#------------------------------------------------------------------------------
#$Date: 2019-11-02 07:48:34 +0200 (Sat, 02 Nov 2019) $
#$Revision: 221006 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/12/78/4127834.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4127834
loop_
_publ_author_name
'Chiu, Tzu-Hao'
'Liao, Jian-Hong'
'Gam, Franck'
'Chantrenne, Isaac'
'Kahlal, Samia'
'Saillard, Jean-Yves'
'Liu, C. W.'
_publ_section_title
;
 Homoleptic Platinum/Silver Superatoms Protected by Dithiolates: Linear
 Assemblies of Two and Three Centered Icosahedra Isolobal to
 Ne₂ and I₃<sup/>.
;
_journal_issue                   33
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              12957
_journal_page_last               12961
_journal_paper_doi               10.1021/jacs.9b05000
_journal_volume                  141
_journal_year                    2019
_chemical_formula_sum            'C102 H238 Ag33 O34 P17 Pt2 S34'
_chemical_formula_weight         7575.33
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_cell_angle_alpha                90
_cell_angle_beta                 99.1282(14)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   32.668(2)
_cell_length_b                   17.4136(13)
_cell_length_c                   37.113(3)
_cell_measurement_reflns_used    9790
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      26.41
_cell_measurement_theta_min      2.22
_cell_volume                     20845(3)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0351
_diffrn_reflns_av_unetI/netI     0.0378
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       38
_diffrn_reflns_limit_h_min       -38
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       42
_diffrn_reflns_limit_l_min       -44
_diffrn_reflns_number            57021
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_min         1.544
_exptl_absorpt_coefficient_mu    4.877
_exptl_absorpt_correction_T_max  0.7454
_exptl_absorpt_correction_T_min  0.5457
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.414
_exptl_crystal_description       plate
_exptl_crystal_F_000             14512
_exptl_crystal_size_max          0.120
_exptl_crystal_size_mid          0.040
_exptl_crystal_size_min          0.030
_refine_diff_density_max         1.934
_refine_diff_density_min         -2.120
_refine_diff_density_rms         0.209
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.143
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1018
_refine_ls_number_reflns         18267
_refine_ls_number_restraints     282
_refine_ls_restrained_S_all      1.143
_refine_ls_R_factor_all          0.0578
_refine_ls_R_factor_gt           0.0460
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+974.7290P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0993
_refine_ls_wR_factor_ref         0.1055
_reflns_Friedel_coverage         0.000
_reflns_number_gt                15620
_reflns_number_total             18267
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ja9b05000_si_003.cif
_cod_data_source_block           2
_cod_database_code               4127834
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;
_shelx_estimated_absorpt_t_min   0.592
_shelx_estimated_absorpt_t_max   0.867
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Ag1 Ag 0.39939(2) 0.30069(4) 0.11711(2) 0.02107(16) Uani 1 1 d . . .
Ag2 Ag 0.41896(2) 0.16559(4) 0.16561(2) 0.02192(16) Uani 1 1 d . . .
Ag3 Ag 0.36614(2) 0.28179(4) 0.18764(2) 0.02185(16) Uani 1 1 d . . .
Ag4 Ag 0.46526(2) 0.40889(4) 0.13155(2) 0.02185(16) Uani 1 1 d . . .
Ag5 Ag 0.48216(2) 0.24502(4) 0.12787(2) 0.02158(16) Uani 1 1 d . . .
Ag6 Ag 0.50087(2) 0.18719(4) 0.20228(2) 0.01864(15) Uani 1 1 d . . .
Ag7 Ag 0.42687(2) 0.21561(4) 0.24214(2) 0.02299(17) Uani 1 1 d . . .
Ag8 Ag 0.41933(2) 0.37817(4) 0.24260(2) 0.02175(16) Uani 1 1 d . . .
Ag9 Ag 0.39611(2) 0.43220(4) 0.16951(2) 0.02115(16) Uani 1 1 d . . .
Ag10 Ag 0.53024(2) 0.33629(4) 0.18189(2) 0.01910(16) Uani 1 1 d . . .
Ag11 Ag 0.5000 0.31414(6) 0.2500 0.0162(2) Uani 1 2 d S T P
Ag12 Ag 0.48045(2) 0.45284(4) 0.20737(2) 0.02005(16) Uani 1 1 d . . .
Ag13 Ag 0.33852(2) 0.18353(5) 0.11981(2) 0.02650(18) Uani 1 1 d . . .
Ag14 Ag 0.48685(2) 0.07939(5) 0.13748(2) 0.02753(18) Uani 1 1 d . . .
Ag15 Ag 0.56801(2) 0.19722(4) 0.15477(2) 0.02535(17) Uani 1 1 d . . .
Ag16 Ag 0.31789(3) 0.35575(5) 0.12716(2) 0.02779(18) Uani 1 1 d . . .
Ag17 Ag 0.37865(3) 0.45714(5) 0.08830(2) 0.03019(19) Uani 1 1 d . . .
C1 C 0.2399(4) 0.5319(8) 0.1579(4) 0.045(3) Uani 1 1 d . U .
H1A H 0.2506 0.5234 0.1840 0.054 Uiso 1 1 calc R U .
H1B H 0.2393 0.4820 0.1450 0.054 Uiso 1 1 calc R U .
C2 C 0.1965(4) 0.5666(9) 0.1533(4) 0.056(4) Uani 1 1 d . U .
H2A H 0.1789 0.5346 0.1668 0.067 Uiso 1 1 calc R U .
H2B H 0.1982 0.6185 0.1644 0.067 Uiso 1 1 calc R U .
C3 C 0.1762(4) 0.5725(10) 0.1145(5) 0.067(4) Uani 1 1 d . U .
H3A H 0.1930 0.6051 0.1010 0.100 Uiso 1 1 calc R U .
H3B H 0.1486 0.5951 0.1133 0.100 Uiso 1 1 calc R U .
H3C H 0.1737 0.5212 0.1035 0.100 Uiso 1 1 calc R U .
C4 C 0.3103(4) 0.6703(7) 0.0869(4) 0.046(3) Uani 1 1 d . U .
H4A H 0.2827 0.6921 0.0886 0.055 Uiso 1 1 calc R U .
H4B H 0.3067 0.6302 0.0677 0.055 Uiso 1 1 calc R U .
C5 C 0.3380(5) 0.7317(8) 0.0770(4) 0.052(3) Uani 1 1 d . U .
H5A H 0.3649 0.7088 0.0734 0.063 Uiso 1 1 calc R U .
H5B H 0.3435 0.7692 0.0972 0.063 Uiso 1 1 calc R U .
C6 C 0.3190(5) 0.7728(9) 0.0425(4) 0.063(4) Uani 1 1 d . U .
H6A H 0.3132 0.7356 0.0225 0.094 Uiso 1 1 calc R U .
H6B H 0.3384 0.8117 0.0362 0.094 Uiso 1 1 calc R U .
H6C H 0.2932 0.7977 0.0463 0.094 Uiso 1 1 calc R U .
C7 C 0.2001(7) 0.2924(12) 0.1427(9) 0.154(10) Uani 1 1 d D U .
H7A H 0.2136 0.3357 0.1319 0.185 Uiso 1 1 calc R U .
H7B H 0.1959 0.3075 0.1676 0.185 Uiso 1 1 calc R U .
C8 C 0.1593(8) 0.2755(15) 0.1200(9) 0.174(14) Uani 1 1 d D U .
H8A H 0.1457 0.2311 0.1299 0.209 Uiso 1 1 calc R U .
H8B H 0.1626 0.2645 0.0945 0.209 Uiso 1 1 calc R U .
C9 C 0.1346(8) 0.3489(14) 0.1225(8) 0.147(10) Uani 1 1 d D U .
H9A H 0.1470 0.3784 0.1439 0.221 Uiso 1 1 calc R U .
H9B H 0.1059 0.3358 0.1247 0.221 Uiso 1 1 calc R U .
H9C H 0.1348 0.3797 0.1004 0.221 Uiso 1 1 calc R U .
C10 C 0.2577(6) 0.2114(12) 0.2476(3) 0.097(6) Uani 1 1 d D U .
H10A H 0.2682 0.2646 0.2515 0.117 Uiso 1 1 calc R U .
H10B H 0.2816 0.1762 0.2537 0.117 Uiso 1 1 calc R U .
C11 C 0.2274(7) 0.1962(19) 0.2731(6) 0.152(10) Uani 1 1 d D U .
H11A H 0.2306 0.2371 0.2919 0.183 Uiso 1 1 calc R U .
H11B H 0.2350 0.1470 0.2857 0.183 Uiso 1 1 calc R U .
C12 C 0.1825(8) 0.1923(15) 0.2565(8) 0.163(11) Uani 1 1 d D U .
H12A H 0.1748 0.2391 0.2424 0.245 Uiso 1 1 calc R U .
H12B H 0.1655 0.1878 0.2759 0.245 Uiso 1 1 calc R U .
H12C H 0.1778 0.1476 0.2404 0.245 Uiso 1 1 calc R U .
C13 C 0.3120(5) 0.3607(9) -0.0299(4) 0.058(4) Uani 1 1 d . U .
H13A H 0.3047 0.3163 -0.0463 0.069 Uiso 1 1 calc R U .
H13B H 0.3423 0.3689 -0.0271 0.069 Uiso 1 1 calc R U .
C14 C 0.2897(5) 0.4304(10) -0.0456(4) 0.066(4) Uani 1 1 d . U .
H14A H 0.2595 0.4207 -0.0484 0.079 Uiso 1 1 calc R U .
H14B H 0.2967 0.4392 -0.0703 0.079 Uiso 1 1 calc R U .
C15 C 0.2994(8) 0.5022(12) -0.0233(6) 0.111(7) Uani 1 1 d . U .
H15A H 0.3003 0.4903 0.0026 0.167 Uiso 1 1 calc R U .
H15B H 0.2779 0.5408 -0.0309 0.167 Uiso 1 1 calc R U .
H15C H 0.3264 0.5224 -0.0272 0.167 Uiso 1 1 calc R U .
