) 0.4688(4) 0.47(2) Uani 1 1 d . . .
F96 F 0.3209(7) 0.1965(5) 0.67530(18) 0.252(8) Uani 1 1 d . . .
C97 C 0.1410(9) 0.4756(10) 0.58744(16) 0.118(9) Uani 1 1 d . . .
C99 C 0.4308(6) 0.1479(9) 0.4783(2) 0.133(8) Uani 1 1 d . U .
C100 C 0.2837(7) 0.1968(7) 0.6410(3) 0.163(12) Uani 1 1 d . . .
C102 C 0.1135(9) 0.4193(7) 0.5925(2) 0.151(9) Uani 1 1 d . . .
C106 C 0.3408(14) 0.4416(11) 0.4530(3) 0.178(15) Uani 1 1 d . . .
C108 C 0.3874(11) 0.4904(7) 0.4748(2) 0.142(10) Uani 1 1 d . U .
C116 C 0.4086(8) 0.2723(7) 0.63622(19) 0.135(7) Uani 1 1 d . . .
C125 C 0.2252(3) 0.6768(6) 0.57241(16) 0.152(8) Uani 1 1 d D . .
C140 C 0.4562(3) 0.3992(4) 0.47252(10) 0.33(4) Uani 1 1 d D . .
F143 F 0.1148(15) 0.2036(17) 0.71800(17) 0.53(3) Uani 1 1 d . . .
F145 F 0.1248(13) 0.1399(13) 0.7027(3) 0.320(15) Uiso 1 1 d . . .
C148 C 0.4361(9) 0.2847(7) 0.6485(2) 0.141(8) Uani 1 1 d . . .
C149 C 0.3639(4) 0.2493(4) 0.44055(10) 0.203(14) Uani 1 1 d . . .
C112 C 0.3082(4) 0.2390(6) 0.44490(11) 0.157(12) Uani 1 1 d G . .
C57 C 0.2993(6) 0.2382(7) 0.45686(12) 0.126(7) Uani 1 1 d G U .
C45 C 0.3460(7) 0.2478(7) 0.46448(10) 0.130(9) Uani 1 1 d G . .
C110 C 0.4017(6) 0.2582(7) 0.46013(10) 0.166(13) Uani 1 1 d G . .
C114 C 0.4107(5) 0.2590(6) 0.44817(11) 0.178(10) Uani 1 1 d G . .
C154 C 0.3178(12) 0.3860(10) 0.44490(12) 0.155(12) Uani 1 1 d D . .
C157 C 0.3595(13) 0.5574(12) 0.4876(3) 0.203(14) Uani 1 1 d . . .
C163 C 0.3927(15) 0.3715(11) 0.5922(2) 0.180(17) Uani 1 1 d . . .
C174 C 0.4297(5) 0.4188(5) 0.46275(9) 0.156(10) Uani 1 1 d D . .
C183 C 0.1395(6) 0.6960(8) 0.5761(4) 0.357(19) Uani 1 1 d D . .
C192 C 0.4950(15) 0.2824(15) 0.6481(3) 0.197(18) Uani 1 1 d . . .
C193 C 0.1607(3) 0.6487(10) 0.56827(19) 0.208(16) Uani 1 1 d D . .
C1 C 0.2234(11) 0.1887(7) 0.6421(3) 0.151(11) Uani 1 1 d . . .
C2 C 0.1124(13) 0.1282(15) 0.6505(3) 0.304(17) Uani 1 1 d . . .
C4 C 0.1813(16) 0.1357(11) 0.6496(3) 0.244(16) Uani 1 1 d . . .
C113 C 0.2950(13) 0.4128(5) 0.43339(10) 0.29(3) Uani 1 1 d D . .
C121 C -0.1120(3) -0.0062(4) 0.40632(13) 0.41(2) Uani 1 1 d D . .
C141 C 0.5094(3) 0.3917(4) 0.47606(9) 0.35(2) Uani 1 1 d D . .
C198 C 0.5262(6) 0.3638(5) 0.48592(10) 0.52(3) Uani 1 1 d D . .
C5 C 0.5305(16) 0.3049(15) 0.6587(4) 0.23(2) Uani 1 1 d . . .
F9 F 0.1094(8) 0.2126(8) 0.62997(18) 0.199(8) Uiso 1 1 d . . .
F16 F 0.1034(8) 0.2058(6) 0.60733(16) 0.231(8) Uani 1 1 d . . .
C179 C 0.1484(3) 0.2581(3) 0.62405(8) 0.141(12) Uani 1 1 d . . .
C14 C 0.1953(4) 0.3091(3) 0.62950(9) 0.085(6) Uani 1 1 d G . .
C47 C 0.2390(4) 0.3571(3) 0.62286(12) 0.078(5) Uani 1 1 d G . .
C119 C 0.2358(6) 0.3541(4) 0.61077(12) 0.118(8) Uani 1 1 d G . .
C129 C 0.1889(7) 0.3031(5) 0.60531(9) 0.162(11) Uani 1 1 d G . .
C38 C 0.1452(5) 0.2551(4) 0.61195(8) 0.214(11) Uani 1 1 d G . .
F18 F 0.6345(5) 0.6099(9) 0.61075(16) 0.233(9) Uani 1 1 d . . .
Br29 Br 0.4738(14) 0.4863(19) 0.5631(2) 0.60(3) Uani 0.3333 1 d . . .
C13 C -0.2069(3) -0.0128(4) 0.41392(9) 0.40(3) Uani 1 1 d D . .
C0AA C -0.0840(4) -0.0383(4) 0.40012(13) 0.240(19) Uani 1 1 d D . .
C177 C -0.2600(3) -0.0082(5) 0.40935(19) 0.60(4) Uani 1 1 d D U .
C184 C -0.1797(3) -0.0347(4) 0.40478(10) 0.60(6) Uani 1 1 d D . .
C294 C 0.2847(10) 0.3663(5) 0.42423(9) 0.27(2) Uani 1 1 d D . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ag1 Ag1 Ag1 60.002(1) 2_665 3_565
Ag1 Ag1 Ag5 59.39(2) 3_565 3_565
Ag1 Ag1 Ag5 89.83(2) 2_665 3_565
Ag1 Ag1 Ag8 126.68(3) 3_565 3_565
Ag1 Ag1 Ag8 67.20(3) 2_665 3_565
Ag1 Ag1 Ag8 116.20(3) 2_665 2_665
Ag1 Ag1 Ag8 56.62(3) 3_565 2_665
Ag2 Ag1 Ag1 121.39(2) 3_565 2_665
Ag2 Ag1 Ag1 118.32(3) 3_565 3_565
Ag2 Ag1 Ag5 58.97(2) 3_565 3_565
Ag2 Ag1 Ag5 60.67(2) 3_565 .
Ag2 Ag1 Ag8 94.68(3) 3_565 2_665
Ag2 Ag1 Ag8 94.43(3) 3_565 3_565
Ag5 Ag1 Ag1 60.78(2) . 2_665
Ag5 Ag1 Ag1 90.64(2) . 3_565
Ag5 Ag1 Ag5 60.39(3) . 3_565
Ag5 Ag1 Ag8 64.54(3) 3_565 2_665
Ag5 Ag1 Ag8 124.75(3) . 2_665
Ag5 Ag1 Ag8 69.10(3) . 3_565
Ag8 Ag1 Ag5 129.40(3) 3_565 3_565
Ag8 Ag1 Ag8 166.04(4) 3_565 2_665
S1 Ag1 Ag1 79.92(6) 3_565 2_665
S1 Ag1 Ag1 107.09(6) 3_565 3_565
S1 Ag1 Ag2 134.58(6) 3_565 3_565
S1 Ag1 Ag5 166.17(6) 3_565 3_565
S1 Ag1 Ag5 120.55(8) 3_565 .
S1 Ag1 Ag8 111.75(8) 3_565 2_665
S1 Ag1 Ag8 54.62(8) 3_565 3_565
S1 Ag1 S2 109.50(9) 3_565 2_665
S2 Ag1 Ag1 165.79(6) 2_665 2_665
S2 Ag1 Ag1 106.29(6) 2_665 3_565
S2 Ag1 Ag2 59.82(6) 2_665 3_565
S2 Ag1 Ag5 79.00(6) 2_665 3_565
S2 Ag1 Ag5 119.10(7) 2_665 .
S2 Ag1 Ag8 50.94(5) 2_665 2_665
S2 Ag1 Ag8 126.83(6) 2_665 3_565
Ag1 Ag2 Ag4 121.67(3) 2_665 14_456
Ag1 Ag2 Ag4 119.86(3) 2_665 .
Ag1 Ag2 Ag5 59.93(2) 2_665 2_665
Ag1 Ag2 Ag6 86.27(3) 2_665 .
Ag1 Ag2 Ag7 179.62(4) 2_665 15_556
Ag1 Ag2 Ag9 95.47(3) 2_665 .
Ag4 Ag2 Ag4 60.181(19) . 14_456
Ag4 Ag2 Ag5 59.95(2) . 2_665
Ag4 Ag2 Ag6 121.31(3) 14_456 .
Ag4 Ag2 Ag6 61.16(3) . .
Ag4 Ag2 Ag7 60.17(3) . 15_556
Ag4 Ag2 Ag7 58.70(2) 14_456 15_556
Ag4 Ag2 Ag9 119.30(3) . .
Ag4 Ag2 Ag9 59.31(2) 14_456 .
Ag5 Ag2 Ag1 61.50(2) . 2_665
Ag5 Ag2 Ag4 90.56(2) 2_665 14_456
Ag5 Ag2 Ag4 60.18(2) . 14_456
Ag5 Ag2 Ag4 90.56(2) . .
Ag5 Ag2 Ag5 60.99(3) . 2_665
Ag5 Ag2 Ag6 58.12(2) 2_665 .
Ag5 Ag2 Ag6 119.07(3) . .
Ag5 Ag2 Ag7 120.11(3) 2_665 15_556
Ag5 Ag2 Ag7 118.87(3) . 15_556
Ag5 Ag2 Ag9 124.47(3) 2_665 .
Ag5 Ag2 Ag9 63.53(2) . .
Ag7 Ag2 Ag6 93.44(3) 15_556 .
Ag9 Ag2 Ag6 177.39(3) . .
Ag9 Ag2 Ag7 84.81(3) . 15_556
S2 Ag2 Ag1 56.06(7) 3_565 2_665
S2 Ag2 Ag4 168.96(6) 3_565 .
S2 Ag2 Ag4 111.93(6) 3_565 14_456
S2 Ag2 Ag5 114.71(7) 3_565 2_665
S2 Ag2 Ag5 78.51(6) 3_565 .
S2 Ag2 Ag6 125.78(6) 3_565 .
S2 Ag2 Ag7 123.99(8) 3_565 15_556
S2 Ag2 Ag9 54.24(6) 3_565 .
S5 Ag2 Ag1 123.71(8) . 2_665
S5 Ag2 Ag4 79.31(8) . .
S5 Ag2 Ag4 113.75(8) . 14_456
S5 Ag2 Ag5 112.77(8) . 2_665
S5 Ag2 Ag5 169.87(8) . .
S5 Ag2 Ag6 55.69(8) . .
S5 Ag2 Ag7 55.91(8) . 15_556
S5 Ag2 Ag9 121.71(8) . .
S5 Ag2 S2 111.62(10) . 3_565
S1 Ag3 S1 92.87(9) 3_565 .
