#------------------------------------------------------------------------------
#$Date: 2019-11-25 08:48:01 +0200 (Mon, 25 Nov 2019) $
#$Revision: 240558 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/12/99/4129918.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4129918
loop_
_publ_author_name
'Chorazy, Szymon'
'Stanek, Jan J.'
'Nogaś, Wojciech'
'Majcher, Anna M.'
'Rams, Michał'
'Kozieł, Marcin'
'Juszyńska-Gałązka, Ewa'
'Nakabayashi, Koji'
'Ohkoshi, Shin-ichi'
'Sieklucka, Barbara'
'Podgajny, Robert'
_publ_section_title
;
 Tuning of Charge Transfer Assisted Phase Transition and Slow Magnetic
 Relaxation Functionalities in {Fe(9-x)Co(x)[W(CN)8]6} (x = 0-9) Molecular
 Solid Solution.
;
_journal_issue                   5
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              1635
_journal_page_last               1646
_journal_paper_doi               10.1021/jacs.5b11924
_journal_volume                  138
_journal_year                    2016
_chemical_formula_moiety         'C84 H60 Co4 Fe5 N48 O36 W6'
_chemical_formula_sum            'C84 H60 Co4 Fe5 N48 O36 W6'
_chemical_formula_weight         3935.87
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_conform_dict_location     ftp://ftp.iucr.org/pub/cif_core.dic
_audit_conform_dict_name         cif_core.dic
_audit_conform_dict_version      2.4.3
_audit_creation_date             2015-01-26T18:50:30-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                90
_cell_angle_beta                 114.3980(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   28.599(2)
_cell_length_b                   18.6690(15)
_cell_length_c                   32.103(2)
_cell_measurement_reflns_used    56982
_cell_measurement_temperature    130(2)
_cell_measurement_theta_max      27.479
_cell_measurement_theta_min      3.01
_cell_measurement_wavelength     0.71075
_cell_volume                     15609.6(19)
_computing_molecular_graphics    'Ortep for Windows (Farrugia, 2012)'
_computing_publication_material  'WinGX publication routines (Farrugia, 2012)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      130(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Rigaku R-AXIS RAPID'
_diffrn_measurement_method       ω
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71075
_diffrn_reflns_av_R_equivalents  0.131
_diffrn_reflns_av_unetI/netI     0.1494
_diffrn_reflns_Laue_measured_fraction_full 0.993
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_limit_h_max       37
_diffrn_reflns_limit_h_min       -37
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       41
_diffrn_reflns_limit_l_min       -41
_diffrn_reflns_number            56982
_diffrn_reflns_point_group_measured_fraction_full 0.993
_diffrn_reflns_point_group_measured_fraction_max 0.992
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.479
_diffrn_reflns_theta_min         3.01
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    5.335
_exptl_absorpt_correction_T_max  0.556
_exptl_absorpt_correction_T_min  0.499
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'ABSCOR (Rigaku, 1995)'
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.675
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             7480
_exptl_crystal_size_max          0.19
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.11
_refine_diff_density_max         1.407
_refine_diff_density_min         -1.943
_refine_diff_density_rms         0.193
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.058
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     840
_refine_ls_number_reflns         17752
_refine_ls_number_restraints     85
_refine_ls_restrained_S_all      1.056
_refine_ls_R_factor_all          0.1846
_refine_ls_R_factor_gt           0.0974
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0657P)²+233.2657P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1809
_refine_ls_wR_factor_ref         0.2174
_reflns_Friedel_coverage         0
_reflns_number_gt                9286
_reflns_number_total             17752
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ja5b11924_si_003.cif
_cod_data_source_block           Co4Fe5W6_LT
_cod_original_cell_volume        15610(2)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4129918
_shelx_estimated_absorpt_t_min   0.43
_shelx_estimated_absorpt_t_max   0.591
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
W1 W 0.42003(2) 0.83607(4) 0.11979(2) 0.0533(2) Uani 1 1 d . . . . .
W2 W 0.67571(2) 0.65920(4) 0.23652(2) 0.04702(19) Uani 1 1 d . . . . .
W3 W 0.44092(2) 0.44429(4) 0.12561(2) 0.04736(19) Uani 1 1 d . . . . .
Co1 Co 0.5 0.64603(16) 0.25 0.0355(6) Uani 1 2 d S T P . .
Co2 Co 0.60657(7) 0.92342(14) 0.23313(8) 0.0605(7) Uani 0.75 1 d . . P . .
Fe2 Fe 0.60657(7) 0.92342(14) 0.23313(8) 0.0605(7) Uani 0.25 1 d . . P . .
Fe5 Fe 0.28404(7) 0.62428(15) 0.08779(7) 0.0544(7) Uani 1 1 d . . . . .