C16 C 0.3063(4) 0.1598(8) 0.0021(4) 0.048(3) Uani 1 1 d . U .
H16A H 0.2822 0.1827 -0.0137 0.058 Uiso 1 1 calc R U .
H16B H 0.2967 0.1385 0.0240 0.058 Uiso 1 1 calc R U .
C17 C 0.3241(5) 0.0977(9) -0.0177(5) 0.068(4) Uani 1 1 d . U .
H17A H 0.3308 0.1186 -0.0409 0.081 Uiso 1 1 calc R U .
H17B H 0.3503 0.0803 -0.0029 0.081 Uiso 1 1 calc R U .
C18 C 0.2966(7) 0.0312(13) -0.0260(8) 0.136(11) Uani 1 1 d . U .
H18A H 0.2937 0.0046 -0.0032 0.204 Uiso 1 1 calc R U .
H18B H 0.3084 -0.0040 -0.0422 0.204 Uiso 1 1 calc R U .
H18C H 0.2693 0.0487 -0.0380 0.204 Uiso 1 1 calc R U .
C19 C 0.3095(4) -0.0470(8) 0.1074(4) 0.052(3) Uani 1 1 d . U .
H19A H 0.3140 -0.0872 0.0896 0.062 Uiso 1 1 calc R U .
H19B H 0.3000 0.0003 0.0939 0.062 Uiso 1 1 calc R U .
C20 C 0.2779(4) -0.0729(8) 0.1295(4) 0.058(4) Uani 1 1 d . U .
H20A H 0.2513 -0.0809 0.1130 0.070 Uiso 1 1 calc R U .
H20B H 0.2736 -0.0317 0.1468 0.070 Uiso 1 1 calc R U .
C21 C 0.2892(4) -0.1455(8) 0.1504(4) 0.056(4) Uani 1 1 d . U .
H21A H 0.2894 -0.1884 0.1333 0.084 Uiso 1 1 calc R U .
H21B H 0.2688 -0.1556 0.1665 0.084 Uiso 1 1 calc R U .
H21C H 0.3168 -0.1399 0.1651 0.084 Uiso 1 1 calc R U .
C22 C 0.4370(7) -0.1140(17) 0.1042(6) 0.161(10) Uani 1 1 d D U .
H22A H 0.4323 -0.1527 0.1226 0.193 Uiso 1 1 calc R U .
H22B H 0.4608 -0.0817 0.1148 0.193 Uiso 1 1 calc R U .
C23 C 0.4469(9) -0.1542(16) 0.0707(7) 0.158(11) Uani 1 1 d D U .
H23A H 0.4586 -0.1197 0.0537 0.190 Uiso 1 1 calc R U .
H23B H 0.4234 -0.1841 0.0576 0.190 Uiso 1 1 calc R U .
C24 C 0.4793(11) -0.203(2) 0.0937(9) 0.215(17) Uani 1 1 d D U .
H24A H 0.5019 -0.1706 0.1056 0.322 Uiso 1 1 calc R U .
H24B H 0.4903 -0.2410 0.0781 0.322 Uiso 1 1 calc R U .
H24C H 0.4667 -0.2303 0.1123 0.322 Uiso 1 1 calc R U .
C25 C 0.4372(4) 0.5385(7) 0.0058(3) 0.037(3) Uani 1 1 d . U .
H25A H 0.4161 0.5117 0.0175 0.044 Uiso 1 1 calc R U .
H25B H 0.4509 0.5003 -0.0081 0.044 Uiso 1 1 calc R U .
C26 C 0.4169(4) 0.5993(7) -0.0195(3) 0.039(3) Uani 1 1 d . U .
H26A H 0.3963 0.5748 -0.0385 0.047 Uiso 1 1 calc R U .
H26B H 0.4382 0.6240 -0.0319 0.047 Uiso 1 1 calc R U .
C27 C 0.3956(5) 0.6601(9) -0.0005(4) 0.058(4) Uani 1 1 d . U .
H27A H 0.3729 0.6368 0.0100 0.087 Uiso 1 1 calc R U .
H27B H 0.3845 0.6998 -0.0180 0.087 Uiso 1 1 calc R U .
H27C H 0.4156 0.6832 0.0190 0.087 Uiso 1 1 calc R U .
C28 C 0.5346(4) 0.5882(8) 0.1256(3) 0.041(3) Uani 1 1 d . U .
H28A H 0.5321 0.5348 0.1341 0.049 Uiso 1 1 calc R U .
H28B H 0.5220 0.6229 0.1419 0.049 Uiso 1 1 calc R U .
C29 C 0.5792(4) 0.6083(9) 0.1266(4) 0.051(3) Uani 1 1 d . U .
H29A H 0.5937 0.6055 0.1521 0.062 Uiso 1 1 calc R U .
H29B H 0.5813 0.6618 0.1181 0.062 Uiso 1 1 calc R U .
C30 C 0.6006(5) 0.5554(10) 0.1032(4) 0.069(4) Uani 1 1 d . U .
H30A H 0.5993 0.5025 0.1120 0.103 Uiso 1 1 calc R U .
H30B H 0.6296 0.5709 0.1045 0.103 Uiso 1 1 calc R U .
H30C H 0.5866 0.5584 0.0778 0.103 Uiso 1 1 calc R U .
C31 C 0.4888(4) 0.2643(9) 0.0071(3) 0.050(3) Uani 1 1 d . U .
H31A H 0.5022 0.3033 -0.0065 0.060 Uiso 1 1 calc R U .
H31B H 0.4790 0.2898 0.0280 0.060 Uiso 1 1 calc R U .
C32 C 0.4520(6) 0.2275(12) -0.0180(5) 0.086(5) Uani 1 1 d . U .
H32A H 0.4620 0.1928 -0.0358 0.103 Uiso 1 1 calc R U .
H32B H 0.4347 0.1975 -0.0034 0.103 Uiso 1 1 calc R U .
C33 C 0.4287(6) 0.2886(13) -0.0362(5) 0.096(6) Uani 1 1 d . U .
H33A H 0.4190 0.3224 -0.0183 0.145 Uiso 1 1 calc R U .
H33B H 0.4048 0.2677 -0.0527 0.145 Uiso 1 1 calc R U .
H33C H 0.4462 0.3178 -0.0504 0.145 Uiso 1 1 calc R U .
C34 C 0.5429(6) 0.0414(10) 0.0396(6) 0.117(8) Uani 1 1 d D U .
H34A H 0.5216 0.0563 0.0188 0.141 Uiso 1 1 calc R U .
H34B H 0.5301 0.0049 0.0550 0.141 Uiso 1 1 calc R U .
C35 C 0.5783(8) 0.0028(14) 0.0257(8) 0.153(10) Uani 1 1 d D U .
H35A H 0.5676 -0.0378 0.0079 0.184 Uiso 1 1 calc R U .
H35B H 0.5970 -0.0214 0.0461 0.184 Uiso 1 1 calc R U .
C36 C 0.6019(13) 0.0630(18) 0.0072(12) 0.26(2) Uani 1 1 d D U .
H36A H 0.5949 0.1144 0.0152 0.390 Uiso 1 1 calc R U .
H36B H 0.5942 0.0590 -0.0193 0.390 Uiso 1 1 calc R U .
H36C H 0.6318 0.0544 0.0140 0.390 Uiso 1 1 calc R U .
C37 C 0.3537(4) 0.0414(7) 0.2512(3) 0.036(3) Uani 1 1 d . U .
H37A H 0.3274 0.0699 0.2510 0.043 Uiso 1 1 calc R U .
H37B H 0.3705 0.0703 0.2358 0.043 Uiso 1 1 calc R U .
C38 C 0.3441(6) -0.0335(9) 0.2350(5) 0.073(5) Uani 1 1 d . U .
H38A H 0.3703 -0.0594 0.2317 0.088 Uiso 1 1 calc R U .
H38B H 0.3273 -0.0270 0.2106 0.088 Uiso 1 1 calc R U .
C39 C 0.3206(6) -0.0842(11) 0.2582(5) 0.098(6) Uani 1 1 d . U .
H39A H 0.3397 -0.1030 0.2794 0.147 Uiso 1 1 calc R U .
H39B H 0.3086 -0.1280 0.2436 0.147 Uiso 1 1 calc R U .
H39C H 0.2984 -0.0543 0.2664 0.147 Uiso 1 1 calc R U .
C40 C 0.4669(3) -0.1001(7) 0.3037(5) 0.061(4) Uani 1 1 d D U .
H40A H 0.4761 -0.0950 0.3303 0.073 Uiso 1 1 calc R U .
H40B H 0.4876 -0.0742 0.2910 0.073 Uiso 1 1 calc R U .
C41 C 0.4646(6) -0.1834(7) 0.2935(6) 0.095(6) Uani 1 1 d D U .
H41A H 0.4908 -0.2081 0.3048 0.113 Uiso 1 1 calc R U .
H41B H 0.4630 -0.1872 0.2667 0.113 Uiso 1 1 calc R U .
C42 C 0.4291(5) -0.2287(8) 0.3043(6) 0.088(6) Uani 1 1 d D U .
H42A H 0.4310 -0.2281 0.3309 0.133 Uiso 1 1 calc R U .
H42B H 0.4305 -0.2819 0.2959 0.133 Uiso 1 1 calc R U .
H42C H 0.4028 -0.2057 0.2931 0.133 Uiso 1 1 calc R U .
C43 C 0.3068(4) 0.4363(6) 0.2709(3) 0.034(2) Uani 1 1 d . U .
H43A H 0.2889 0.4266 0.2472 0.040 Uiso 1 1 calc R U .
H43B H 0.3318 0.4639 0.2660 0.040 Uiso 1 1 calc R U .
C44 C 0.2840(4) 0.4853(7) 0.2939(4) 0.044(3) Uani 1 1 d . U .
H44A H 0.2613 0.4543 0.3014 0.053 Uiso 1 1 calc R U .
H44B H 0.2710 0.5281 0.2787 0.053 Uiso 1 1 calc R U .
C45 C 0.3094(4) 0.5187(8) 0.3277(4) 0.055(4) Uani 1 1 d . U .