S1 Ag3 S1 92.86(9) 3_565 2_665
S1 Ag3 S1 92.87(9) . 2_665
P13 Ag3 S1 123.20(7) . .
P13 Ag3 S1 123.21(6) . 3_565
P13 Ag3 S1 123.21(7) . 2_665
Ag2 Ag4 Ag2 178.61(3) . 15_556
Ag2 Ag4 Ag4 60.33(3) . 14_456
Ag2 Ag4 Ag4 119.97(3) . 15_556
Ag2 Ag4 Ag5 120.18(3) . 15_556
Ag2 Ag4 Ag5 60.24(2) . 2_665
Ag2 Ag4 Ag6 60.64(3) . .
Ag2 Ag4 Ag6 120.35(3) 15_556 .
Ag2 Ag4 Ag7 60.41(2) . 15_556
Ag2 Ag4 Ag15 89.56(2) . .
Ag2 Ag4 Ag21 89.69(3) 15_556 .
Ag2 Ag4 Ag21 91.67(3) . .
Ag4 Ag4 Ag2 118.64(3) 14_456 15_556
Ag4 Ag4 Ag2 59.50(3) 15_556 15_556
Ag4 Ag4 Ag4 119.991(2) 15_556 14_456
Ag4 Ag4 Ag6 88.06(3) 15_556 .
Ag4 Ag4 Ag6 120.93(4) 14_456 .
Ag4 Ag4 Ag7 178.57(4) 15_556 15_556
Ag4 Ag4 Ag7 58.83(3) 14_456 15_556
Ag4 Ag4 Ag15 60.0 15_556 .
Ag4 Ag4 Ag21 118.19(3) 15_556 .
Ag4 Ag4 Ag21 121.81(3) 14_456 .
Ag5 Ag4 Ag2 119.22(3) 2_665 15_556
Ag5 Ag4 Ag2 58.78(2) 15_556 15_556
Ag5 Ag4 Ag4 59.73(2) 2_665 15_556
Ag5 Ag4 Ag4 89.35(3) 15_556 15_556
Ag5 Ag4 Ag4 59.86(2) 15_556 14_456
Ag5 Ag4 Ag4 90.81(2) 2_665 14_456
Ag5 Ag4 Ag5 119.78(3) 15_556 2_665
Ag5 Ag4 Ag6 58.04(2) 2_665 .
Ag5 Ag4 Ag6 177.28(3) 15_556 .
Ag5 Ag4 Ag7 89.30(3) 15_556 15_556
Ag5 Ag4 Ag7 120.65(3) 2_665 15_556
Ag5 Ag4 Ag15 59.917(18) 15_556 .
Ag5 Ag4 Ag15 59.870(18) 2_665 .
Ag5 Ag4 Ag21 119.71(3) 2_665 .
Ag5 Ag4 Ag21 120.44(3) 15_556 .
Ag6 Ag4 Ag21 61.68(3) . .
Ag7 Ag4 Ag2 120.31(3) 2_665 .
Ag7 Ag4 Ag2 120.08(3) 15_556 15_556
Ag7 Ag4 Ag2 60.73(3) 2_665 15_556
Ag7 Ag4 Ag4 60.62(3) 2_665 15_556
Ag7 Ag4 Ag4 178.92(4) 2_665 14_456
Ag7 Ag4 Ag5 90.27(3) 2_665 2_665
Ag7 Ag4 Ag5 119.51(3) 2_665 15_556
Ag7 Ag4 Ag6 59.75(3) 2_665 .
Ag7 Ag4 Ag6 93.27(3) 15_556 .
Ag7 Ag4 Ag7 120.55(3) 2_665 15_556
Ag7 Ag4 Ag9 86.50(3) 2_665 15_556
Ag7 Ag4 Ag15 120.62(3) 2_665 .
Ag7 Ag4 Ag21 57.57(3) 2_665 .
Ag7 Ag4 Ag21 62.99(2) 15_556 .
Ag9 Ag4 Ag2 120.21(3) 15_556 .
Ag9 Ag4 Ag2 60.42(3) 15_556 15_556
Ag9 Ag4 Ag4 119.72(4) 15_556 15_556
Ag9 Ag4 Ag4 92.42(4) 15_556 14_456
Ag9 Ag4 Ag5 63.44(2) 15_556 15_556
Ag9 Ag4 Ag5 176.37(3) 15_556 2_665
Ag9 Ag4 Ag6 118.69(3) 15_556 .
Ag9 Ag4 Ag7 60.01(3) 15_556 15_556
Ag9 Ag4 Ag15 123.35(3) 15_556 .
Ag9 Ag4 Ag21 57.02(2) 15_556 .
Ag15 Ag4 Ag2 89.084(19) . 15_556
Ag15 Ag4 Ag4 60.0 . 14_456
Ag15 Ag4 Ag6 117.90(2) . .
Ag15 Ag4 Ag7 118.83(3) . 15_556
Ag15 Ag4 Ag21 178.17(4) . .
Ag1 Ag5 Ag1 59.84(3) . 2_665
Ag1 Ag5 Ag2 59.40(2) . 3_565
Ag1 Ag5 Ag4 179.12(4) . 14_456
Ag1 Ag5 Ag4 119.20(3) . 3_565
Ag1 Ag5 Ag5 60.495(19) . 3_565
Ag1 Ag5 Ag5 90.15(2) . 2_665
Ag1 Ag5 Ag8 62.01(2) 2_665 3_565
Ag1 Ag5 Ag8 55.86(3) . 3_565
Ag1 Ag5 Ag9 121.17(3) . .
Ag1 Ag5 Ag9 91.83(3) 2_665 .
Ag1 Ag5 Ag15 120.23(2) . .
Ag2 Ag5 Ag1 119.35(3) . .
Ag2 Ag5 Ag1 119.18(3) 3_565 2_665
Ag2 Ag5 Ag1 59.54(3) . 2_665
Ag2 Ag5 Ag2 178.60(4) . 3_565
Ag2 Ag5 Ag4 61.03(2) . 14_456
Ag2 Ag5 Ag4 121.45(3) . 3_565
Ag2 Ag5 Ag5 120.41(3) . 3_565
Ag2 Ag5 Ag5 60.41(3) . 2_665
Ag2 Ag5 Ag5 58.60(2) 3_565 3_565
Ag2 Ag5 Ag5 118.60(2) 3_565 2_665
Ag2 Ag5 Ag6 118.93(3) . 3_565
Ag2 Ag5 Ag8 93.47(3) . 3_565
Ag2 Ag5 Ag8 86.26(3) 3_565 3_565
Ag2 Ag5 Ag9 59.36(3) . .
Ag2 Ag5 Ag9 121.67(3) 3_565 .
Ag2 Ag5 Ag15 90.64(2) . .
Ag4 Ag5 Ag1 120.56(3) 14_456 2_665
Ag4 Ag5 Ag1 178.46(3) 3_565 2_665
Ag4 Ag5 Ag2 120.23(3) 14_456 3_565
Ag4 Ag5 Ag2 59.82(2) 3_565 3_565
Ag4 Ag5 Ag4 60.412(15) 14_456 3_565
Ag4 Ag5 Ag5 120.117(18) 14_456 3_565
Ag4 Ag5 Ag5 90.72(3) 14_456 2_665
Ag4 Ag5 Ag5 120.068(17) 3_565 2_665
Ag4 Ag5 Ag5 89.10(2) 3_565 3_565
Ag4 Ag5 Ag8 123.49(3) 14_456 3_565
Ag4 Ag5 Ag8 118.67(3) 3_565 3_565
Ag4 Ag5 Ag9 89.71(3) 3_565 .
Ag4 Ag5 Ag9 58.22(2) 14_456 .
Ag4 Ag5 Ag15 60.338(18) 3_565 .
Ag4 Ag5 Ag15 60.387(17) 14_456 .
Ag5 Ag5 Ag1 59.12(2) 2_665 2_665
Ag5 Ag5 Ag1 89.36(2) 3_565 2_665
Ag5 Ag5 Ag5 59.999(1) 3_565 2_665
Ag5 Ag5 Ag8 120.96(2) 2_665 3_565
Ag5 Ag5 Ag8 116.29(2) 3_565 3_565
Ag5 Ag5 Ag9 178.31(2) 3_565 .
Ag5 Ag5 Ag9 119.72(4) 2_665 .
Ag6 Ag5 Ag1 88.15(3) 3_565 .
Ag6 Ag5 Ag1 118.34(3) 3_565 2_665
Ag6 Ag5 Ag2 62.01(3) 3_565 3_565
Ag6 Ag5 Ag4 90.97(3) 3_565 14_456
Ag6 Ag5 Ag4 62.47(3) 3_565 3_565
Ag6 Ag5 Ag5 120.57(3) 3_565 3_565
Ag6 Ag5 Ag5 177.45(2) 3_565 2_665
Ag6 Ag5 Ag8 56.48(2) 3_565 3_565
Ag6 Ag5 Ag9 59.79(3) 3_565 .
Ag6 Ag5 Ag15 122.80(3) 3_565 .
Ag9 Ag5 Ag8 65.36(3) . 3_565
Ag15 Ag5 Ag1 118.85(3) . 2_665
Ag15 Ag5 Ag2 89.59(2) . 3_565
Ag15 Ag5 Ag5 59.739(11) . 3_565
Ag15 Ag5 Ag5 59.739(11) . 2_665
Ag15 Ag5 Ag8 175.46(3) . 3_565
Ag15 Ag5 Ag9 118.60(3) . .
Ag2 Ag6 Ag4 58.20(3) . .
Ag2 Ag6 Ag21 90.73(3) . .
Ag4 Ag6 Ag21 62.38(3) . .
Ag5 Ag6 Ag2 59.87(2) 2_665 .
Ag5 Ag6 Ag4 59.50(2) 2_665 .
Ag5 Ag6 Ag7 90.15(3) 2_665 2_665
Ag5 Ag6 Ag8 69.28(3) 2_665 .
Ag5 Ag6 Ag9 63.27(2) 2_665 2_665
Ag5 Ag6 Ag21 121.86(3) 2_665 .
Ag7 Ag6 Ag2 116.23(3) 2_665 .
Ag7 Ag6 Ag4 58.09(2) 2_665 .
Ag7 Ag6 Ag8 130.66(4) 2_665 .
Ag7 Ag6 Ag9 59.44(3) 2_665 2_665
Ag7 Ag6 Ag21 57.37(3) 2_665 .
Ag8 Ag6 Ag2 92.04(3) . .
Ag8 Ag6 Ag4 128.43(3) . .
Ag8 Ag6 Ag9 71.31(3) . 2_665
Ag8 Ag6 Ag21 168.07(3) . .
Ag9 Ag6 Ag2 123.01(3) 2_665 .
Ag9 Ag6 Ag4 90.01(3) 2_665 .
Ag9 Ag6 Ag21 116.46(4) 2_665 .
S4 Ag6 Ag2 135.66(8) . .
S4 Ag6 Ag4 165.00(8) . .
S4 Ag6 Ag5 118.95(6) . 2_665
S4 Ag6 Ag7 107.99(8) . 2_665
S4 Ag6 Ag8 54.53(7) . .
S4 Ag6 Ag9 77.03(7) . 2_665
S4 Ag6 Ag21 116.69(7) . .
S4 Ag6 S5 113.89(9) . .
S5 Ag6 Ag2 56.02(7) . .