Fe3 Fe 0.63001(7) 0.38414(14) 0.24786(7) 0.0465(6) Uani 1 1 d . . . . .
Co4 Co 0.52814(8) 0.65267(14) 0.06799(7) 0.0572(6) Uani 0.75 1 d . . P . .
Fe4 Fe 0.52814(8) 0.65267(14) 0.06799(7) 0.0572(6) Uani 0.25 1 d . . P . .
C11 C 0.4542(5) 0.7557(9) 0.1742(5) 0.048(4) Uani 1 1 d . . . . .
N11 N 0.4743(4) 0.7178(6) 0.2037(4) 0.034(3) Uani 1 1 d . . . . .
C12 C 0.4092(5) 0.8770(11) 0.1790(6) 0.061(5) Uani 1 1 d . . . . .
N12 N 0.4053(5) 0.8987(8) 0.2111(5) 0.060(4) Uani 1 1 d . . . . .
C13 C 0.4928(6) 0.8751(10) 0.1632(5) 0.053(4) Uani 1 1 d . . . . .
N13 N 0.5336(5) 0.8942(8) 0.1890(4) 0.058(4) Uani 1 1 d . . . . .
C14 C 0.4654(5) 0.7692(9) 0.0979(4) 0.042(4) Uani 1 1 d . . . . .
N14 N 0.4903(4) 0.7290(8) 0.0876(4) 0.051(3) Uani 1 1 d . . . . .
C15 C 0.3630(6) 0.7537(11) 0.1073(5) 0.059(5) Uani 1 1 d . . . . .
N15 N 0.3324(5) 0.7108(9) 0.0990(5) 0.068(4) Uani 1 1 d . . . . .
C16 C 0.3510(11) 0.8958(19) 0.0951(8) 0.142(13) Uani 1 1 d . . . . .
N16 N 0.3103(11) 0.923(2) 0.0834(8) 0.214(18) Uani 1 1 d . . . . .
C17 C 0.3827(7) 0.8274(11) 0.0455(7) 0.068(5) Uani 1 1 d . . . . .
N17 N 0.3614(6) 0.8238(9) 0.0069(5) 0.078(5) Uani 1 1 d . . . . .
C18A C 0.4353(10) 0.9326(17) 0.0970(7) 0.128(11) Uani 1 1 d . . . . .
N18A N 0.4447(11) 0.9833(18) 0.0832(8) 0.222(18) Uani 1 1 d . . . . .
C21 C 0.6032(5) 0.6541(9) 0.2441(5) 0.049(4) Uani 1 1 d . . . . .
N21 N 0.5647(4) 0.6483(6) 0.2465(4) 0.038(3) Uani 1 1 d . . . . .
C22 C 0.6486(5) 0.7629(11) 0.2330(5) 0.056(5) Uani 1 1 d . . . . .
N22 N 0.6341(5) 0.8217(10) 0.2315(5) 0.066(4) Uani 1 1 d . . . . .
C23 C 0.6558(5) 0.5502(12) 0.2363(5) 0.055(5) Uani 1 1 d . . . . .
N23 N 0.6463(5) 0.4894(9) 0.2393(4) 0.054(4) Uani 1 1 d . . . . .
C24 C 0.6181(6) 0.6484(9) 0.1675(6) 0.054(4) Uani 1 1 d . . . . .
N24 N 0.5868(5) 0.6456(8) 0.1314(4) 0.060(4) Uani 1 1 d . . . . .
C25 C 0.6963(4) 0.6393(8) 0.3061(6) 0.046(4) Uani 1 1 d . . . . .
N25 N 0.7055(4) 0.6289(8) 0.3452(4) 0.056(4) Uani 1 1 d . . . . .
C26 C 0.7382(6) 0.5968(12) 0.2400(7) 0.080(6) Uani 1 1 d . . . . .
N26 N 0.7737(6) 0.5626(11) 0.2423(7) 0.115(7) Uani 1 1 d . . . . .
C27 C 0.7025(6) 0.7073(17) 0.1899(7) 0.116(10) Uani 1 1 d . . . A 1
N27A N 0.7194(13) 0.753(3) 0.1698(13) 0.085(12) Uani 0.5 1 d . U P A 1
N27B N 0.7165(17) 0.718(3) 0.1591(14) 0.092(15) Uiso 0.5 1 d . . P B 2
C28 C 0.7416(6) 0.7244(11) 0.2763(6) 0.063(5) Uani 1 1 d . . . . .
N28 N 0.7756(5) 0.7617(9) 0.2949(5) 0.072(4) Uani 1 1 d . . . . .