H45A H 0.3217 0.4770 0.3436 0.082 Uiso 1 1 calc R U .
H45B H 0.2915 0.5499 0.3408 0.082 Uiso 1 1 calc R U .
H45C H 0.3315 0.5509 0.3208 0.082 Uiso 1 1 calc R U .
C46 C 0.3326(3) 0.2958(7) 0.3690(3) 0.033(3) Uani 1 1 d . U .
H46A H 0.3436 0.2427 0.3712 0.039 Uiso 1 1 calc R U .
H46B H 0.3046 0.2948 0.3543 0.039 Uiso 1 1 calc R U .
C47 C 0.3309(4) 0.3287(7) 0.4062(3) 0.034(3) Uani 1 1 d . U .
H47A H 0.3191 0.3812 0.4035 0.041 Uiso 1 1 calc R U .
H47B H 0.3593 0.3324 0.4200 0.041 Uiso 1 1 calc R U .
C48 C 0.3046(4) 0.2797(9) 0.4273(4) 0.052(4) Uani 1 1 d . U .
H48A H 0.2767 0.2743 0.4133 0.078 Uiso 1 1 calc R U .
H48B H 0.3028 0.3042 0.4508 0.078 Uiso 1 1 calc R U .
H48C H 0.3172 0.2288 0.4316 0.078 Uiso 1 1 calc R U .
C49 C 0.4348(4) 0.6545(7) 0.2021(3) 0.036(3) Uani 1 1 d . U .
H49A H 0.4128 0.6409 0.2164 0.043 Uiso 1 1 calc R U .
H49B H 0.4416 0.6081 0.1888 0.043 Uiso 1 1 calc R U .
C50 C 0.4195(4) 0.7165(7) 0.1753(4) 0.047(3) Uani 1 1 d . U .
H50A H 0.4412 0.7263 0.1601 0.057 Uiso 1 1 calc R U .
H50B H 0.3948 0.6968 0.1590 0.057 Uiso 1 1 calc R U .
C51 C 0.4085(5) 0.7900(9) 0.1906(5) 0.070(5) Uani 1 1 d . U .
H51A H 0.3879 0.7812 0.2067 0.105 Uiso 1 1 calc R U .
H51B H 0.3969 0.8245 0.1707 0.105 Uiso 1 1 calc R U .
H51C H 0.4333 0.8134 0.2046 0.105 Uiso 1 1 calc R U .
O1 O 0.2664(2) 0.5862(4) 0.1422(2) 0.0355(19) Uani 1 1 d . U .
O2 O 0.3280(2) 0.6369(4) 0.1213(2) 0.0323(17) Uani 1 1 d . U .
O3 O 0.2259(3) 0.2261(6) 0.1445(4) 0.094(4) Uani 1 1 d D U .
O4 O 0.2411(4) 0.2021(7) 0.2104(3) 0.077(3) Uani 1 1 d D U .
O5 O 0.3000(2) 0.3457(5) 0.0056(2) 0.0362(19) Uani 1 1 d . U .
O6 O 0.3374(2) 0.2180(5) 0.0128(2) 0.0350(18) Uani 1 1 d . U .
O7 O 0.3480(3) -0.0321(5) 0.1324(2) 0.042(2) Uani 1 1 d . U .
O8 O 0.4014(3) -0.0677(5) 0.0957(3) 0.065(3) Uani 1 1 d D U .
O9 O 0.4678(2) 0.5740(4) 0.0334(2) 0.0344(18) Uani 1 1 d . U .
O10 O 0.5131(2) 0.5960(5) 0.0882(2) 0.0341(18) Uani 1 1 d . U .
O11 O 0.5183(3) 0.2042(5) 0.0202(2) 0.0390(19) Uani 1 1 d . U .
O12 O 0.5567(3) 0.1081(5) 0.0606(2) 0.050(2) Uani 1 1 d D U .
O13 O 0.3761(2) 0.0395(4) 0.28844(19) 0.0270(16) Uani 1 1 d . U .
O14 O 0.4272(2) -0.0638(4) 0.2937(2) 0.0272(16) Uani 1 1 d D U .
O15 O 0.3191(2) 0.3624(4) 0.2888(2) 0.0287(16) Uani 1 1 d . U .
O16 O 0.3598(2) 0.3449(4) 0.35206(18) 0.0228(15) Uani 1 1 d . U .
O17 O 0.4712(2) 0.6806(4) 0.22628(19) 0.0258(16) Uani 1 1 d . U .
P1 P 0.31115(9) 0.55995(16) 0.13566(8) 0.0274(6) Uani 1 1 d . . .
P2 P 0.26461(9) 0.21935(19) 0.17847(9) 0.0378(7) Uani 1 1 d . . .
P3 P 0.32810(8) 0.29216(17) 0.03427(7) 0.0262(6) Uani 1 1 d . . .
P4 P 0.38724(9) 0.00197(16) 0.11779(8) 0.0295(6) Uani 1 1 d . . .
P5 P 0.47547(9) 0.54129(16) 0.07357(7) 0.0252(6) Uani 1 1 d . . .
P6 P 0.52597(9) 0.17801(16) 0.06129(8) 0.0277(6) Uani 1 1 d . . .
P7 P 0.42335(8) 0.02558(14) 0.29951(7) 0.0200(5) Uani 1 1 d . . .
P8 P 0.36286(8) 0.33957(15) 0.31002(7) 0.0195(5) Uani 1 1 d . . .
P9 P 0.5000 0.6202(2) 0.2500 0.0210(8) Uani 1 2 d S T P
Pt1 Pt 0.44731(2) 0.30895(2) 0.18465(2) 0.01515(8) Uani 1 1 d . . .
S1 S 0.34570(9) 0.53138(17) 0.18225(8) 0.0321(6) Uani 1 1 d . . .
S2 S 0.30319(8) 0.48281(16) 0.09467(8) 0.0293(6) Uani 1 1 d . . .
S3 S 0.29089(8) 0.32362(16) 0.18686(8) 0.0296(6) Uani 1 1 d . . .
S4 S 0.29945(10) 0.13293(17) 0.16794(9) 0.0374(7) Uani 1 1 d . . .
S5 S 0.29186(8) 0.26793(16) 0.07140(7) 0.0265(6) Uani 1 1 d . . .
S6 S 0.38454(8) 0.33822(17) 0.04874(7) 0.0286(6) Uani 1 1 d . . .
S7 S 0.37389(9) 0.08822(17) 0.08350(8) 0.0308(6) Uani 1 1 d . . .
S8 S 0.42742(8) 0.01998(15) 0.16405(8) 0.0273(6) Uani 1 1 d . . .
S9 S 0.42853(9) 0.56474(16) 0.10060(8) 0.0320(6) Uani 1 1 d . . .
S10 S 0.49309(9) 0.43236(16) 0.07394(8) 0.0324(6) Uani 1 1 d . . .
S11 S 0.55578(9) 0.25933(16) 0.09246(7) 0.0285(6) Uani 1 1 d . . .
S12 S 0.47105(9) 0.14397(16) 0.07403(7) 0.0289(6) Uani 1 1 d . . .
S13 S 0.45590(8) 0.07887(14) 0.26544(7) 0.0230(5) Uani 1 1 d . . .
S14 S 0.56370(8) 0.04990(15) 0.14714(7) 0.0250(5) Uani 1 1 d . . .
S15 S 0.37218(8) 0.23089(14) 0.29590(7) 0.0216(5) Uani 1 1 d . . .
S16 S 0.59449(8) 0.41940(14) 0.19596(7) 0.0215(5) Uani 1 1 d . . .
S17 S 0.53304(8) 0.55809(15) 0.22006(8) 0.0285(6) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
S6 Ag1 Pt1 150.90(7) . .
S6 Ag1 Ag5 104.47(7) . .
Pt1 Ag1 Ag5 59.75(2) . .
S6 Ag1 Ag4 92.06(7) . .
Pt1 Ag1 Ag4 59.20(2) . .
Ag5 Ag1 Ag4 61.65(3) . .
S6 Ag1 Ag13 101.01(7) . .
Pt1 Ag1 Ag13 107.74(3) . .
Ag5 Ag1 Ag13 113.76(3) . .
Ag4 Ag1 Ag13 166.93(4) . .
S6 Ag1 Ag16 90.54(7) . .
Pt1 Ag1 Ag16 105.50(3) . .
Ag5 Ag1 Ag16 164.73(4) . .
Ag4 Ag1 Ag16 115.95(3) . .
Ag13 Ag1 Ag16 64.87(3) . .
S6 Ag1 Ag17 54.44(7) . .
Pt1 Ag1 Ag17 110.26(3) . .
Ag5 Ag1 Ag17 121.48(3) . .
Ag4 Ag1 Ag17 65.32(3) . .
Ag13 Ag1 Ag17 123.18(3) . .
Ag16 Ag1 Ag17 65.29(3) . .
S6 Ag1 Ag2 141.49(7) . .
Pt1 Ag1 Ag2 56.65(2) . .
Ag5 Ag1 Ag2 62.34(3) . .
Ag4 Ag1 Ag2 109.07(3) . .
Ag13 Ag1 Ag2 59.87(3) . .
Ag16 Ag1 Ag2 107.27(3) . .
Ag17 Ag1 Ag2 164.00(4) . .
S6 Ag1 Ag3 147.45(7) . .
Pt1 Ag1 Ag3 56.11(2) . .
Ag5 Ag1 Ag3 107.91(3) . .
Ag4 Ag1 Ag3 105.98(3) . .
Ag13 Ag1 Ag3 62.78(3) . .
Ag16 Ag1 Ag3 57.33(3) . .
Ag17 Ag1 Ag3 108.72(3) . .
Ag2 Ag1 Ag3 57.21(2) . .
S6 Ag1 Ag9 114.80(7) . .
Pt1 Ag1 Ag9 56.24(2) . .
Ag5 Ag1 Ag9 107.38(3) . .
Ag4 Ag1 Ag9 58.62(3) . .
Ag13 Ag1 Ag9 115.01(3) . .
Ag16 Ag1 Ag9 62.64(3) . .