S5 Ag6 Ag4 77.86(7) . .
S5 Ag6 Ag5 114.82(8) . 2_665
S5 Ag6 Ag7 107.36(8) . 2_665
S5 Ag6 Ag8 121.96(8) . .
S5 Ag6 Ag9 165.91(8) . 2_665
S5 Ag6 Ag21 51.41(8) . .
Ag2 Ag7 Ag21 90.97(3) 14_456 14_456
Ag2 Ag7 Ag21 94.93(3) 14_456 3_565
Ag4 Ag7 Ag2 60.57(2) 3_565 14_456
Ag4 Ag7 Ag2 59.43(3) 14_456 14_456
Ag4 Ag7 Ag4 60.55(3) 3_565 14_456
Ag4 Ag7 Ag6 62.16(3) 3_565 3_565
Ag4 Ag7 Ag9 93.20(3) 3_565 .
Ag4 Ag7 Ag21 127.38(3) 14_456 3_565
Ag4 Ag7 Ag21 62.69(3) 14_456 14_456
Ag4 Ag7 Ag21 123.25(3) 3_565 14_456
Ag4 Ag7 Ag21 66.82(3) 3_565 3_565
Ag6 Ag7 Ag2 122.60(3) 3_565 14_456
Ag6 Ag7 Ag4 89.35(3) 3_565 14_456
Ag6 Ag7 Ag21 65.70(3) 3_565 3_565
Ag6 Ag7 Ag21 117.48(3) 3_565 14_456
Ag9 Ag7 Ag2 118.78(4) . 14_456
Ag9 Ag7 Ag4 59.55(3) . 14_456
Ag9 Ag7 Ag6 60.78(3) . 3_565
Ag9 Ag7 Ag21 56.81(3) . 14_456
Ag9 Ag7 Ag21 126.04(4) . 3_565
Ag21 Ag7 Ag21 169.93(4) 3_565 14_456
S5 Ag7 Ag2 56.73(6) 14_456 14_456
S5 Ag7 Ag4 79.31(7) 14_456 14_456
S5 Ag7 Ag4 116.39(6) 14_456 3_565
S5 Ag7 Ag6 166.82(8) 14_456 3_565
S5 Ag7 Ag9 107.11(9) 14_456 .
S5 Ag7 Ag21 51.10(8) 14_456 14_456
S5 Ag7 Ag21 126.80(9) 14_456 3_565
S10 Ag7 Ag2 134.40(9) 3_565 14_456
S10 Ag7 Ag4 118.12(10) 3_565 3_565
S10 Ag7 Ag4 165.12(9) 3_565 14_456
S10 Ag7 Ag6 77.93(9) 3_565 3_565
S10 Ag7 Ag9 106.79(8) 3_565 .
S10 Ag7 Ag21 53.90(9) 3_565 3_565
S10 Ag7 Ag21 116.48(9) 3_565 14_456
S10 Ag7 S5 112.25(11) 3_565 14_456
Ag1 Ag8 Ag1 56.18(3) 2_665 3_565
Ag1 Ag8 Ag5 53.45(2) 3_565 2_665
Ag1 Ag8 Ag5 55.05(2) 2_665 2_665
Ag1 Ag8 Ag6 86.15(3) 2_665 .
Ag6 Ag8 Ag1 107.57(3) . 3_565
Ag6 Ag8 Ag5 54.25(2) . 2_665
S1 Ag8 Ag1 55.57(7) . 2_665
S1 Ag8 Ag1 74.36(6) . 3_565
S1 Ag8 Ag5 108.10(8) . 2_665
S1 Ag8 Ag6 133.57(8) . .
S1 Ag8 S2 112.96(9) . .
S1 Ag8 S4 136.56(9) . .
S2 Ag8 Ag1 107.87(8) . 2_665
S2 Ag8 Ag1 52.99(7) . 3_565
S2 Ag8 Ag5 73.43(7) . 2_665
S2 Ag8 Ag6 102.50(7) . .
S4 Ag8 Ag1 149.04(7) . 3_565
S4 Ag8 Ag1 135.66(8) . 2_665
S4 Ag8 Ag5 105.89(7) . 2_665
S4 Ag8 Ag6 55.47(7) . .
S4 Ag8 S2 102.04(10) . .
Ag2 Ag9 Ag5 57.11(2) . .
Ag2 Ag9 Ag6 113.85(3) . 3_565
Ag4 Ag9 Ag2 60.27(3) 14_456 .
Ag4 Ag9 Ag5 58.34(2) 14_456 .
Ag4 Ag9 Ag6 89.28(3) 14_456 3_565
Ag4 Ag9 Ag7 60.43(3) 14_456 .
Ag4 Ag9 Ag21 66.67(3) 14_456 14_456
Ag6 Ag9 Ag5 56.93(2) 3_565 .
Ag7 Ag9 Ag2 120.36(3) . .
Ag7 Ag9 Ag5 86.74(3) . .
Ag7 Ag9 Ag6 59.78(3) . 3_565
Ag7 Ag9 Ag21 66.70(3) . 14_456
Ag21 Ag9 Ag2 95.25(3) 14_456 .
Ag21 Ag9 Ag5 125.00(3) 14_456 .
Ag21 Ag9 Ag6 126.35(4) 14_456 3_565
S2 Ag9 Ag2 59.63(6) 3_565 .
S2 Ag9 Ag4 118.08(7) 3_565 14_456
S2 Ag9 Ag5 77.68(8) 3_565 .
S2 Ag9 Ag6 101.70(7) 3_565 3_565
S2 Ag9 Ag7 160.72(8) 3_565 .
S2 Ag9 Ag21 131.93(7) 3_565 14_456
S2 Ag9 S7 116.47(11) 3_565 14_456
S7 Ag9 Ag2 138.06(9) 14_456 .
S7 Ag9 Ag4 117.20(8) 14_456 14_456
S7 Ag9 Ag5 162.42(9) 14_456 .
S7 Ag9 Ag6 107.83(9) 14_456 3_565
S7 Ag9 Ag7 77.14(8) 14_456 .
S7 Ag9 Ag21 54.40(8) 14_456 14_456
S3 Ag10 S3 92.82(10) 3 .
S3 Ag10 S3 92.82(10) 3 2
S3 Ag10 S3 92.82(10) 2 .
P16 Ag10 S3 123.24(7) . 2
P16 Ag10 S3 123.25(7) . .
P16 Ag10 S3 123.24(7) . 3
Ag11 Ag11 Ag11 60.0 3 2
Ag11 Ag11 Ag13 59.54(2) 3 3
Ag11 Ag11 Ag13 89.941(19) 2 3
Ag11 Ag11 Ag23 67.19(5) 2 .
Ag11 Ag11 Ag23 56.61(3) 3 3
Ag11 Ag11 Ag23 116.23(3) 2 3
Ag11 Ag11 Ag23 126.72(5) 3 .
Ag13 Ag11 Ag11 90.60(2) . 3
Ag13 Ag11 Ag11 60.68(3) . 2
Ag13 Ag11 Ag13 60.42(3) . 3
Ag13 Ag11 Ag23 124.52(3) . 3
Ag13 Ag11 Ag23 68.74(3) . .
Ag13 Ag11 Ag23 64.29(3) 3 3
Ag14 Ag11 Ag11 118.76(2) . 3
Ag14 Ag11 Ag11 121.21(3) . 2
Ag14 Ag11 Ag13 59.24(3) . 3
Ag14 Ag11 Ag13 60.58(3) . .
Ag14 Ag11 Ag23 94.95(4) . 3
Ag14 Ag11 Ag23 93.60(3) . .
Ag23 Ag11 Ag13 129.04(4) . 3
Ag23 Ag11 Ag23 166.66(5) . 3
S3 Ag11 Ag11 79.85(10) . 2
S3 Ag11 Ag11 107.14(7) . 3
S3 Ag11 Ag13 120.33(9) . .
S3 Ag11 Ag13 166.36(8) . 3
S3 Ag11 Ag14 134.08(7) . .
S3 Ag11 Ag23 112.19(8) . 3
S3 Ag11 Ag23 54.82(7) . .
S3 Ag11 S6 109.98(12) . 3
S6 Ag11 Ag11 165.55(10) 3 2
S6 Ag11 Ag11 106.14(10) 3 3
S6 Ag11 Ag13 118.89(8) 3 .
S6 Ag11 Ag13 78.53(8) 3 3
S6 Ag11 Ag14 59.88(8) 3 .
S6 Ag11 Ag23 127.01(10) 3 .
S6 Ag11 Ag23 50.80(10) 3 3
Ag12 Ag12 Ag12 119.993(1) 12_556 11_556
Ag12 Ag12 Ag14 59.39(3) 12_556 12_556
Ag12 Ag12 Ag14 118.79(4) 11_556 12_556
Ag12 Ag12 Ag18 178.87(4) 12_556 .
Ag12 Ag12 Ag18 58.96(3) 11_556 .
Ag12 Ag12 Ag20 121.21(4) 11_556 .
Ag12 Ag12 Ag20 87.68(4) 12_556 .
Ag12 Ag12 Ag24 118.19(4) 12_556 .
Ag12 Ag12 Ag24 121.81(4) 11_556 .
Ag13 Ag12 Ag12 89.42(3) 11_556 12_556
Ag13 Ag12 Ag12 90.67(3) . 11_556
Ag13 Ag12 Ag12 59.59(3) . 12_556
Ag13 Ag12 Ag12 59.84(3) 11_556 11_556
Ag13 Ag12 Ag13 119.53(3) 11_556 .
Ag13 Ag12 Ag14 58.96(3) 11_556 12_556
Ag13 Ag12 Ag14 120.20(3) 11_556 .
Ag13 Ag12 Ag14 118.97(4) . 12_556
Ag13 Ag12 Ag18 89.62(3) 11_556 .
Ag13 Ag12 Ag18 120.46(4) . .
Ag13 Ag12 Ag20 177.01(4) 11_556 .
Ag13 Ag12 Ag20 58.18(2) . .
Ag13 Ag12 Ag22 59.728(18) . .
Ag13 Ag12 Ag22 59.811(17) 11_556 .
Ag13 Ag12 Ag24 119.73(3) . .
Ag13 Ag12 Ag24 120.67(3) 11_556 .
Ag14 Ag12 Ag12 119.74(4) . 12_556
Ag14 Ag12 Ag12 60.37(3) . 11_556
Ag14 Ag12 Ag13 60.15(3) . .
Ag14 Ag12 Ag14 178.52(4) . 12_556
Ag14 Ag12 Ag18 60.32(3) . .
Ag14 Ag12 Ag20 119.90(3) 12_556 .
Ag14 Ag12 Ag20 60.87(3) . .
Ag14 Ag12 Ag22 89.54(2) . .
Ag14 Ag12 Ag24 89.89(3) 12_556 .
Ag14 Ag12 Ag24 91.58(3) . .
Ag16 Ag12 Ag12 92.76(4) 11_556 11_556
Ag16 Ag12 Ag12 119.71(4) 11_556 12_556
Ag16 Ag12 Ag13 63.78(3) 11_556 11_556
Ag16 Ag12 Ag13 176.21(3) 11_556 .
Ag16 Ag12 Ag14 120.42(4) 11_556 .
Ag16 Ag12 Ag14 60.54(3) 11_556 12_556
Ag16 Ag12 Ag18 60.32(3) 11_556 .
Ag16 Ag12 Ag20 118.44(3) 11_556 .
Ag16 Ag12 Ag22 123.58(3) 11_556 .
Ag16 Ag12 Ag24 56.90(3) 11_556 .
Ag18 Ag12 Ag12 60.57(4) 12_556 12_556
Ag18 Ag12 Ag12 178.91(5) 12_556 11_556
Ag18 Ag12 Ag13 119.48(4) 12_556 11_556
Ag18 Ag12 Ag13 90.42(3) 12_556 .
Ag18 Ag12 Ag14 60.54(3) 12_556 12_556
Ag18 Ag12 Ag14 120.32(3) 12_556 .
Ag18 Ag12 Ag14 120.52(3) . 12_556
Ag18 Ag12 Ag16 86.16(3) 12_556 11_556
Ag18 Ag12 Ag18 120.46(3) 12_556 .
Ag18 Ag12 Ag20 59.52(3) 12_556 .
Ag18 Ag12 Ag20 93.27(3) . .
Ag18 Ag12 Ag22 120.57(4) 12_556 .
Ag18 Ag12 Ag24 57.61(3) 12_556 .
Ag18 Ag12 Ag24 62.85(3) . .
Ag20 Ag12 Ag24 61.55(3) . .
Ag22 Ag12 Ag12 60.0 . 12_556
Ag22 Ag12 Ag12 60.0 . 11_556
Ag22 Ag12 Ag14 88.98(3) . 12_556
Ag22 Ag12 Ag18 118.96(3) . .
Ag22 Ag12 Ag20 117.90(3) . .
Ag22 Ag12 Ag24 178.18(4) . .
Ag11 Ag13 Ag11 59.78(4) . 2
Ag11 Ag13 Ag12 119.17(4) . .
Ag11 Ag13 Ag12 179.21(4) . 12_556
Ag11 Ag13 Ag13 59.23(2) 2 2
Ag11 Ag13 Ag13 90.040(19) . 2
Ag11 Ag13 Ag13 60.35(2) . 3
Ag11 Ag13 Ag13 89.39(2) 2 3
Ag11 Ag13 Ag14 59.31(3) . .
Ag11 Ag13 Ag16 91.57(3) 2 .
Ag11 Ag13 Ag16 121.32(3) . .
Ag11 Ag13 Ag22 120.03(3) . .
Ag11 Ag13 Ag23 55.93(3) . .
Ag11 Ag13 Ag23 62.16(3) 2 .
Ag12 Ag13 Ag11 120.49(4) 12_556 2
Ag12 Ag13 Ag11 178.55(4) . 2
Ag12 Ag13 Ag12 60.573(16) 12_556 .
Ag12 Ag13 Ag13 120.184(18) . 2
Ag12 Ag13 Ag13 90.72(3) 12_556 2
Ag12 Ag13 Ag13 89.19(3) . 3
Ag12 Ag13 Ag13 120.267(18) 12_556 3
Ag12 Ag13 Ag14 59.87(3) . .
Ag12 Ag13 Ag14 120.44(3) 12_556 .
Ag12 Ag13 Ag16 58.07(3) 12_556 .
Ag12 Ag13 Ag16 89.86(3) . .
Ag12 Ag13 Ag22 60.59(2) 12_556 .
Ag12 Ag13 Ag23 123.42(3) 12_556 .
Ag12 Ag13 Ag23 118.30(3) . .
Ag13 Ag13 Ag13 60.0 2 3
Ag13 Ag13 Ag16 178.34(3) 3 .
Ag13 Ag13 Ag16 119.45(5) 2 .
Ag13 Ag13 Ag23 121.21(2) 2 .
Ag13 Ag13 Ag23 116.19(3) 3 .
Ag14 Ag13 Ag11 119.05(3) . 2
Ag14 Ag13 Ag11 59.41(3) 2 2
Ag14 Ag13 Ag11 119.17(4) 2 .
Ag14 Ag13 Ag12 61.09(3) 2 12_556
Ag14 Ag13 Ag12 121.66(4) 2 .
Ag14 Ag13 Ag13 60.22(4) 2 2
Ag14 Ag13 Ag13 118.81(3) . 2
Ag14 Ag13 Ag13 120.21(4) 2 3
Ag14 Ag13 Ag13 58.81(3) . 3
Ag14 Ag13 Ag14 178.39(4) 2 .
Ag14 Ag13 Ag16 121.73(3) . .
Ag14 Ag13 Ag16 59.28(3) 2 .
Ag14 Ag13 Ag22 90.65(3) 2 .
Ag14 Ag13 Ag23 85.73(3) . .
Ag14 Ag13 Ag23 93.75(4) 2 .
Ag16 Ag13 Ag23 65.47(3) . .
Ag20 Ag13 Ag11 88.71(3) . .
Ag20 Ag13 Ag11 118.36(3) . 2
Ag20 Ag13 Ag12 62.23(3) . .
Ag20 Ag13 Ag12 90.53(3) . 12_556
Ag20 Ag13 Ag13 120.96(5) . 3
Ag20 Ag13 Ag13 177.58(3) . 2
Ag20 Ag13 Ag14 62.17(3) . .
Ag20 Ag13 Ag14 118.74(4) . 2
Ag20 Ag13 Ag16 59.66(3) . .
Ag20 Ag13 Ag22 122.72(3) . .
Ag20 Ag13 Ag23 56.41(3) . .
Ag22 Ag13 Ag11 118.92(3) . 2
Ag22 Ag13 Ag12 60.503(19) . .
Ag22 Ag13 Ag13 59.689(10) . 3
Ag22 Ag13 Ag13 59.690(10) . 2
Ag22 Ag13 Ag14 89.82(3) . .
Ag22 Ag13 Ag16 118.65(3) . .
Ag22 Ag13 Ag23 175.21(4) . .
Ag11 Ag14 Ag12 121.31(3) . 11_556
Ag11 Ag14 Ag12 120.08(4) . .
Ag11 Ag14 Ag13 60.11(3) . .
Ag11 Ag14 Ag16 95.31(3) . 3
Ag11 Ag14 Ag18 179.60(5) . .
Ag11 Ag14 Ag20 86.89(3) . .
Ag12 Ag14 Ag12 60.23(2) . 11_556
Ag12 Ag14 Ag13 59.98(3) . .
Ag12 Ag14 Ag16 59.14(3) 11_556 3
Ag12 Ag14 Ag16 119.15(3) . 3
Ag12 Ag14 Ag18 60.31(3) . .
Ag12 Ag14 Ag20 60.87(3) . .
Ag12 Ag14 Ag20 121.07(4) 11_556 .
Ag13 Ag14 Ag11 61.36(2) 3 .
Ag13 Ag14 Ag12 90.49(3) . 11_556
Ag13 Ag14 Ag12 90.50(3) 3 .
Ag13 Ag14 Ag12 59.96(2) 3 11_556
Ag13 Ag14 Ag13 60.97(3) 3 .
Ag13 Ag14 Ag16 63.62(3) 3 3
Ag13 Ag14 Ag16 124.53(3) . 3
Ag13 Ag14 Ag18 120.28(4) . .
Ag13 Ag14 Ag18 118.86(3) 3 .
Ag13 Ag14 Ag20 58.13(3) . .
Ag13 Ag14 Ag20 119.07(4) 3 .
Ag16 Ag14 Ag20 177.20(4) 3 .
Ag18 Ag14 Ag12 58.91(2) . 11_556
Ag18 Ag14 Ag16 84.53(3) . 3
Ag18 Ag14 Ag20 93.26(3) . .
S6 Ag14 Ag11 56.39(7) 3 .
S6 Ag14 Ag12 168.18(9) 3 .
S6 Ag14 Ag12 110.71(8) 3 11_556
S6 Ag14 Ag13 77.96(9) 3 3
S6 Ag14 Ag13 115.05(8) 3 .
S6 Ag14 Ag16 53.26(7) 3 3
S6 Ag14 Ag18 123.26(7) 3 .
S6 Ag14 Ag20 127.24(8) 3 .
S11 Ag14 Ag11 124.03(8) . .
S11 Ag14 Ag12 79.68(8) . .
S11 Ag14 Ag12 113.92(8) . 11_556
S11 Ag14 Ag13 113.24(9) . .
S11 Ag14 Ag13 170.18(9) . 3
S11 Ag14 Ag16 121.17(9) . 3
S11 Ag14 Ag18 55.82(8) . .
S11 Ag14 Ag20 56.05(8) . .
S11 Ag14 S6 111.83(12) . 3
Ag4 Ag15 Ag4 60.000(1) 3_565 14_456
Ag4 Ag15 Ag4 119.998(1) 3_565 2_665
Ag4 Ag15 Ag4 119.999(1) 14_456 15_556
Ag4 Ag15 Ag4 60.002(1) 15_556 2_665
Ag4 Ag15 Ag4 119.999(1) 13_566 15_556
Ag4 Ag15 Ag4 60.000(1) 3_565 13_566
Ag4 Ag15 Ag4 180.0 13_566 .
Ag4 Ag15 Ag4 60.0 . 15_556
Ag4 Ag15 Ag4 180.0 14_456 2_665
Ag4 Ag15 Ag4 60.0 14_456 .
Ag4 Ag15 Ag4 180.0 3_565 15_556
Ag4 Ag15 Ag4 60.0 13_566 2_665
Ag4 Ag15 Ag4 120.0 . 2_665
Ag4 Ag15 Ag4 120.0 3_565 .
Ag4 Ag15 Ag4 120.0 13_566 14_456
Ag5 Ag15 Ag4 120.20(2) 13_566 3_565
Ag5 Ag15 Ag4 120.21(2) 2_665 13_566
Ag5 Ag15 Ag4 90.770(18) 13_566 .
Ag5 Ag15 Ag4 120.301(17) 3_565 .
Ag5 Ag15 Ag4 59.79(2) 14_456 13_566
Ag5 Ag15 Ag4 120.299(17) 14_456 15_556
Ag5 Ag15 Ag4 90.763(18) 15_556 3_565
Ag5 Ag15 Ag4 90.770(18) 3_565 15_556
Ag5 Ag15 Ag4 120.295(17) 15_556 13_566
Ag5 Ag15 Ag4 90.767(18) 14_456 2_665
Ag5 Ag15 Ag4 89.232(18) 15_556 15_556
Ag5 Ag15 Ag4 59.79(2) 3_565 2_665
Ag5 Ag15 Ag4 90.769(18) . 13_566
Ag5 Ag15 Ag4 120.21(2) 3_565 14_456
Ag5 Ag15 Ag4 89.230(18) 13_566 13_566
Ag5 Ag15 Ag4 89.231(18) . .
Ag5 Ag15 Ag4 120.21(2) 14_456 .
Ag5 Ag15 Ag4 59.698(17) 13_566 2_665
Ag5 Ag15 Ag4 89.234(18) 2_665 2_665
Ag5 Ag15 Ag4 89.228(18) 14_456 14_456
Ag5 Ag15 Ag4 59.79(2) 15_556 14_456
Ag5 Ag15 Ag4 59.703(17) 15_556 .