Ag17 Ag1 Ag9 60.37(3) . .
Ag2 Ag1 Ag9 103.70(3) . .
Ag3 Ag1 Ag9 57.82(2) . .
S8 Ag2 Pt1 152.26(7) . .
S8 Ag2 Ag6 92.61(7) . .
Pt1 Ag2 Ag6 59.68(2) . .
S8 Ag2 Ag3 141.39(7) . .
Pt1 Ag2 Ag3 58.14(2) . .
Ag6 Ag2 Ag3 109.63(3) . .
S8 Ag2 Ag13 100.62(7) . .
Pt1 Ag2 Ag13 106.99(3) . .
Ag6 Ag2 Ag13 164.62(4) . .
Ag3 Ag2 Ag13 64.00(3) . .
S8 Ag2 Ag7 108.83(7) . .
Pt1 Ag2 Ag7 60.20(2) . .
Ag6 Ag2 Ag7 64.20(3) . .
Ag3 Ag2 Ag7 58.64(3) . .
Ag13 Ag2 Ag7 117.69(3) . .
S8 Ag2 Ag1 141.90(7) . .
Pt1 Ag2 Ag1 57.41(2) . .
Ag6 Ag2 Ag1 106.42(3) . .
Ag3 Ag2 Ag1 62.05(3) . .
Ag13 Ag2 Ag1 58.23(3) . .
Ag7 Ag2 Ag1 109.15(3) . .
S8 Ag2 Ag14 53.57(6) . .
Pt1 Ag2 Ag14 108.06(3) . .
Ag6 Ag2 Ag14 62.53(3) . .
Ag3 Ag2 Ag14 165.03(4) . .
Ag13 Ag2 Ag14 119.95(3) . .
Ag7 Ag2 Ag14 121.84(3) . .
Ag1 Ag2 Ag14 106.59(3) . .
S8 Ag2 Ag5 111.18(7) . .
Pt1 Ag2 Ag5 57.85(2) . .
Ag6 Ag2 Ag5 59.75(3) . .
Ag3 Ag2 Ag5 107.29(3) . .
Ag13 Ag2 Ag5 107.53(3) . .
Ag7 Ag2 Ag5 110.58(3) . .
Ag1 Ag2 Ag5 56.73(2) . .
Ag14 Ag2 Ag5 57.88(3) . .
S3 Ag3 Pt1 153.26(7) . .
S3 Ag3 Ag16 56.65(7) . .
Pt1 Ag3 Ag16 108.20(3) . .
S3 Ag3 Ag7 133.15(7) . .
Pt1 Ag3 Ag7 61.54(2) . .
Ag16 Ag3 Ag7 169.65(4) . .
S3 Ag3 Ag2 145.05(7) . .
Pt1 Ag3 Ag2 58.26(2) . .
Ag16 Ag3 Ag2 112.29(3) . .
Ag7 Ag3 Ag2 62.11(3) . .
S3 Ag3 Ag9 95.68(7) . .
Pt1 Ag3 Ag9 57.80(2) . .
Ag16 Ag3 Ag9 64.79(3) . .
Ag7 Ag3 Ag9 107.86(3) . .
Ag2 Ag3 Ag9 109.26(3) . .
S3 Ag3 Ag8 107.59(7) . .
Pt1 Ag3 Ag8 57.46(2) . .
Ag16 Ag3 Ag8 118.44(3) . .
Ag7 Ag3 Ag8 58.38(3) . .
Ag2 Ag3 Ag8 106.34(3) . .
Ag9 Ag3 Ag8 58.03(3) . .
S3 Ag3 Ag1 115.98(7) . .
Pt1 Ag3 Ag1 56.97(2) . .
Ag16 Ag3 Ag1 59.60(3) . .
Ag7 Ag3 Ag1 110.86(3) . .
Ag2 Ag3 Ag1 60.74(3) . .
Ag9 Ag3 Ag1 61.27(3) . .
Ag8 Ag3 Ag1 106.41(3) . .
S3 Ag3 Ag13 89.58(7) . .
Pt1 Ag3 Ag13 103.08(3) . .
Ag16 Ag3 Ag13 63.18(3) . .
Ag7 Ag3 Ag13 116.11(3) . .
Ag2 Ag3 Ag13 58.79(3) . .
Ag9 Ag3 Ag13 112.27(3) . .
Ag8 Ag3 Ag13 160.48(3) . .
Ag1 Ag3 Ag13 56.29(2) . .
S10 Ag4 Pt1 149.93(7) . .
S10 Ag4 Ag1 108.40(8) . .
Pt1 Ag4 Ag1 58.49(2) . .
S10 Ag4 Ag9 145.21(8) . .
Pt1 Ag4 Ag9 57.78(2) . .
Ag1 Ag4 Ag9 63.66(3) . .
S10 Ag4 Ag12 140.01(8) . .
Pt1 Ag4 Ag12 59.58(2) . .
Ag1 Ag4 Ag12 111.56(3) . .
Ag9 Ag4 Ag12 60.72(3) . .
S10 Ag4 Ag10 107.27(8) . .
Pt1 Ag4 Ag10 58.64(2) . .
Ag1 Ag4 Ag10 106.75(3) . .
Ag9 Ag4 Ag10 107.40(3) . .
Ag12 Ag4 Ag10 59.30(3) . .
S10 Ag4 Ag5 91.31(7) . .
Pt1 Ag4 Ag5 58.62(2) . .
Ag1 Ag4 Ag5 59.08(3) . .
Ag9 Ag4 Ag5 109.31(3) . .
Ag12 Ag4 Ag5 107.53(3) . .
Ag10 Ag4 Ag5 58.41(3) . .
S10 Ag4 Ag17 86.51(8) . .
Pt1 Ag4 Ag17 104.93(3) . .
Ag1 Ag4 Ag17 59.18(3) . .
Ag9 Ag4 Ag17 59.86(3) . .
Ag12 Ag4 Ag17 115.46(3) . .
Ag10 Ag4 Ag17 163.52(3) . .
Ag5 Ag4 Ag17 113.61(3) . .
S12 Ag5 Pt1 144.62(7) . .
S12 Ag5 Ag10 154.57(7) . .
Pt1 Ag5 Ag10 59.10(2) . .
S12 Ag5 Ag1 96.16(7) . .
Pt1 Ag5 Ag1 58.33(2) . .
Ag10 Ag5 Ag1 108.47(3) . .
S12 Ag5 Ag14 55.30(6) . .
Pt1 Ag5 Ag14 108.91(3) . .
Ag10 Ag5 Ag14 117.23(3) . .
Ag1 Ag5 Ag14 112.72(3) . .
S12 Ag5 Ag6 118.01(7) . .
Pt1 Ag5 Ag6 57.96(2) . .
Ag10 Ag5 Ag6 60.86(3) . .
Ag1 Ag5 Ag6 107.66(3) . .
Ag14 Ag5 Ag6 62.71(3) . .
S12 Ag5 Ag4 133.07(7) . .
Pt1 Ag5 Ag4 57.94(2) . .
Ag10 Ag5 Ag4 60.33(3) . .
Ag1 Ag5 Ag4 59.28(3) . .
Ag14 Ag5 Ag4 166.54(4) . .
Ag6 Ag5 Ag4 107.89(3) . .
S12 Ag5 S11 75.02(8) . .
Pt1 Ag5 S11 140.34(6) . .
Ag10 Ag5 S11 82.37(6) . .
Ag1 Ag5 S11 137.65(6) . .
Ag14 Ag5 S11 96.22(6) . .
Ag6 Ag5 S11 113.03(6) . .
Ag4 Ag5 S11 96.48(6) . .
S12 Ag5 Ag15 94.43(7) . .
Pt1 Ag5 Ag15 109.80(3) . .
Ag10 Ag5 Ag15 61.76(3) . .
Ag1 Ag5 Ag15 168.13(4) . .
Ag14 Ag5 Ag15 69.46(3) . .
Ag6 Ag5 Ag15 62.30(3) . .
Ag4 Ag5 Ag15 116.00(3) . .
S11 Ag5 Ag15 50.97(6) . .
S12 Ag5 Ag2 91.37(6) . .
Pt1 Ag5 Ag2 55.80(2) . .
Ag10 Ag5 Ag2 105.84(3) . .
Ag1 Ag5 Ag2 60.93(3) . .
Ag14 Ag5 Ag2 60.89(3) . .
Ag6 Ag5 Ag2 57.04(2) . .
Ag4 Ag5 Ag2 106.22(3) . .
S11 Ag5 Ag2 157.06(6) . .
Ag15 Ag5 Ag2 113.53(3) . .
S13 Ag6 Pt1 165.07(6) 2_655 .
S13 Ag6 Ag2 122.76(7) 2_655 .
Pt1 Ag6 Ag2 58.16(2) . .
S13 Ag6 Ag11 110.14(6) 2_655 .
Pt1 Ag6 Ag11 58.702(18) . .
Ag2 Ag6 Ag11 107.56(3) . .
S13 Ag6 Ag10 127.14(7) 2_655 .
Pt1 Ag6 Ag10 58.38(2) . .
Ag2 Ag6 Ag10 108.63(3) . .
Ag11 Ag6 Ag10 60.20(2) . .
S13 Ag6 Ag5 136.18(6) 2_655 .
Pt1 Ag6 Ag5 58.65(2) . .
Ag2 Ag6 Ag5 63.22(3) . .
Ag11 Ag6 Ag5 107.54(3) . .
Ag10 Ag6 Ag5 58.20(2) . .
S13 Ag6 Ag7 57.72(6) 2_655 2_655
Pt1 Ag6 Ag7 116.62(3) . 2_655
Ag2 Ag6 Ag7 163.65(4) . 2_655
Ag11 Ag6 Ag7 60.90(2) . 2_655
Ag10 Ag6 Ag7 76.67(3) . 2_655
Ag5 Ag6 Ag7 129.49(3) . 2_655
S13 Ag6 Ag14 85.24(6) 2_655 .
Pt1 Ag6 Ag14 106.11(3) . .
Ag2 Ag6 Ag14 61.51(3) . .