Ag5 Ag15 Ag4 59.794(19) 13_566 15_556
Ag5 Ag15 Ag4 120.21(2) . 15_556
Ag5 Ag15 Ag4 59.699(17) . 14_456
Ag5 Ag15 Ag4 59.794(19) . 3_565
Ag5 Ag15 Ag4 59.700(17) 2_665 15_556
Ag5 Ag15 Ag4 89.234(18) 3_565 3_565
Ag5 Ag15 Ag4 59.701(17) 3_565 13_566
Ag5 Ag15 Ag4 120.297(17) 13_566 14_456
Ag5 Ag15 Ag4 59.696(17) 14_456 3_565
Ag5 Ag15 Ag4 59.79(2) 2_665 .
Ag5 Ag15 Ag4 120.20(2) 15_556 2_665
Ag5 Ag15 Ag4 120.305(17) 2_665 3_565
Ag5 Ag15 Ag4 120.305(17) . 2_665
Ag5 Ag15 Ag4 90.771(18) 2_665 14_456
Ag5 Ag15 Ag5 119.48(2) 15_556 .
Ag5 Ag15 Ag5 60.51(2) 14_456 13_566
Ag5 Ag15 Ag5 60.52(2) 15_556 13_566
Ag5 Ag15 Ag5 119.48(2) 14_456 3_565
Ag5 Ag15 Ag5 119.48(2) 15_556 2_665
Ag5 Ag15 Ag5 60.51(2) 14_456 15_556
Ag5 Ag15 Ag5 180.0 15_556 3_565
Ag5 Ag15 Ag5 60.52(2) . 3_565
Ag5 Ag15 Ag5 180.0 13_566 .
Ag5 Ag15 Ag5 180.00(3) 14_456 2_665
Ag5 Ag15 Ag5 119.48(2) 14_456 .
Ag5 Ag15 Ag5 60.52(2) . 2_665
Ag5 Ag15 Ag5 119.48(2) 13_566 3_565
Ag5 Ag15 Ag5 119.48(2) 13_566 2_665
Ag5 Ag15 Ag5 60.52(2) 3_565 2_665
Ag12 Ag16 Ag13 58.15(2) 12_556 .
Ag12 Ag16 Ag14 60.32(3) 12_556 2
Ag12 Ag16 Ag18 60.43(3) 12_556 12_556
Ag12 Ag16 Ag20 88.83(3) 12_556 .
Ag12 Ag16 Ag24 66.75(3) 12_556 12_556
Ag14 Ag16 Ag13 57.10(2) 2 .
Ag14 Ag16 Ag20 113.75(3) 2 .
Ag18 Ag16 Ag13 86.60(3) 12_556 .
Ag18 Ag16 Ag14 120.41(4) 12_556 2
Ag18 Ag16 Ag20 59.38(3) 12_556 .
Ag20 Ag16 Ag13 56.83(3) . .
Ag24 Ag16 Ag13 124.89(4) 12_556 .
Ag24 Ag16 Ag14 95.53(4) 12_556 2
Ag24 Ag16 Ag18 66.50(3) 12_556 12_556
Ag24 Ag16 Ag20 125.77(4) 12_556 .
S6 Ag16 Ag12 118.43(7) . 12_556
S6 Ag16 Ag13 77.71(8) . .
S6 Ag16 Ag14 60.07(7) . 2
S6 Ag16 Ag18 160.22(10) . 12_556
S6 Ag16 Ag20 101.47(10) . .
S6 Ag16 Ag24 132.74(11) . 12_556
S6 Ag16 S8 117.27(11) . 12_556
S8 Ag16 Ag12 116.69(9) 12_556 12_556
S8 Ag16 Ag13 161.52(9) 12_556 .
S8 Ag16 Ag14 138.61(9) 12_556 2
S8 Ag16 Ag18 76.29(8) 12_556 12_556
S8 Ag16 Ag20 107.27(9) 12_556 .
S8 Ag16 Ag24 54.06(9) 12_556 12_556
S7 Ag17 S4 97.99(8) 15_556 .
S7 Ag17 S10 94.33(10) 15_556 .
S10 Ag17 S4 95.27(12) . .
P14 Ag17 S4 115.80(16) . .
P14 Ag17 S7 121.87(14) . 15_556
P14 Ag17 S10 125.30(13) . .
Ag12 Ag18 Ag12 60.46(3) 11_556 .
Ag12 Ag18 Ag14 60.55(2) 11_556 .
Ag12 Ag18 Ag16 93.03(3) 11_556 11_556
Ag12 Ag18 Ag20 61.92(3) 11_556 11_556
Ag12 Ag18 Ag24 66.55(3) 11_556 11_556
Ag12 Ag18 Ag24 127.01(3) . 11_556
Ag12 Ag18 Ag24 62.63(3) . .
Ag12 Ag18 Ag24 123.10(4) 11_556 .
Ag14 Ag18 Ag12 59.37(3) . .
Ag14 Ag18 Ag24 95.09(3) . 11_556
Ag14 Ag18 Ag24 90.94(3) . .
Ag16 Ag18 Ag12 59.26(3) 11_556 .
Ag16 Ag18 Ag14 118.42(4) 11_556 .
Ag16 Ag18 Ag24 125.80(4) 11_556 11_556
Ag16 Ag18 Ag24 56.56(3) 11_556 .
Ag20 Ag18 Ag12 88.93(3) 11_556 .
Ag20 Ag18 Ag14 122.31(3) 11_556 .
Ag20 Ag18 Ag16 60.73(3) 11_556 11_556
Ag20 Ag18 Ag24 117.20(4) 11_556 .
Ag20 Ag18 Ag24 65.48(3) 11_556 11_556
Ag24 Ag18 Ag24 170.34(4) 11_556 .
S9 Ag18 Ag12 118.36(10) 11_556 11_556
S9 Ag18 Ag12 164.88(9) 11_556 .
S9 Ag18 Ag14 134.76(10) 11_556 .
S9 Ag18 Ag16 106.80(9) 11_556 11_556
S9 Ag18 Ag20 78.25(9) 11_556 11_556
S9 Ag18 Ag24 54.35(10) 11_556 11_556
S9 Ag18 Ag24 116.30(10) 11_556 .
S9 Ag18 S11 112.08(12) 11_556 .
S11 Ag18 Ag12 79.58(9) . .
S11 Ag18 Ag12 116.35(7) . 11_556
S11 Ag18 Ag14 56.65(7) . .
S11 Ag18 Ag16 107.26(8) . 11_556
S11 Ag18 Ag20 166.82(9) . 11_556
S11 Ag18 Ag24 51.51(8) . .
S11 Ag18 Ag24 126.91(9) . 11_556
S8 Ag19 S9 92.95(12) 12_556 .
S8 Ag19 S12 98.91(12) 12_556 .
S9 Ag19 S12 95.27(12) . .
P15 Ag19 S8 123.58(18) . 12_556
P15 Ag19 S9 124.73(18) . .
P15 Ag19 S12 115.05(17) . .
Ag12 Ag20 Ag14 58.26(3) . .
Ag12 Ag20 Ag24 62.57(3) . .
Ag13 Ag20 Ag12 59.59(2) . .
Ag13 Ag20 Ag14 59.70(3) . .
Ag13 Ag20 Ag16 63.51(3) . .
Ag13 Ag20 Ag18 90.69(3) . 12_556
Ag13 Ag20 Ag23 69.06(3) . .
Ag13 Ag20 Ag24 122.15(4) . .
Ag14 Ag20 Ag24 90.72(4) . .
Ag16 Ag20 Ag12 90.54(3) . .
Ag16 Ag20 Ag14 123.11(3) . .
Ag16 Ag20 Ag24 117.25(4) . .
Ag18 Ag20 Ag12 58.56(3) 12_556 .
Ag18 Ag20 Ag14 116.75(3) 12_556 .
Ag18 Ag20 Ag16 59.88(3) 12_556 .
Ag18 Ag20 Ag23 131.30(5) 12_556 .
Ag18 Ag20 Ag24 57.71(3) 12_556 .
Ag23 Ag20 Ag12 128.23(3) . .
Ag23 Ag20 Ag14 91.20(3) . .
Ag23 Ag20 Ag16 71.50(4) . .
Ag23 Ag20 Ag24 167.57(4) . .
S11 Ag20 Ag12 78.06(8) . .
S11 Ag20 Ag13 114.40(6) . .
S11 Ag20 Ag14 55.65(6) . .
S11 Ag20 Ag16 166.98(9) . .
S11 Ag20 Ag18 108.10(8) . 12_556
S11 Ag20 Ag23 120.58(9) . .
S11 Ag20 Ag24 51.78(8) . .
S12 Ag20 Ag12 166.66(10) . .
S12 Ag20 Ag13 119.51(9) . .
S12 Ag20 Ag14 134.22(9) . .
S12 Ag20 Ag16 78.12(10) . .
S12 Ag20 Ag18 108.97(9) . 12_556
S12 Ag20 Ag23 54.81(8) . .
S12 Ag20 Ag24 116.45(8) . .
S12 Ag20 S11 112.31(12) . .
Ag4 Ag21 Ag7 54.32(3) . 15_556
Ag6 Ag21 Ag4 55.94(2) . .
Ag6 Ag21 Ag7 84.68(3) . 15_556
Ag7 Ag21 Ag4 55.61(2) 2_665 .
Ag7 Ag21 Ag6 56.92(3) 2_665 .
Ag7 Ag21 Ag7 109.93(4) 2_665 15_556
Ag9 Ag21 Ag4 56.31(2) 15_556 .
Ag9 Ag21 Ag6 112.25(3) 15_556 .
Ag9 Ag21 Ag7 56.50(3) 15_556 15_556
Ag9 Ag21 Ag7 84.87(3) 15_556 2_665
S5 Ag21 Ag4 75.11(6) . .
S5 Ag21 Ag6 53.54(7) . .
S5 Ag21 Ag7 108.99(7) . 2_665
S5 Ag21 Ag7 52.77(8) . 15_556
S5 Ag21 Ag9 108.45(9) . 15_556
S7 Ag21 Ag4 109.57(8) . .
S7 Ag21 Ag6 157.34(9) . .
S7 Ag21 Ag7 132.92(8) . 2_665
S7 Ag21 Ag7 72.76(8) . 15_556
S7 Ag21 Ag9 56.63(7) . 15_556
S7 Ag21 S5 108.40(11) . .
S10 Ag21 Ag4 109.06(7) . .
S10 Ag21 Ag6 73.95(8) . .
S10 Ag21 Ag7 158.43(8) . 15_556
S10 Ag21 Ag7 55.66(6) . 2_665
S10 Ag21 Ag9 129.51(9) . 15_556
S10 Ag21 S5 113.20(12) . .
S10 Ag21 S7 128.69(12) . .
Ag12 Ag22 Ag12 120.0 2 .
Ag12 Ag22 Ag12 120.0 10_556 12_556
Ag12 Ag22 Ag12 60.0 10_556 2
Ag12 Ag22 Ag12 60.0 12_556 2
Ag12 Ag22 Ag12 180.0 12_556 3
Ag12 Ag22 Ag12 180.0 10_556 .
Ag12 Ag22 Ag12 60.0 11_556 .
Ag12 Ag22 Ag12 120.0 3 .
Ag12 Ag22 Ag12 60.0 10_556 3
Ag12 Ag22 Ag12 119.998(1) 3 2
Ag12 Ag22 Ag12 60.0 3 11_556
Ag12 Ag22 Ag12 180.0 2 11_556
Ag12 Ag22 Ag12 119.998(1) 10_556 11_556
Ag12 Ag22 Ag12 60.0 12_556 .
Ag12 Ag22 Ag12 119.998(1) 12_556 11_556
Ag13 Ag22 Ag12 120.23(2) 10_556 .
Ag13 Ag22 Ag12 120.40(2) . 3
Ag13 Ag22 Ag12 90.69(2) 2 12_556
Ag13 Ag22 Ag12 120.23(2) 3 12_556
Ag13 Ag22 Ag12 90.69(2) 11_556 3
Ag13 Ag22 Ag12 120.23(2) 12_556 3
Ag13 Ag22 Ag12 89.31(2) . 2
Ag13 Ag22 Ag12 120.23(2) 11_556 2
Ag13 Ag22 Ag12 89.31(2) 2 3
Ag13 Ag22 Ag12 59.77(2) 11_556 11_556
Ag13 Ag22 Ag12 59.77(2) 3 3
Ag13 Ag22 Ag12 59.77(2) . .
Ag13 Ag22 Ag12 89.31(2) 10_556 11_556
Ag13 Ag22 Ag12 59.61(2) 2 10_556
Ag13 Ag22 Ag12 59.61(2) 12_556 2
Ag13 Ag22 Ag12 59.77(2) 12_556 12_556
Ag13 Ag22 Ag12 59.61(2) 3 11_556
Ag13 Ag22 Ag12 120.39(2) 12_556 11_556
Ag13 Ag22 Ag12 59.61(2) 11_556 .
Ag13 Ag22 Ag12 120.39(2) 2 .
Ag13 Ag22 Ag12 90.69(2) 12_556 .
Ag13 Ag22 Ag12 89.31(2) 11_556 12_556
Ag13 Ag22 Ag12 120.23(2) . 10_556
Ag13 Ag22 Ag12 59.61(2) 10_556 3
Ag13 Ag22 Ag12 59.77(2) 2 2
Ag13 Ag22 Ag12 90.69(2) 3 10_556
Ag13 Ag22 Ag12 120.39(2) 3 2
Ag13 Ag22 Ag12 59.77(2) 10_556 10_556
Ag13 Ag22 Ag12 90.69(2) . 11_556
Ag13 Ag22 Ag12 89.31(2) 3 .
Ag13 Ag22 Ag12 120.23(2) 2 11_556
Ag13 Ag22 Ag12 120.39(2) 10_556 12_556
Ag13 Ag22 Ag12 120.39(2) 11_556 10_556
Ag13 Ag22 Ag12 59.60(2) . 12_556
Ag13 Ag22 Ag12 90.69(2) 10_556 2
Ag13 Ag22 Ag12 89.31(2) 12_556 10_556
Ag13 Ag22 Ag13 119.37(2) 11_556 3
Ag13 Ag22 Ag13 180.000(17) 11_556 2
Ag13 Ag22 Ag13 119.37(2) 3 10_556
Ag13 Ag22 Ag13 180.000(17) 12_556 3
Ag13 Ag22 Ag13 119.37(2) 2 12_556
Ag13 Ag22 Ag13 60.63(2) 2 3
Ag13 Ag22 Ag13 60.63(2) . 3
Ag13 Ag22 Ag13 60.63(2) 12_556 10_556
Ag13 Ag22 Ag13 60.63(2) 11_556 12_556
Ag13 Ag22 Ag13 119.37(2) . 11_556
Ag13 Ag22 Ag13 60.63(2) . 2
Ag13 Ag22 Ag13 60.63(2) 11_556 10_556
Ag13 Ag22 Ag13 119.37(2) 2 10_556
Ag13 Ag22 Ag13 180.0 . 10_556
Ag13 Ag22 Ag13 119.37(2) . 12_556
Ag11 Ag23 Ag11 56.20(4) . 2
Ag11 Ag23 Ag13 53.54(2) 2 .
Ag11 Ag23 Ag13 55.33(3) . .
Ag11 Ag23 Ag20 87.07(4) . .
Ag20 Ag23 Ag11 107.90(4) . 2
Ag20 Ag23 Ag13 54.53(3) . .
S3 Ag23 Ag11 55.42(7) . .
S3 Ag23 Ag11 74.17(8) . 2
S3 Ag23 Ag13 108.17(7) . .
S3 Ag23 Ag20 134.47(10) . .
S3 Ag23 S6 113.17(12) . .
S3 Ag23 S12 135.90(12) . .
S6 Ag23 Ag11 108.30(7) . .
S6 Ag23 Ag11 53.42(6) . 2
S6 Ag23 Ag13 73.47(7) . .
S6 Ag23 Ag20 101.82(8) . .
S12 Ag23 Ag11 135.98(11) . .
S12 Ag23 Ag11 149.86(10) . 2
S12 Ag23 Ag13 106.63(9) . .
S12 Ag23 Ag20 55.54(9) . .
S12 Ag23 S6 102.06(12) . .
Ag12 Ag24 Ag18 54.51(3) . .
Ag16 Ag24 Ag12 56.35(2) 11_556 .
Ag16 Ag24 Ag18 56.95(3) 11_556 .
Ag16 Ag24 Ag18 84.75(4) 11_556 12_556
Ag16 Ag24 Ag20 112.22(3) 11_556 .
Ag18 Ag24 Ag12 55.84(3) 12_556 .
Ag18 Ag24 Ag18 110.34(4) 12_556 .
Ag18 Ag24 Ag20 56.80(3) 12_556 .
Ag20 Ag24 Ag12 55.88(2) . .
Ag20 Ag24 Ag18 84.88(3) . .
S8 Ag24 Ag12 109.95(7) . .
S8 Ag24 Ag16 57.25(7) . 11_556
S8 Ag24 Ag18 133.51(10) . 12_556
S8 Ag24 Ag18 72.67(7) . .
S8 Ag24 Ag20 157.41(8) . .
S8 Ag24 S9 128.52(11) . .
S8 Ag24 S11 107.79(13) . .
S9 Ag24 Ag12 109.08(9) . .
S9 Ag24 Ag16 128.94(10) . 11_556
S9 Ag24 Ag18 158.71(9) . .
S9 Ag24 Ag18 55.40(9) . 12_556
S9 Ag24 Ag20 74.01(9) . .
S9 Ag24 S11 113.62(12) . .
S11 Ag24 Ag12 75.25(7) . .
S11 Ag24 Ag16 108.72(8) . 11_556
S11 Ag24 Ag18 109.36(9) . 12_556
S11 Ag24 Ag18 52.60(7) . .
S11 Ag24 Ag20 53.99(9) . .
Ag1 S1 Ag3 102.74(10) 2_665 .
Ag8 S1 Ag1 69.80(8) . 2_665
Ag8 S1 Ag3 139.41(10) . .
C10 S1 Ag1 106.2(4) . 2_665
C10 S1 Ag3 108.9(4) . .
C10 S1 Ag8 111.4(4) . .
Ag1 S2 Ag2 64.12(7) 3_565 2_665
Ag8 S2 Ag1 76.07(9) . 3_565
Ag8 S2 Ag2 114.39(11) . 2_665
Ag8 S2 Ag9 83.00(7) . 2_665
Ag9 S2 Ag1 109.80(11) 2_665 3_565
Ag9 S2 Ag2 66.13(7) 2_665 2_665
C3 S2 Ag1 128.5(3) . 3_565
C3 S2 Ag2 137.1(2) . 2_665
C3 S2 Ag8 108.5(2) . .
C3 S2 Ag9 121.7(3) . 2_665
Ag11 S3 Ag10 102.67(9) . .
Ag23 S3 Ag10 139.52(16) . .
Ag23 S3 Ag11 69.76(9) . .
C29 S3 Ag10 108.8(4) . .
C29 S3 Ag11 104.5(5) . .
C29 S3 Ag23 111.6(4) . .
Ag6 S4 Ag17 98.13(10) . .
Ag8 S4 Ag6 70.00(9) . .
Ag8 S4 Ag17 144.98(11) . .
C47 S4 Ag6 112.6(4) . .
C47 S4 Ag8 116.1(4) . .
C47 S4 Ag17 98.9(4) . .
Ag6 S5 Ag2 68.29(6) . .
Ag7 S5 Ag2 67.35(8) 15_556 .
Ag7 S5 Ag6 109.20(10) 15_556 .
Ag21 S5 Ag2 113.90(10) . .
Ag21 S5 Ag6 75.06(10) . .
Ag21 S5 Ag7 76.12(10) . 15_556
C11 S5 Ag2 137.1(5) . .
C11 S5 Ag6 128.1(5) . .
C11 S5 Ag7 122.2(5) . 15_556
C11 S5 Ag21 108.9(5) . .
Ag11 S6 Ag14 63.73(6) 2 2
Ag16 S6 Ag11 110.32(12) . 2
Ag16 S6 Ag14 66.66(8) . 2
Ag16 S6 Ag23 83.91(13) . .
Ag23 S6 Ag11 75.78(10) . 2
Ag23 S6 Ag14 114.49(13) . 2
C15 S6 Ag11 129.5(4) . 2
C15 S6 Ag14 138.7(6) . 2
C15 S6 Ag16 120.2(4) . .
C15 S6 Ag23 106.8(6) . .
Ag17 S7 Ag9 97.09(12) 14_456 15_556
Ag21 S7 Ag9 68.96(7) . 15_556
Ag21 S7 Ag17 141.89(15) . 14_456
C55 S7 Ag9 119.8(4) . 15_556
C55 S7 Ag17 105.2(4) . 14_456
C55 S7 Ag21 112.5(4) . .
Ag19 S8 Ag16 96.81(10) 11_556 11_556
Ag24 S8 Ag16 68.69(9) . 11_556
Ag24 S8 Ag19 142.69(13) . 11_556
C27 S8 Ag16 122.0(4) . 11_556
C27 S8 Ag19 107.4(4) . 11_556
C27 S8 Ag24 109.4(4) . .
Ag18 S9 Ag19 99.51(13) 12_556 .
Ag24 S9 Ag18 70.25(8) . 12_556
Ag24 S9 Ag19 138.72(15) . .
C34 S9 Ag18 110.2(4) . 12_556
C34 S9 Ag19 112.5(4) . .
C34 S9 Ag24 108.5(4) . .
Ag7 S10 Ag17 98.89(10) 2_665 .
Ag21 S10 Ag7 70.44(10) . 2_665
Ag21 S10 Ag17 139.70(15) . .
C31 S10 Ag7 106.1(4) . 2_665
C31 S10 Ag17 109.6(4) . .
C31 S10 Ag21 110.7(4) . .
Ag14 S11 Ag20 68.31(8) . .
Ag18 S11 Ag14 67.53(7) . .
Ag18 S11 Ag20 108.82(12) . .
Ag24 S11 Ag14 113.47(13) . .
Ag24 S11 Ag18 75.89(10) . .
Ag24 S11 Ag20 74.23(10) . .
C56 S11 Ag14 135.4(5) . .
C56 S11 Ag18 119.8(6) . .
C56 S11 Ag20 131.0(6) . .
C56 S11 Ag24 110.8(5) . .
Ag20 S12 Ag19 97.81(12) . .
Ag23 S12 Ag19 143.98(18) . .
Ag23 S12 Ag20 69.66(8) . .
C57 S12 Ag19 99.4(5) . .
C57 S12 Ag20 110.8(6) . .
C57 S12 Ag23 116.6(5) . .
C82 P13 Ag3 113.3(6) 3_565 .
C82 P13 Ag3 113.3(6) 2_665 .
C82 P13 Ag3 113.3(6) . .