Ag11 Ag6 Ag14 164.62(3) . .
Ag10 Ag6 Ag14 111.18(3) . .
Ag5 Ag6 Ag14 58.57(3) . .
Ag7 Ag6 Ag14 132.04(3) 2_655 .
S13 Ag6 Ag15 85.27(6) 2_655 .
Pt1 Ag6 Ag15 107.93(3) . .
Ag2 Ag6 Ag15 116.41(3) . .
Ag11 Ag6 Ag15 113.48(3) . .
Ag10 Ag6 Ag15 59.88(2) . .
Ag5 Ag6 Ag15 59.37(3) . .
Ag7 Ag6 Ag15 79.78(3) 2_655 .
Ag14 Ag6 Ag15 66.78(3) . .
S13 Ag6 Ag7 108.31(6) 2_655 .
Pt1 Ag6 Ag7 58.14(2) . .
Ag2 Ag6 Ag7 59.72(3) . .
Ag11 Ag6 Ag7 59.09(2) . .
Ag10 Ag6 Ag7 107.40(3) . .
Ag5 Ag6 Ag7 109.79(3) . .
Ag7 Ag6 Ag7 104.03(3) 2_655 .
Ag14 Ag6 Ag7 116.84(3) . .
Ag15 Ag6 Ag7 165.93(3) . .
S13 Ag7 Ag8 156.60(6) . .
S13 Ag7 Ag3 140.15(6) . .
Ag8 Ag7 Ag3 63.20(3) . .
S13 Ag7 Pt1 129.95(6) . .
Ag8 Ag7 Pt1 57.74(2) . .
Ag3 Ag7 Pt1 56.98(2) . .
S13 Ag7 S15 94.91(7) . .
Ag8 Ag7 S15 80.83(5) . .
Ag3 Ag7 S15 90.90(6) . .
Pt1 Ag7 S15 135.13(6) . .
S13 Ag7 Ag11 104.49(6) . .
Ag8 Ag7 Ag11 58.94(3) . .
Ag3 Ag7 Ag11 107.49(3) . .
Pt1 Ag7 Ag11 56.849(17) . .
S15 Ag7 Ag11 117.53(6) . .
S13 Ag7 Ag6 53.94(6) . 2_655
Ag8 Ag7 Ag6 103.05(3) . 2_655
Ag3 Ag7 Ag6 165.01(4) . 2_655
Pt1 Ag7 Ag6 111.53(3) . 2_655
S15 Ag7 Ag6 92.69(6) . 2_655
Ag11 Ag7 Ag6 58.12(2) . 2_655
S13 Ag7 Ag2 91.20(6) . .
Ag8 Ag7 Ag2 107.83(3) . .
Ag3 Ag7 Ag2 59.25(3) . .
Pt1 Ag7 Ag2 55.96(2) . .
S15 Ag7 Ag2 136.33(6) . .
Ag11 Ag7 Ag2 102.45(3) . .
Ag6 Ag7 Ag2 124.68(3) 2_655 .
S13 Ag7 Ag6 75.19(6) . .
Ag8 Ag7 Ag6 103.85(3) . .
Ag3 Ag7 Ag6 103.68(3) . .
Pt1 Ag7 Ag6 55.51(2) . .
S15 Ag7 Ag6 165.28(6) . .
Ag11 Ag7 Ag6 56.48(2) . .
Ag6 Ag7 Ag6 72.71(3) 2_655 .
Ag2 Ag7 Ag6 56.09(2) . .
S16 Ag8 Pt1 166.34(7) 2_655 .
S16 Ag8 Ag11 108.93(6) 2_655 .
Pt1 Ag8 Ag11 58.882(17) . .
S16 Ag8 Ag7 108.67(6) 2_655 .
Pt1 Ag8 Ag7 61.19(2) . .
Ag11 Ag8 Ag7 61.88(3) . .
S16 Ag8 Ag9 135.43(7) 2_655 .
Pt1 Ag8 Ag9 58.14(2) . .
Ag11 Ag8 Ag9 108.91(3) . .
Ag7 Ag8 Ag9 109.42(3) . .
S16 Ag8 Ag12 121.71(6) 2_655 .
Pt1 Ag8 Ag12 59.94(2) . .
Ag11 Ag8 Ag12 61.21(3) . .
Ag7 Ag8 Ag12 112.45(3) . .
Ag9 Ag8 Ag12 61.10(3) . .
S16 Ag8 Ag3 128.07(6) 2_655 .
Pt1 Ag8 Ag3 56.41(2) . .
Ag11 Ag8 Ag3 106.09(3) . .
Ag7 Ag8 Ag3 58.42(3) . .
Ag9 Ag8 Ag3 59.82(3) . .
Ag12 Ag8 Ag3 108.42(3) . .
S16 Ag8 Ag10 52.46(6) 2_655 2_655
Pt1 Ag8 Ag10 114.15(3) . 2_655
Ag11 Ag8 Ag10 57.855(19) . 2_655
Ag7 Ag8 Ag10 74.77(3) . 2_655
Ag9 Ag8 Ag10 163.20(3) . 2_655
Ag12 Ag8 Ag10 102.13(3) . 2_655
Ag3 Ag8 Ag10 130.87(3) . 2_655
S1 Ag9 Pt1 155.88(7) . .
S1 Ag9 Ag8 97.60(7) . .
Pt1 Ag9 Ag8 58.87(2) . .
S1 Ag9 Ag4 142.01(8) . .
Pt1 Ag9 Ag4 59.02(2) . .
Ag8 Ag9 Ag4 107.93(3) . .
S1 Ag9 Ag12 115.33(7) . .
Pt1 Ag9 Ag12 59.63(2) . .
Ag8 Ag9 Ag12 59.59(3) . .
Ag4 Ag9 Ag12 59.77(3) . .
S1 Ag9 Ag3 108.91(8) . .
Pt1 Ag9 Ag3 57.43(2) . .
Ag8 Ag9 Ag3 62.15(3) . .
Ag4 Ag9 Ag3 107.78(3) . .
Ag12 Ag9 Ag3 109.08(3) . .
S1 Ag9 Ag17 93.69(7) . .
Pt1 Ag9 Ag17 109.45(3) . .
Ag8 Ag9 Ag17 167.97(4) . .
Ag4 Ag9 Ag17 64.42(3) . .
Ag12 Ag9 Ag17 118.72(3) . .
Ag3 Ag9 Ag17 110.12(3) . .
S1 Ag9 Ag1 138.00(7) . .
Pt1 Ag9 Ag1 56.74(2) . .
Ag8 Ag9 Ag1 109.31(3) . .
Ag4 Ag9 Ag1 57.72(2) . .
Ag12 Ag9 Ag1 106.10(3) . .
Ag3 Ag9 Ag1 60.91(3) . .
Ag17 Ag9 Ag1 58.97(3) . .
S1 Ag9 Ag16 82.90(7) . .
Pt1 Ag9 Ag16 101.37(3) . .
Ag8 Ag9 Ag16 114.56(3) . .
Ag4 Ag9 Ag16 109.97(3) . .
Ag12 Ag9 Ag16 160.84(3) . .
Ag3 Ag9 Ag16 56.45(3) . .
Ag17 Ag9 Ag16 62.70(3) . .
Ag1 Ag9 Ag16 56.96(2) . .
S16 Ag10 Pt1 150.90(6) . .
S16 Ag10 Ag5 144.56(6) . .
Pt1 Ag10 Ag5 59.56(2) . .
S16 Ag10 Ag12 91.29(6) . .
Pt1 Ag10 Ag12 59.84(2) . .
Ag5 Ag10 Ag12 110.64(3) . .
S16 Ag10 Ag11 106.47(6) . .
Pt1 Ag10 Ag11 58.065(16) . .
Ag5 Ag10 Ag11 108.49(3) . .
Ag12 Ag10 Ag11 60.79(3) . .
S16 Ag10 Ag4 112.52(6) . .
Pt1 Ag10 Ag4 58.39(2) . .
Ag5 Ag10 Ag4 61.26(3) . .
Ag12 Ag10 Ag4 60.26(3) . .
Ag11 Ag10 Ag4 107.88(3) . .
S16 Ag10 Ag6 138.80(6) . .
Pt1 Ag10 Ag6 58.13(2) . .
Ag5 Ag10 Ag6 60.94(3) . .
Ag12 Ag10 Ag6 108.64(3) . .
Ag11 Ag10 Ag6 58.63(3) . .
Ag4 Ag10 Ag6 108.67(3) . .
S16 Ag10 Ag15 99.24(6) . .
Pt1 Ag10 Ag15 109.54(3) . .
Ag5 Ag10 Ag15 61.00(3) . .
Ag12 Ag10 Ag15 169.35(3) . .
Ag11 Ag10 Ag15 114.04(3) . .
Ag4 Ag10 Ag15 116.15(3) . .
Ag6 Ag10 Ag15 62.07(3) . .
S16 Ag10 Ag8 51.41(6) . 2_655
Pt1 Ag10 Ag8 112.93(3) . 2_655
Ag5 Ag10 Ag8 157.94(3) . 2_655
Ag12 Ag10 Ag8 77.45(3) . 2_655
Ag11 Ag10 Ag8 56.38(2) . 2_655
Ag4 Ag10 Ag8 135.38(3) . 2_655
Ag6 Ag10 Ag8 97.16(3) . 2_655
Ag15 Ag10 Ag8 107.97(3) . 2_655
Pt1 Ag11 Pt1 176.22(4) . 2_655
Pt1 Ag11 Ag8 58.947(17) . .
Pt1 Ag11 Ag8 122.81(2) 2_655 .
Pt1 Ag11 Ag8 122.80(2) . 2_655
Pt1 Ag11 Ag8 58.948(17) 2_655 2_655
Ag8 Ag11 Ag8 133.68(5) . 2_655
Pt1 Ag11 Ag6 59.285(19) . .
Pt1 Ag11 Ag6 117.34(3) 2_655 .
Ag8 Ag11 Ag6 110.33(2) . .
Ag8 Ag11 Ag6 105.41(2) 2_655 .