C82 P13 C82 105.4(6) . 2_665
C82 P13 C82 105.4(6) . 3_565
C82 P13 C82 105.4(6) 3_565 2_665
C81 P14 Ag17 116.3(8) . .
C81 P14 C100 100.3(11) . .
C100 P14 Ag17 115.5(8) . .
C116 P14 Ag17 115.6(6) . .
C116 P14 C81 107.4(11) . .
C116 P14 C100 99.4(9) . .
C106 P15 Ag19 113.2(8) . .
C108 P15 Ag19 117.3(8) . .
C108 P15 C106 99.1(13) . .
C108 P15 C174 108.5(10) . .
C174 P15 Ag19 117.2(5) . .
C174 P15 C106 98.6(12) . .
C0AA P16 Ag10 110.4(5) . .
C0AA P16 Ag10 110.4(5) 3 .
C0AA P16 Ag10 110.4(5) 2 .
C0AA P16 C0AA 108.5(5) . 3
C0AA P16 C0AA 108.5(5) 3 2
C0AA P16 C0AA 108.5(5) . 2
C18 C3 S2 121.8(4) . .
C18 C3 C90 120.0 . .
C90 C3 S2 118.2(4) . .
C58 C18 C3 120.0 . .
C18 C58 C79 120.0 . .
F18 C58 C18 119.1(12) . .
F18 C58 C79 119.7(12) . .
C78 C79 C58 120.0 . .
F25 C79 C58 114.5(11) . .
F25 C79 C78 125.4(11) . .
C90 C78 C79 120.0 . .
C78 C90 C3 120.0 . .
C27 C6 C122 120.0 . .
C6 C27 S8 119.0(5) . .
C6 C27 C66 120.0 . .
C66 C27 S8 120.6(5) . .
C80 C66 C27 120.0 . .
C66 C80 C104 120.0 . .
F49 C80 C66 121.4(11) . .
F49 C80 C104 118.6(11) . .
C122 C104 C80 120.0 . .
F19 C104 C80 117.9(11) . .
F19 C104 C122 122.0(11) . .
C104 C122 C6 120.0 . .
C56 C9 C32 120.8(15) . .
C40 C10 S1 120.6(11) . .
C75 C10 S1 120.2(9) . .
C75 C10 C40 119.2(12) . .
C17 C11 S5 117.0(9) . .
C36 C11 S5 117.0(11) . .
C36 C11 C17 126.0(12) . .
C33 C15 S6 122.4(11) . .
C74 C15 S6 120.8(15) . .
C74 C15 C33 116.7(15) . .
C23 C16 C136 120.0 . .
C31 C23 C16 120.0 . .
C23 C31 S10 122.3(6) . .
C23 C31 C65 120.0 . .
C65 C31 S10 117.6(6) . .
C31 C65 C115 120.0 . .
C136 C115 C65 120.0 . .
F96 C115 C65 118.7(11) . .
F96 C115 C136 120.7(11) . .
C115 C136 C16 120.0 . .
F24 C136 C16 124.3(9) . .
F24 C136 C115 115.7(9) . .
C26 C17 C11 116.6(13) . .
C17 C26 C69 120.0(17) . .
C39 C28 C46 120.6(14) . .
C46 C29 S3 119.8(12) . .
C67 C29 S3 121.7(10) . .
C67 C29 C46 118.4(14) . .
C83 C32 C9 115.4(18) . .
C85 C33 C15 122.6(18) . .
C11 C36 C42 114.2(16) . .
C28 C39 F4 119.4(14) . .
C28 C39 C88 120.8(19) . .
C88 C39 F4 119.6(16) . .
C10 C40 C51 129.5(18) . .
C157 C41 C108 120.4(16) . .
F44 C42 C36 118.5(19) . .
F44 C42 C69 121.5(17) . .
C69 C42 C36 120.0(16) . .
C34 C43 C84 120.0 . .
C43 C34 S9 121.0(5) . .
C43 C34 C63 120.0 . .
C63 C34 S9 118.9(5) . .
C98 C63 C34 120.0 . .
C63 C98 C95 120.0 . .
F92 C98 C63 118.8(14) . .
F92 C98 C95 121.2(14) . .
C84 C95 C98 120.0 . .
F59 C95 C98 109.4(12) . .
F59 C95 C84 129.3(11) . .
C95 C84 C43 120.0 . .
C28 C46 C29 116.7(16) . .
C102 C51 C40 99.1(18) . .
C55 C52 C77 120.0 . .
C52 C55 S7 120.2(4) . .
C68 C55 S7 119.7(4) . .
C68 C55 C52 120.0 . .
C55 C68 C134 120.0 . .
C160 C134 C68 120.0 . .
F143 C134 C68 164.3(16) . .
F143 C134 C160 75.0(17) . .
C134 C160 F143 52.1(16) . .
C134 C160 F145 155.7(13) . .
C77 C160 C134 120.0 . .
C77 C160 F143 171.1(14) . .
C77 C160 F145 83.7(13) . .
F145 C160 F143 104(2) . .
C52 C77 F145 168.8(10) . .
C160 C77 C52 120.0 . .
C160 C77 F145 49.8(11) . .
C56 C54 C99 117.6(17) . .
C9 C56 S11 119.0(11) . .
C9 C56 C54 125.0(15) . .
C54 C56 S11 116.1(13) . .
F12 C60 C85 115.9(18) . .
F12 C60 C87 126.5(18) . .
C87 C60 C85 116.7(16) . .
C29 C67 C88 120.1(14) . .
F13 C69 C42 115.5(17) . .
C26 C69 F13 121.5(19) . .
C26 C69 C42 123.0(16) . .
C91 C73 C81 102.6(13) . .
C15 C74 C87 123(2) . .
C10 C75 C97 113.3(16) . .
C73 C81 P14 105.5(10) . .
C125 C82 P13 112.2(10) . .
C32 C83 F8 117.9(18) . .
C32 C83 C99 124.1(17) . .
C99 C83 F8 118.0(15) . .
C33 C85 C60 119.4(18) . .
F72 C85 C33 127(2) . .
F72 C85 C60 113.1(18) . .
C60 C87 C74 121(2) . .
C39 C88 F61 117.6(18) . .
C39 C88 C67 122.3(18) . .
C67 C88 F61 119.8(16) . .
C73 C91 C163 104.1(17) . .
C75 C97 F62 110.8(18) . .
C102 C97 F62 124.4(18) . .
C102 C97 C75 124(2) . .
F35 C99 C54 122(2) . .
C83 C99 F35 118.5(18) . .
C83 C99 C54 117.1(16) . .
C1 C100 P14 112.2(16) . .
C51 C102 F14 123.2(16) . .
C97 C102 F14 102.6(19) . .
C97 C102 C51 134.1(19) . .
C154 C106 P15 108.2(19) . .
C41 C108 P15 119.3(13) . .
C148 C116 P14 116.7(16) . .
C193 C125 C82 109.0(14) . .
C141 C140 C174 144.2(9) . .
C134 F143 C160 52.8(7) . .
C160 F145 C77 46.5(10) . .
C192 C148 C116 109(2) . .
C112 C149 C114 120.0 . .
C149 C112 C57 120.0 . .
C112 C57 S12 121.3(8) . .
C45 C57 S12 118.4(8) . .
C45 C57 C112 120.0 . .
C57 C45 C110 120.0 . .
C45 C110 F94 115.6(16) . .
C114 C110 F94 123.4(16) . .
C114 C110 C45 120.0 . .
F76 C114 C149 121.9(11) . .
F76 C114 C110 118.1(11) . .
C110 C114 C149 120.0 . .
C106 C154 C113 99(2) . .
C41 C157 C93 114.6(19) . .
C140 C174 P15 111.1(8) . .
C5 C192 C148 113(3) . .
C125 C193 C183 98.3(15) . .
C100 C1 C4 114(3) . .
C1 C4 C2 112(3) . .
C294 C113 C154 101.0(16) . .
C0AA C121 C184 114.9(8) . .
C198 C141 C140 137.9(10) . .
F9 C179 C14 120.9(10) . .
F9 C179 C38 119.0(10) . .
C38 C179 C14 120.0 . .
C47 C14 C179 120.0 . .
C14 C47 S4 121.9(6) . .
C119 C47 S4 117.9(6) . .
C119 C47 C14 120.0 . .
C47 C119 C129 120.0 . .
C119 C129 C38 120.0 . .
F16 C38 C179 117.7(10) . .
F16 C38 C129 122.2(10) . .
C179 C38 C129 120.0 . .
C177 C13 C184 112.1(11) . .
C121 C0AA P16 104.8(7) . .
C121 C184 C13 111.3(8) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 Ag1 2.8807(14) 2_665
Ag1 Ag1 2.8808(14) 3_565
Ag1 Ag2 2.8517(10) 3_565
Ag1 Ag5 2.9076(10) 3_565
Ag1 Ag5 2.8671(9) .
Ag1 Ag8 2.8955(12) 3_565
Ag1 Ag8 3.1966(10) 2_665
Ag1 S1 2.545(3) 3_565
Ag1 S2 2.630(3) 2_665
Ag2 Ag1 2.8522(10) 2_665
Ag2 Ag4 2.9001(10) 14_456
Ag2 Ag4 2.8757(10) .
Ag2 Ag5 2.8883(8) 2_665
Ag2 Ag5 2.8350(8) .
Ag2 Ag6 2.9487(12) .
Ag2 Ag7 2.9047(10) 15_556
Ag2 Ag9 2.9045(13) .
Ag2 S2 2.741(3) 3_565
Ag2 S5 2.632(3) .
Ag3 S1 2.619(3) 2_665
Ag3 S1 2.619(3) .
Ag3 S1 2.619(3) 3_565
Ag3 P13 2.423(7) .
Ag4 Ag2 2.9005(10) 15_556
Ag4 Ag4 2.8957(6) 15_556
Ag4 Ag4 2.8959(6) 14_456
Ag4 Ag5 2.8760(9) 15_556
Ag4 Ag5 2.8797(9) 2_665
Ag4 Ag6 2.9638(10) .
Ag4 Ag7 2.8978(11) 15_556
Ag4 Ag7 2.8453(10) 2_665
Ag4 Ag9 2.8722(10) 15_556
Ag4 Ag15 2.8956(6) .
Ag4 Ag21 3.1697(10) .
Ag5 Ag1 2.9079(10) 2_665
Ag5 Ag2 2.8883(9) 3_565
Ag5 Ag4 2.8799(9) 3_565
Ag5 Ag4 2.8758(9) 14_456
Ag5 Ag5 2.9047(12) 3_565
Ag5 Ag5 2.9047(12) 2_665
Ag5 Ag6 2.8355(10) 3_565
Ag5 Ag8 3.2682(11) 3_565
Ag5 Ag9 3.0221(9) .
Ag5 Ag15 2.8820(7) .
Ag6 Ag5 2.8355(10) 2_665
Ag6 Ag7 2.8952(11) 2_665
Ag6 Ag8 2.9128(11) .
Ag6 Ag9 2.9241(10) 2_665
Ag6 Ag21 3.1493(11) .
Ag6 S4 2.554(3) .
Ag6 S5 2.621(3) .
Ag7 Ag2 2.9049(10) 14_456
Ag7 Ag4 2.8453(10) 3_565
Ag7 Ag4 2.8975(11) 14_456
Ag7 Ag6 2.8951(11) 3_565
Ag7 Ag9 2.8854(12) .
Ag7 Ag21 3.1779(14) 14_456
Ag7 Ag21 2.9100(11) 3_565
Ag7 S5 2.607(3) 14_456
Ag7 S10 2.550(3) 3_565
Ag8 Ag1 2.8954(12) 2_665
Ag8 Ag1 3.1965(10) 3_565
Ag8 Ag5 3.2679(11) 2_665
Ag8 S1 2.516(3) .
Ag8 S2 2.557(3) .
Ag8 S4 2.524(3) .
Ag9 Ag4 2.8720(10) 14_456
Ag9 Ag6 2.9241(11) 3_565
Ag9 Ag21 2.8956(12) 14_456
Ag9 S2 2.577(3) 3_565
Ag9 S7 2.591(2) 14_456
Ag10 S3 2.617(3) .
Ag10 S3 2.616(3) 3
Ag10 S3 2.616(3) 2
Ag10 P16 2.422(8) .
Ag11 Ag11 2.8754(15) 3
Ag11 Ag11 2.8754(15) 2
Ag11 Ag13 2.9009(11) 3
Ag11 Ag13 2.8684(11) .
Ag11 Ag14 2.8452(12) .
Ag11 Ag23 3.1896(12) 3
Ag11 Ag23 2.8892(12) .
Ag11 S3 2.535(3) .
Ag11 S6 2.642(3) 3
Ag12 Ag12 2.8979(6) 12_556
Ag12 Ag12 2.8980(6) 11_556
Ag12 Ag13 2.8698(10) 11_556
Ag12 Ag13 2.8767(10) .
Ag12 Ag14 2.8735(11) .
Ag12 Ag14 2.9018(11) 12_556
Ag12 Ag16 2.8670(11) 11_556
Ag12 Ag18 2.8538(9) 12_556
Ag12 Ag18 2.9011(13) .
Ag12 Ag20 2.9515(11) .
Ag12 Ag22 2.8979(6) .
Ag12 Ag24 3.1643(10) .
Ag13 Ag11 2.9012(10) 2
Ag13 Ag12 2.8694(10) 12_556
Ag13 Ag13 2.9030(9) 3
Ag13 Ag13 2.9029(10) 2
Ag13 Ag14 2.8817(13) .
Ag13 Ag14 2.8402(11) 2
Ag13 Ag16 3.0306(10) .
Ag13 Ag20 2.8343(9) .
Ag13 Ag22 2.8755(7) .
Ag13 Ag23 3.2503(12) .
Ag14 Ag12 2.9019(11) 11_556
Ag14 Ag13 2.8403(11) 3
Ag14 Ag16 2.9080(11) 3
Ag14 Ag18 2.9013(12) .
Ag14 Ag20 2.9516(11) .
Ag14 S6 2.744(3) 3
Ag14 S11 2.623(3) .
Ag15 Ag4 2.8957(6) 13_566
Ag15 Ag4 2.8956(6) 15_556
Ag15 Ag4 2.8957(6) 3_565
Ag15 Ag4 2.8957(6) 14_456
Ag15 Ag4 2.8957(6) 2_665
Ag15 Ag5 2.8823(7) 14_456
Ag15 Ag5 2.8820(7) 3_565
Ag15 Ag5 2.8822(7) 13_566
Ag15 Ag5 2.8820(7) 2_665
Ag15 Ag5 2.8822(7) 15_556
Ag16 Ag12 2.8669(11) 12_556
Ag16 Ag14 2.9081(11) 2
Ag16 Ag18 2.8976(13) 12_556
Ag16 Ag20 2.9224(15) .
Ag16 Ag24 2.8851(13) 12_556
Ag16 S6 2.538(3) .
Ag16 S8 2.604(3) 12_556
Ag17 S4 2.651(4) .
Ag17 S7 2.577(4) 15_556
Ag17 S10 2.609(4) .
Ag17 P14 2.402(5) .
Ag18 Ag12 2.8539(10) 11_556
Ag18 Ag16 2.8980(13) 11_556
Ag18 Ag20 2.8830(12) 11_556
Ag18 Ag24 2.9125(14) 11_556
Ag18 Ag24 3.1705(12) .
Ag18 S9 2.547(3) 11_556
Ag18 S11 2.597(3) .
Ag19 S8 2.603(4) 12_556
Ag19 S9 2.606(4) .
Ag19 S12 2.660(4) .
Ag19 P15 2.403(5) .
Ag20 Ag18 2.8828(12) 12_556
Ag20 Ag23 2.8991(14) .
Ag20 Ag24 3.1347(14) .
Ag20 S11 2.635(4) .
Ag20 S12 2.549(3) .
Ag21 Ag7 2.9101(11) 2_665
Ag21 Ag7 3.1780(13) 15_556
Ag21 Ag9 2.8955(12) 15_556
Ag21 S5 2.548(4) .
Ag21 S7 2.523(3) .
Ag21 S10 2.495(4) .
Ag22 Ag12 2.8979(6) 11_556
Ag22 Ag12 2.8979(6) 2
Ag22 Ag12 2.8979(6) 12_556
Ag22 Ag12 2.8979(6) 3
Ag22 Ag12 2.8979(6) 10_556
Ag22 Ag13 2.8757(7) 11_556
Ag22 Ag13 2.8757(7) 2
Ag22 Ag13 2.8757(7) 12_556
Ag22 Ag13 2.8757(7) 10_556
Ag22 Ag13 2.8757(7) 3
Ag23 Ag11 3.1896(12) 2
Ag23 S3 2.517(3) .
Ag23 S6 2.550(5) .
Ag23 S12 2.527(3) .
Ag24 Ag16 2.8850(13) 11_556
Ag24 Ag18 2.9125(14) 12_556
Ag24 S8 2.507(4) .
Ag24 S9 2.515(4) .
Ag24 S11 2.559(4) .
S1 Ag1 2.545(3) 2_665
S1 C10 1.743(11) .
S2 Ag1 2.630(3) 3_565
S2 Ag2 2.740(3) 2_665
S2 Ag9 2.577(3) 2_665
S2 C3 1.758(8) .
S3 C29 1.761(15) .
S4 C47 1.782(8) .
S5 Ag7 2.607(3) 15_556
S5 C11 1.817(12) .
S6 Ag11 2.642(3) 2
S6 Ag14 2.745(3) 2
S6 C15 1.772(14) .
S7 Ag9 2.591(2) 15_556
S7 Ag17 2.577(4) 14_456
S7 C55 1.805(7) .
S8 Ag16 2.604(3) 11_556
S8 Ag19 2.602(4) 11_556
S8 C27 1.751(9) .
S9 Ag18 2.547(3) 12_556
S9 C34 1.732(10) .
S10 Ag7 2.550(3) 2_665
S10 C31 1.787(9) .
S11 C56 1.834(15) .
S12 C57 1.763(12) .
P13 C82 1.868(14) 3_565
P13 C82 1.868(14) 2_665
P13 C82 1.868(14) .
P14 C81 1.83(2) .
P14 C100 1.914(19) .
P14 C116 1.77(2) .
P15 C106 1.91(3) .
P15 C108 1.74(2) .
P15 C174 1.806(15) .
P16 C0AA 1.965(10) 3
P16 C0AA 1.965(10) .
P16 C0AA 1.965(10) 2
C3 C18 1.3900 .
C3 C90 1.3900 .
C18 C58 1.3900 .
C58 C79 1.3900 .
C58 F18 1.323(16) .
C79 C78 1.3900 .
C79 F25 1.310(14) .
C78 C90 1.3900 .
F4 C39 1.38(2) .
C6 C27 1.3900 .
C6 C122 1.3900 .
C27 C66 1.3900 .
C66 C80 1.3900 .
C80 C104 1.3900 .
C80 F49 1.283(18) .
C104 C122 1.3900 .
C104 F19 1.318(15) .
F8 C83 1.38(2) .
C9 C32 1.40(2) .
C9 C56 1.30(2) .
C10 C40 1.48(2) .
C10 C75 1.37(2) .
C11 C17 1.41(2) .
C11 C36 1.401(19) .
F12 C60 1.30(2) .
F13 C69 1.38(2) .
F14 C102 1.45(2) .
C15 C33 1.41(3) .
C15 C74 1.38(2) .
C16 C23 1.3900 .
C16 C136 1.3900 .
C23 C31 1.3900 .
C31 C65 1.3900 .
C65 C115 1.3900 .
C115 C136 1.3900 .
C115 F96 1.31(2) .
C136 F24 1.316(15) .
C17 C26 1.37(2) .
C26 C69 1.37(3) .
C28 C39 1.33(2) .
C28 C46 1.37(3) .
C29 C46 1.49(2) .
C29 C67 1.32(2) .
C32 C83 1.35(2) .
C33 C85 1.29(3) .
F35 C99 1.40(3) .
C36 C42 1.42(2) .
C39 C88 1.33(2) .
C40 C51 1.54(3) .
C41 C108 1.54(3) .
C41 C157 1.45(3) .
C42 F44 1.33(2) .
C42 C69 1.40(3) .
C43 C34 1.3900 .
C43 C84 1.3900 .
C34 C63 1.3900 .
C63 C98 1.3900 .
C98 C95 1.3900 .
C98 F92 1.278(19) .
C95 C84 1.3900 .
C95 F59 1.354(19) .
C51 C102 1.40(4) .
C52 C55 1.3900 .
C52 C77 1.3900 .
C55 C68 1.3900 .
C68 C134 1.3900 .
C134 C160 1.3900 .
C134 F143 1.38(3) .
C160 C77 1.3900 .
C160 F143 1.68(2) .
C160 F145 1.46(4) .
C77 F145 1.91(4) .
C54 C56 1.33(2) .
C54 C99 1.40(2) .
C60 C85 1.55(3) .
C60 C87 1.30(3) .
F61 C88 1.37(2) .
F62 C97 1.41(3) .
C67 C88 1.36(3) .
F72 C85 1.23(3) .
C73 C81 1.65(2) .
C73 C91 1.56(3) .
C74 C87 1.40(3) .
C75 C97 1.41(2) .
F76 C114 1.36(2) .
C82 C125 1.59(2) .
C83 C99 1.38(3) .
C91 C163 1.65(3) .
C93 C157 1.57(4) .
F94 C110 1.47(4) .
C97 C102 1.36(3) .
C100 C1 1.44(3) .
C106 C154 1.54(3) .
C116 C148 1.53(3) .
C125 C193 1.493(12) .
C140 C174 1.509(13) .
C140 C141 1.506(11) .
C148 C192 1.52(5) .
C149 C112 1.3900 .
C149 C114 1.3900 .
C112 C57 1.3900 .
C57 C45 1.3900 .
C45 C110 1.3900 .
C110 C114 1.3900 .
C154 C113 1.71(3) .
C183 C193 1.78(4) .
C192 C5 1.45(5) .
C1 C4 1.49(4) .
C2 C4 1.66(5) .
C113 C294 1.499(14) .
C121 C0AA 1.497(14) .
C121 C184 1.499(9) .
C141 C198 1.502(14) .
F9 C179 1.275(18) .
F16 C38 1.279(15) .
C179 C14 1.3900 .
C179 C38 1.3900 .
C14 C47 1.3900 .
C47 C119 1.3900 .
C119 C129 1.3900 .
C129 C38 1.3900 .
C13 C177 1.500(13) .
C13 C184 1.502(13) .