Pt1 Ag11 Ag6 117.35(3) . 2_655
Pt1 Ag11 Ag6 59.284(19) 2_655 2_655
Ag8 Ag11 Ag6 105.42(2) . 2_655
Ag8 Ag11 Ag6 110.33(2) 2_655 2_655
Ag6 Ag11 Ag6 77.55(4) . 2_655
Pt1 Ag11 Ag10 58.892(17) . .
Pt1 Ag11 Ag10 121.700(17) 2_655 .
Ag8 Ag11 Ag10 107.77(3) . .
Ag8 Ag11 Ag10 65.76(2) 2_655 .
Ag6 Ag11 Ag10 61.17(2) . .
Ag6 Ag11 Ag10 133.70(4) 2_655 .
Pt1 Ag11 Ag10 121.701(17) . 2_655
Pt1 Ag11 Ag10 58.892(17) 2_655 2_655
Ag8 Ag11 Ag10 65.77(2) . 2_655
Ag8 Ag11 Ag10 107.77(3) 2_655 2_655
Ag6 Ag11 Ag10 133.70(4) . 2_655
Ag6 Ag11 Ag10 61.17(2) 2_655 2_655
Ag10 Ag11 Ag10 164.62(5) . 2_655
Pt1 Ag11 Ag12 124.21(3) . 2_655
Pt1 Ag11 Ag12 59.511(19) 2_655 2_655
Ag8 Ag11 Ag12 81.16(3) . 2_655
Ag8 Ag11 Ag12 59.94(3) 2_655 2_655
Ag6 Ag11 Ag12 165.04(2) . 2_655
Ag6 Ag11 Ag12 109.35(2) 2_655 2_655
Ag10 Ag11 Ag12 106.88(3) . 2_655
Ag10 Ag11 Ag12 59.13(2) 2_655 2_655
Pt1 Ag11 Ag12 59.511(19) . .
Pt1 Ag11 Ag12 124.21(3) 2_655 .
Ag8 Ag11 Ag12 59.94(3) . .
Ag8 Ag11 Ag12 81.16(3) 2_655 .
Ag6 Ag11 Ag12 109.36(2) . .
Ag6 Ag11 Ag12 165.04(2) 2_655 .
Ag10 Ag11 Ag12 59.13(2) . .
Ag10 Ag11 Ag12 106.88(3) 2_655 .
Ag12 Ag11 Ag12 67.36(4) 2_655 .
Pt1 Ag11 Ag7 117.24(3) . 2_655
Pt1 Ag11 Ag7 60.228(18) 2_655 2_655
Ag8 Ag11 Ag7 167.12(4) . 2_655
Ag8 Ag11 Ag7 59.18(2) 2_655 2_655
Ag6 Ag11 Ag7 60.98(3) . 2_655
Ag6 Ag11 Ag7 64.43(3) 2_655 2_655
Ag10 Ag11 Ag7 77.13(2) . 2_655
Ag10 Ag11 Ag7 112.34(2) 2_655 2_655
Ag12 Ag11 Ag7 109.20(2) 2_655 2_655
Ag12 Ag11 Ag7 130.52(2) . 2_655
Pt1 Ag11 Ag7 60.231(18) . .
Pt1 Ag11 Ag7 117.24(3) 2_655 .
Ag8 Ag11 Ag7 59.19(2) . .
Ag8 Ag11 Ag7 167.12(4) 2_655 .
Ag6 Ag11 Ag7 64.43(3) . .
Ag6 Ag11 Ag7 60.98(3) 2_655 .
Ag10 Ag11 Ag7 112.34(2) . .
Ag10 Ag11 Ag7 77.13(2) 2_655 .
Ag12 Ag11 Ag7 130.51(2) 2_655 .
Ag12 Ag11 Ag7 109.20(2) . .
Ag7 Ag11 Ag7 107.97(4) 2_655 .
S17 Ag12 Pt1 158.48(7) . .
S17 Ag12 Ag10 99.94(7) . .
Pt1 Ag12 Ag10 58.56(2) . .
S17 Ag12 Ag8 138.82(7) . .
Pt1 Ag12 Ag8 57.90(2) . .
Ag10 Ag12 Ag8 107.66(3) . .
S17 Ag12 Ag4 112.62(7) . .
Pt1 Ag12 Ag4 58.06(2) . .
Ag10 Ag12 Ag4 60.44(3) . .
Ag8 Ag12 Ag4 107.49(3) . .
S17 Ag12 Ag11 114.91(7) . .
Pt1 Ag12 Ag11 57.434(19) . .
Ag10 Ag12 Ag11 60.08(2) . .
Ag8 Ag12 Ag11 58.85(2) . .
Ag4 Ag12 Ag11 107.47(3) . .
S17 Ag12 Ag9 138.57(7) . .
Pt1 Ag12 Ag9 56.90(2) . .
Ag10 Ag12 Ag9 107.33(3) . .
Ag8 Ag12 Ag9 59.31(3) . .
Ag4 Ag12 Ag9 59.50(3) . .
Ag11 Ag12 Ag9 105.67(3) . .
S17 Ag12 Ag12 70.23(7) . 2_655
Pt1 Ag12 Ag12 111.682(19) . 2_655
Ag10 Ag12 Ag12 99.64(3) . 2_655
Ag8 Ag12 Ag12 75.41(3) . 2_655
Ag4 Ag12 Ag12 160.00(3) . 2_655
Ag11 Ag12 Ag12 56.318(18) . 2_655
Ag9 Ag12 Ag12 132.26(4) . 2_655
S4 Ag13 S7 118.35(10) . .
S4 Ag13 S5 112.25(10) . .
S7 Ag13 S5 105.57(9) . .
S4 Ag13 Ag1 135.13(8) . .
S7 Ag13 Ag1 94.05(7) . .
S5 Ag13 Ag1 84.71(6) . .
S4 Ag13 Ag2 93.47(8) . .
S7 Ag13 Ag2 78.14(7) . .
S5 Ag13 Ag2 146.61(7) . .
Ag1 Ag13 Ag2 61.91(3) . .
S4 Ag13 Ag3 74.22(8) . .
S7 Ag13 Ag3 134.86(7) . .
S5 Ag13 Ag3 108.33(7) . .
Ag1 Ag13 Ag3 60.93(3) . .
Ag2 Ag13 Ag3 57.21(3) . .
S4 Ag13 Ag16 97.74(8) . .
S7 Ag13 Ag16 143.79(7) . .
S5 Ag13 Ag16 53.47(6) . .
Ag1 Ag13 Ag16 58.30(3) . .
Ag2 Ag13 Ag16 103.97(3) . .
Ag3 Ag13 Ag16 54.93(2) . .
S14 Ag14 S8 131.76(9) . .
S14 Ag14 S12 105.50(9) . .
S8 Ag14 S12 118.51(9) . .
S14 Ag14 Ag5 104.50(7) . .
S8 Ag14 Ag5 115.10(7) . .
S12 Ag14 Ag5 57.18(7) . .
S14 Ag14 Ag2 145.45(7) . .
S8 Ag14 Ag2 54.15(6) . .
S12 Ag14 Ag2 92.73(7) . .
Ag5 Ag14 Ag2 61.23(3) . .
S14 Ag14 Ag6 89.52(6) . .
S8 Ag14 Ag6 88.44(7) . .
S12 Ag14 Ag6 115.90(7) . .
Ag5 Ag14 Ag6 58.72(2) . .
Ag2 Ag14 Ag6 55.97(2) . .
S14 Ag14 Ag15 49.98(6) . .
S8 Ag14 Ag15 144.26(7) . .
S12 Ag14 Ag15 86.87(6) . .
Ag5 Ag14 Ag15 55.79(2) . .
Ag2 Ag14 Ag15 103.56(3) . .
Ag6 Ag14 Ag15 56.63(2) . .
S15 Ag15 S11 123.77(9) 2_655 .
S15 Ag15 S14 109.43(9) 2_655 .
S11 Ag15 S14 109.08(9) . .
S15 Ag15 Ag5 140.00(7) 2_655 .
S11 Ag15 Ag5 64.20(7) . .
S14 Ag15 Ag5 102.19(7) . .
S15 Ag15 Ag10 83.11(6) 2_655 .
S11 Ag15 Ag10 86.97(7) . .
S14 Ag15 Ag10 146.10(7) . .
Ag5 Ag15 Ag10 57.24(2) . .
S15 Ag15 Ag6 98.04(6) 2_655 .
S11 Ag15 Ag6 122.23(7) . .
S14 Ag15 Ag6 88.54(6) . .
Ag5 Ag15 Ag6 58.32(2) . .
Ag10 Ag15 Ag6 58.05(2) . .
S15 Ag15 Ag14 141.51(6) 2_655 .
S11 Ag15 Ag14 94.69(7) . .
S14 Ag15 Ag14 48.66(6) . .
Ag5 Ag15 Ag14 54.75(2) . .
Ag10 Ag15 Ag14 101.94(3) . .
Ag6 Ag15 Ag14 56.59(2) . .
S2 Ag16 S3 122.39(9) . .
S2 Ag16 S5 96.98(9) . .
S3 Ag16 S5 116.30(9) . .
S2 Ag16 Ag3 144.44(7) . .
S3 Ag16 Ag3 56.20(7) . .
S5 Ag16 Ag3 115.60(7) . .
S2 Ag16 Ag1 109.62(7) . .
S3 Ag16 Ag1 118.98(7) . .
S5 Ag16 Ag1 83.96(6) . .
Ag3 Ag16 Ag1 63.07(3) . .
S2 Ag16 Ag9 86.82(7) . .
S3 Ag16 Ag9 91.41(7) . .
S5 Ag16 Ag9 142.99(7) . .
Ag3 Ag16 Ag9 58.76(3) . .
Ag1 Ag16 Ag9 60.40(3) . .
S2 Ag16 Ag13 146.43(7) . .
S3 Ag16 Ag13 88.53(7) . .
S5 Ag16 Ag13 53.80(6) . .
Ag3 Ag16 Ag13 61.88(3) . .
Ag1 Ag16 Ag13 56.83(3) . .
Ag9 Ag16 Ag13 106.79(3) . .
S2 Ag16 Ag17 51.76(7) . .
S3 Ag16 Ag17 146.92(7) . .
S5 Ag16 Ag17 96.58(7) . .
Ag3 Ag16 Ag17 107.65(3) . .
Ag1 Ag16 Ag17 58.22(3) . .
Ag9 Ag16 Ag17 57.52(3) . .
Ag13 Ag16 Ag17 109.81(3) . .
S9 Ag17 S2 117.84(10) . .
S9 Ag17 S6 127.56(9) . .
S2 Ag17 S6 110.84(9) . .
S9 Ag17 Ag1 121.49(8) . .
S2 Ag17 Ag1 107.23(7) . .
S6 Ag17 Ag1 55.30(6) . .
S9 Ag17 Ag9 84.83(7) . .
S2 Ag17 Ag9 87.99(7) . .
S6 Ag17 Ag9 115.95(7) . .
Ag1 Ag17 Ag9 60.66(3) . .
S9 Ag17 Ag4 66.11(7) . .
S2 Ag17 Ag4 143.61(7) . .
S6 Ag17 Ag4 86.17(7) . .
Ag1 Ag17 Ag4 55.51(2) . .
Ag9 Ag17 Ag4 55.71(2) . .
S9 Ag17 Ag16 141.13(7) . .
S2 Ag17 Ag16 51.08(7) . .
S6 Ag17 Ag16 85.41(7) . .
Ag1 Ag17 Ag16 56.49(3) . .
Ag9 Ag17 Ag16 59.78(3) . .
Ag4 Ag17 Ag16 101.36(3) . .
O1 C1 C2 107.4(10) . .
C3 C2 C1 113.3(12) . .
O2 C4 C5 109.5(11) . .
C4 C5 C6 111.5(13) . .
O3 C7 C8 109.7(17) . .
C7 C8 C9 103.7(19) . .
O4 C10 C11 114.1(15) . .
C10 C11 C12 117(2) . .
O5 C13 C14 108.4(12) . .
C13 C14 C15 114.6(15) . .
O6 C16 C17 109.7(11) . .
C18 C17 C16 113.9(15) . .
O7 C19 C20 107.9(11) . .
C19 C20 C21 114.0(13) . .
O8 C22 C23 111.2(17) . .
C22 C23 C24 91.2(18) . .
O9 C25 C26 109.2(10) . .
C25 C26 C27 113.2(10) . .
O10 C28 C29 108.8(10) . .
C28 C29 C30 112.4(12) . .
O11 C31 C32 108.4(13) . .
C33 C32 C31 106.6(17) . .
O12 C34 C35 111.1(15) . .
C34 C35 C36 109(2) . .
C38 C37 O13 114.5(11) . .
C37 C38 C39 112.5(15) . .
O14 C40 C41 110.7(11) . .
C40 C41 C42 116.8(13) . .
O15 C43 C44 111.6(10) . .
C43 C44 C45 116.1(11) . .
O16 C46 C47 106.9(9) . .
C46 C47 C48 111.6(10) . .
O17 C49 C50 109.9(9) . .
C51 C50 C49 116.6(12) . .
C1 O1 P1 119.5(7) . .
C4 O2 P1 122.0(7) . .
C7 O3 P2 118.2(13) . .
C10 O4 P2 124.6(10) . .
C13 O5 P3 119.9(8) . .
C16 O6 P3 122.2(7) . .
C19 O7 P4 120.7(8) . .
C22 O8 P4 128.7(12) . .
C25 O9 P5 120.1(7) . .
C28 O10 P5 120.1(7) . .
C31 O11 P6 121.9(7) . .
C34 O12 P6 119.3(11) . .
C37 O13 P7 125.6(7) . .
C40 O14 P7 119.1(7) . .
C43 O15 P8 127.5(7) . .
C46 O16 P8 122.3(6) . .
C49 O17 P9 119.6(6) . .
O2 P1 O1 100.8(4) . .
O2 P1 S1 109.1(3) . .
O1 P1 S1 110.5(3) . .
O2 P1 S2 108.9(3) . .
O1 P1 S2 107.2(3) . .
S1 P1 S2 118.74(18) . .
O4 P2 O3 100.8(7) . .
O4 P2 S4 112.3(5) . .
O3 P2 S4 107.6(5) . .
O4 P2 S3 108.1(4) . .
O3 P2 S3 108.2(5) . .
S4 P2 S3 118.43(19) . .
O6 P3 O5 106.2(4) . .
O6 P3 S5 111.0(3) . .
O5 P3 S5 104.0(3) . .
O6 P3 S6 102.8(3) . .
O5 P3 S6 110.7(3) . .
S5 P3 S6 121.33(17) . .
O8 P4 O7 102.1(6) . .
O8 P4 S7 107.7(5) . .
O7 P4 S7 113.5(3) . .
O8 P4 S8 111.0(4) . .
O7 P4 S8 102.7(3) . .
S7 P4 S8 118.63(18) . .
O9 P5 O10 96.0(4) . .
O9 P5 S10 110.8(3) . .
O10 P5 S10 111.4(3) . .
O9 P5 S9 112.3(3) . .
O10 P5 S9 108.7(3) . .
S10 P5 S9 115.87(17) . .
O11 P6 O12 102.2(5) . .
O11 P6 S11 110.3(3) . .
O12 P6 S11 107.8(4) . .
O11 P6 S12 107.5(3) . .
O12 P6 S12 111.6(4) . .
S11 P6 S12 116.49(17) . .
O13 P7 O14 102.4(4) . .
O13 P7 S14 105.9(3) . 2_655
O14 P7 S14 109.5(3) . 2_655
O13 P7 S13 111.5(3) . .
O14 P7 S13 108.0(3) . .
S14 P7 S13 118.40(16) 2_655 .
O15 P8 O16 106.5(4) . .
O15 P8 S15 105.8(3) . .
O16 P8 S15 110.5(3) . .
O15 P8 S16 111.2(3) . 2_655
O16 P8 S16 102.8(3) . 2_655
S15 P8 S16 119.32(15) . 2_655
O17 P9 O17 96.6(5) . 2_655
O17 P9 S17 112.2(3) . .
O17 P9 S17 110.2(3) 2_655 .
O17 P9 S17 110.2(3) . 2_655
O17 P9 S17 112.2(3) 2_655 2_655
S17 P9 S17 114.0(2) . 2_655
Ag3 Pt1 Ag2 63.60(2) . .
Ag3 Pt1 Ag9 64.76(2) . .
Ag2 Pt1 Ag9 119.83(3) . .
Ag3 Pt1 Ag1 66.92(2) . .
Ag2 Pt1 Ag1 65.93(2) . .
Ag9 Pt1 Ag1 67.03(2) . .
Ag3 Pt1 Ag11 116.72(2) . .
Ag2 Pt1 Ag11 113.60(3) . .
Ag9 Pt1 Ag11 115.78(3) . .
Ag1 Pt1 Ag11 175.95(2) . .
Ag3 Pt1 Ag8 66.14(2) . .
Ag2 Pt1 Ag8 117.70(3) . .
Ag9 Pt1 Ag8 62.99(2) . .
Ag1 Pt1 Ag8 121.78(3) . .
Ag11 Pt1 Ag8 62.17(2) . .
Ag3 Pt1 Ag6 116.31(3) . .
Ag2 Pt1 Ag6 62.16(2) . .
Ag9 Pt1 Ag6 177.75(3) . .
Ag1 Pt1 Ag6 115.16(3) . .
Ag11 Pt1 Ag6 62.01(2) . .
Ag8 Pt1 Ag6 115.39(3) . .
Ag3 Pt1 Ag4 117.30(3) . .
Ag2 Pt1 Ag4 119.73(3) . .
Ag9 Pt1 Ag4 63.20(2) . .
Ag1 Pt1 Ag4 62.32(2) . .
Ag11 Pt1 Ag4 115.83(3) . .
Ag8 Pt1 Ag4 114.66(3) . .
Ag6 Pt1 Ag4 117.06(3) . .
Ag3 Pt1 Ag10 179.74(3) . .
Ag2 Pt1 Ag10 116.34(3) . .
Ag9 Pt1 Ag10 115.42(3) . .
Ag1 Pt1 Ag10 113.31(2) . .
Ag11 Pt1 Ag10 63.043(18) . .
Ag8 Pt1 Ag10 113.75(3) . .
Ag6 Pt1 Ag10 63.50(2) . .
Ag4 Pt1 Ag10 62.96(2) . .
Ag3 Pt1 Ag5 118.77(3) . .
Ag2 Pt1 Ag5 66.35(2) . .
Ag9 Pt1 Ag5 118.08(3) . .
Ag1 Pt1 Ag5 61.91(2) . .
Ag11 Pt1 Ag5 114.09(2) . .
Ag8 Pt1 Ag5 175.08(3) . .
Ag6 Pt1 Ag5 63.39(2) . .
Ag4 Pt1 Ag5 63.44(2) . .
Ag10 Pt1 Ag5 61.34(2) . .
Ag3 Pt1 Ag12 118.45(3) . .
Ag2 Pt1 Ag12 176.49(3) . .
Ag9 Pt1 Ag12 63.47(2) . .
Ag1 Pt1 Ag12 117.32(3) . .
Ag11 Pt1 Ag12 63.06(3) . .
Ag8 Pt1 Ag12 62.16(2) . .
Ag6 Pt1 Ag12 114.51(3) . .
Ag4 Pt1 Ag12 62.36(2) . .
Ag10 Pt1 Ag12 61.60(2) . .
Ag5 Pt1 Ag12 113.60(2) . .
Ag3 Pt1 Ag7 61.48(2) . .
Ag2 Pt1 Ag7 63.84(2) . .
Ag9 Pt1 Ag7 113.29(3) . .
Ag1 Pt1 Ag7 119.21(3) . .
Ag11 Pt1 Ag7 62.92(2) . .
Ag8 Pt1 Ag7 61.07(2) . .
Ag6 Pt1 Ag7 66.35(2) . .
Ag4 Pt1 Ag7 175.72(3) . .
Ag10 Pt1 Ag7 118.26(2) . .
Ag5 Pt1 Ag7 120.84(3) . .
Ag12 Pt1 Ag7 114.21(3) . .
P1 S1 Ag9 108.24(14) . .
P1 S2 Ag16 103.38(14) . .
P1 S2 Ag17 100.12(14) . .
Ag16 S2 Ag17 77.17(8) . .
P2 S3 Ag3 97.50(14) . .
P2 S3 Ag16 105.01(14) . .
Ag3 S3 Ag16 67.15(7) . .
P2 S4 Ag13 104.39(16) . .
P3 S5 Ag16 105.63(14) . .
P3 S5 Ag13 104.34(13) . .
Ag16 S5 Ag13 72.72(7) . .
P3 S6 Ag17 109.11(14) . .
P3 S6 Ag1 100.54(13) . .
Ag17 S6 Ag1 70.25(7) . .
P4 S7 Ag13 103.24(14) . .
P4 S8 Ag14 99.66(14) . .
P4 S8 Ag2 96.65(13) . .
Ag14 S8 Ag2 72.27(7) . .
P5 S9 Ag17 106.67(14) . .
P5 S10 Ag4 91.02(13) . .
P6 S11 Ag15 102.70(14) . .
P6 S11 Ag5 80.72(12) . .
Ag15 S11 Ag5 64.83(6) . .
P6 S12 Ag14 106.55(14) . .
P6 S12 Ag5 87.76(12) . .
Ag14 S12 Ag5 67.52(7) . .
P7 S13 Ag6 110.93(13) . 2_655
P7 S13 Ag7 115.00(13) . .
Ag6 S13 Ag7 68.34(7) 2_655 .
P7 S14 Ag14 103.42(13) 2_655 .
P7 S14 Ag15 95.87(12) 2_655 .
Ag14 S14 Ag15 81.36(8) . .
P8 S15 Ag15 99.34(12) . 2_655
P8 S15 Ag7 113.83(12) . .
Ag15 S15 Ag7 89.26(8) 2_655 .
P8 S16 Ag8 97.53(12) 2_655 2_655
P8 S16 Ag10 98.55(12) 2_655 .
Ag8 S16 Ag10 76.14(7) 2_655 .
P9 S17 Ag12 94.95(12) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 S6 2.591(3) .
Ag1 Pt1 2.7402(8) .
Ag1 Ag5 2.8403(11) .
Ag1 Ag4 2.8463(11) .
Ag1 Ag13 2.8616(11) .
Ag1 Ag16 2.9088(11) .
Ag1 Ag17 2.9657(11) .
Ag1 Ag2 2.9695(11) .
Ag1 Ag3 3.0068(10) .
Ag1 Ag9 3.0171(11) .
Ag2 S8 2.552(3) .
Ag2 Pt1 2.7168(8) .
Ag2 Ag6 2.8281(10) .
Ag2 Ag3 2.8614(11) .
Ag2 Ag13 2.9111(11) .
Ag2 Ag7 2.9427(11) .
Ag2 Ag14 2.9993(11) .
Ag2 Ag5 3.0091(11) .
Ag3 S3 2.560(3) .
Ag3 Pt1 2.7132(8) .
Ag3 Ag16 2.8387(11) .
Ag3 Ag7 2.8431(11) .
Ag3 Ag9 2.9121(11) .
Ag3 Ag8 2.9788(11) .
Ag3 Ag13 3.0591(11) .
Ag4 S10 2.486(3) .
Ag4 Pt1 2.7608(8) .
Ag4 Ag9 2.8742(11) .
Ag4 Ag12 2.8822(11) .
Ag4 Ag10 2.8875(11) .
Ag4 Ag5 2.9138(11) .
Ag4 Ag17 3.1379(11) .
Ag5 S12 2.644(3) .
Ag5 Pt1 2.7813(8) .
Ag5 Ag10 2.8308(10) .
Ag5 Ag14 2.9072(11) .
Ag5 Ag6 2.9117(10) .
Ag5 S11 2.929(3) .
Ag5 Ag15 2.9441(11) .
Ag6 S13 2.540(3) 2_655
Ag6 Pt1 2.7607(8) .
Ag6 Ag11 2.8357(10) .
Ag6 Ag10 2.9093(10) .
Ag6 Ag7 2.9201(11) 2_655
Ag6 Ag14 3.0278(11) .
Ag6 Ag15 3.0294(11) .
Ag6 Ag7 3.0680(11) .
Ag7 S13 2.656(3) .
Ag7 Ag8 2.8417(11) .
Ag7 Pt1 2.8448(8) .
Ag7 S15 2.894(3) .
Ag7 Ag11 2.9181(9) .
Ag7 Ag6 2.9201(11) 2_655
Ag8 S16 2.499(2) 2_655
Ag8 Pt1 2.7458(8) .
Ag8 Ag11 2.8344(9) .
Ag8 Ag9 2.8579(11) .
Ag8 Ag12 2.8663(11) .
Ag8 Ag10 3.1038(11) 2_655
Ag9 S1 2.483(3) .
Ag9 Pt1 2.7243(8) .
Ag9 Ag12 2.9096(11) .
Ag9 Ag17 3.0085(11) .
Ag9 Ag16 3.0818(11) .
Ag10 S16 2.535(3) .
Ag10 Pt1 2.7683(8) .
Ag10 Ag12 2.8543(10) .
Ag10 Ag11 2.8819(7) .
Ag10 Ag15 2.9656(11) .
Ag10 Ag8 3.1037(11) 2_655
Ag11 Pt1 2.7439(4) .
Ag11 Pt1 2.7439(4) 2_655
Ag11 Ag8 2.8345(8) 2_655
Ag11 Ag6 2.8357(10) 2_655
Ag11 Ag10 2.8820(7) 2_655
Ag11 Ag12 2.9024(11) 2_655
Ag11 Ag12 2.9024(11) .
Ag11 Ag7 2.9180(9) 2_655
Ag12 S17 2.505(3) .
Ag12 Pt1 2.8056(8) .
Ag12 Ag12 3.2192(15) 2_655
Ag13 S4 2.514(3) .
Ag13 S7 2.530(3) .
Ag13 S5 2.616(3) .
Ag13 Ag16 3.0953(12) .
Ag14 S14 2.532(3) .
Ag14 S8 2.534(3) .
Ag14 S12 2.587(3) .
Ag14 Ag15 3.3335(11) .
Ag15 S15 2.526(3) 2_655
Ag15 S11 2.527(3) .
Ag15 S14 2.582(3) .
Ag16 S2 2.529(3) .
Ag16 S3 2.573(3) .
Ag16 S5 2.605(3) .
Ag16 Ag17 3.1694(12) .
Ag17 S9 2.477(3) .
Ag17 S2 2.553(3) .
Ag17 S6 2.564(3) .
C1 O1 1.462(14) .
C1 C2 1.527(17) .
C2 C3 1.49(2) .
C4 O2 1.441(14) .
C4 C5 1.484(18) .
C5 C6 1.511(19) .
C7 O3 1.426(10) .
C7 C8 1.488(10) .
C8 C9 1.523(10) .
C10 O4 1.411(9) .
C10 C11 1.498(10) .
C11 C12 1.500(10) .
C13 O5 1.457(15) .
C13 C14 1.49(2) .
C14 C15 1.50(3) .
C16 O6 1.444(15) .
C16 C17 1.477(18) .
C17 C18 1.47(2) .
C19 O7 1.464(14) .
C19 C20 1.484(19) .
C20 C21 1.50(2) .
C22 O8 1.409(9) .
C22 C23 1.505(10) .
C23 C24 1.514(10) .
C25 O9 1.453(13) .
C25 C26 1.498(16) .
C26 C27 1.503(18) .
C28 O10 1.458(13) .
C28 C29 1.494(17) .
C29 C30 1.51(2) .
C31 O11 1.452(16) .
C31 C32 1.54(2) .
C32 C33 1.42(2) .
C34 O12 1.430(9) .
C34 C35 1.498(10) .
C35 C36 1.528(10) .
C37 C38 1.450(18) .
C37 O13 1.459(12) .
C38 C39 1.52(2) .
C40 O14 1.439(8) .
C40 C41 1.497(9) .
C41 C42 1.508(9) .
C43 O15 1.474(13) .
C43 C44 1.486(16) .
C44 C45 1.507(18) .
C46 O16 1.447(12) .
C46 C47 1.502(15) .
C47 C48 1.516(16) .
C49 O17 1.447(12) .
C49 C50 1.497(16) .
C50 C51 1.47(2) .
O1 P1 1.586(7) .
O2 P1 1.574(8) .
O3 P2 1.640(13) .
O4 P2 1.540(10) .
O5 P3 1.593(8) .
O6 P3 1.572(8) .
O7 P4 1.584(9) .
O8 P4 1.574(9) .
O9 P5 1.577(8) .
O10 P5 1.582(8) .
O11 P6 1.574(8) .
O12 P6 1.580(9) .
O13 P7 1.553(7) .
O14 P7 1.579(7) .
O15 P8 1.571(7) .
O16 P8 1.582(7) .
O17 P9 1.582(7) .
P1 S1 1.973(4) .
P1 S2 2.015(4) .
P2 S4 1.963(4) .
P2 S3 2.011(4) .
P3 S5 1.999(4) .
P3 S6 2.004(4) .
P4 S7 1.972(4) .
P4 S8 2.014(4) .
P5 S10 1.982(4) .
P5 S9 2.003(4) .
P6 S11 1.983(4) .
P6 S12 2.016(4) .
P7 S14 2.003(4) 2_655
P7 S13 2.004(3) .
P8 S15 2.000(4) .
P8 S16 2.005(4) 2_655
P9 O17 1.582(7) 2_655
P9 S17 1.988(3) .
P9 S17 1.988(3) 2_655
S13 Ag6 2.540(3) 2_655
S14 P7 2.003(4) 2_655
S15 Ag15 2.526(3) 2_655
S16 P8 2.006(4) 2_655
S16 Ag8 2.499(2) 2_655