C31 C 0.4661(5) 0.5291(9) 0.1776(5) 0.042(4) Uani 1 1 d . . . . .
N31 N 0.4767(4) 0.5738(7) 0.2043(4) 0.035(3) Uani 1 1 d . . . . .
C32 C 0.5130(6) 0.4142(10) 0.1749(4) 0.050(4) Uani 1 1 d . . . . .
N32 N 0.5556(5) 0.3959(7) 0.2014(4) 0.049(3) Uani 1 1 d . . . . .
C33 C 0.4089(5) 0.4181(11) 0.1723(5) 0.063(5) Uani 1 1 d . . . . .
N33 N 0.3918(4) 0.4023(8) 0.1999(4) 0.054(3) Uani 1 1 d . . . . .
C34 C 0.4712(6) 0.5265(12) 0.0981(4) 0.063(6) Uani 1 1 d . . . . .
N34 N 0.4883(5) 0.5717(9) 0.0840(4) 0.060(4) Uani 1 1 d . . . . .
C35 C 0.3773(6) 0.5146(10) 0.1082(4) 0.054(4) Uani 1 1 d . . . . .
N35 N 0.3437(5) 0.5559(9) 0.1010(4) 0.059(4) Uani 1 1 d . . . . .
C36A C 0.4366(14) 0.335(2) 0.1285(12) 0.073(10) Uani 0.6 1 d . U P . .
N36A N 0.4355(12) 0.273(2) 0.1385(11) 0.095(9) Uani 0.6 1 d . U P . .
C36B C 0.414(2) 0.344(4) 0.112(2) 0.079(17) Uiso 0.4 1 d . . P . .
N36B N 0.4037(17) 0.283(3) 0.1107(16) 0.092(13) Uiso 0.4 1 d . . P . .
C37A C 0.3787(11) 0.4164(18) 0.0656(9) 0.060(7) Uani 0.6 1 d . U P . .
N37A N 0.3481(12) 0.403(2) 0.0281(11) 0.110(10) Uani 0.6 1 d . U P . .
C37B C 0.3998(18) 0.437(3) 0.0552(16) 0.071(13) Uiso 0.4 1 d . . P . .
N37B N 0.375(2) 0.440(3) 0.0177(14) 0.131(19) Uiso 0.4 1 d D . P . .
C38 C 0.4779(6) 0.3954(12) 0.0888(4) 0.066(6) Uani 1 1 d . . . . .
N38 N 0.4996(6) 0.3701(10) 0.0674(5) 0.088(5) Uani 1 1 d . . . . .
O41 O 0.4740(4) 0.6562(7) 0.0014(3) 0.070(4) Uani 1 1 d . . . C 1
C42A C 0.4266(11) 0.694(2) -0.0148(10) 0.052(8) Uani 0.5 1 d . U P C 1
H42A H 0.4075 0.6808 0.0033 0.078 Uiso 0.5 1 calc R U P C 1
H42B H 0.4063 0.6828 -0.047 0.078 Uiso 0.5 1 calc R U P C 1
H42C H 0.4335 0.746 -0.0116 0.078 Uiso 0.5 1 calc R U P C 1
O43 O 0.5655(4) 0.7303(8) 0.0471(4) 0.078(4) Uani 1 1 d . . . D 1
C44 C 0.6189(18) 0.744(3) 0.0604(16) 0.30(3) Uani 1 1 d . U . D 1
H44A H 0.6229 0.7858 0.0435 0.451 Uiso 0.5 1 calc R U P D 1
H44B H 0.6353 0.7544 0.0933 0.451 Uiso 0.5 1 calc R U P D 1
H44C H 0.6351 0.7023 0.0536 0.451 Uiso 0.5 1 calc R U P D 1
H44D H 0.6394 0.7092 0.0835 0.451 Uiso 0.5 1 calc R U P D 1
H44E H 0.6269 0.7406 0.0336 0.451 Uiso 0.5 1 calc R U P D 1
H44F H 0.6271 0.7926 0.0733 0.451 Uiso 0.5 1 calc R U P D 1
O45 O 0.5665(4) 0.5808(8) 0.0437(4) 0.072(4) Uani 1 1 d . . . E 1
C46A C 0.5559(14) 0.515(2) 0.0315(13) 0.064(10) Uani 0.5 1 d . . P E 1
H46A H 0.5707 0.4843 0.0584 0.096 Uiso 0.5 1 calc R U P E 1
H46B H 0.5704 0.5026 0.0096 0.096 Uiso 0.5 1 calc R U P E 1
H46C H 0.5186 0.5091 0.0171 0.096 Uiso 0.5 1 calc R U P E 1
O51 O 0.2690(4) 0.6203(8) 0.0187(4) 0.080(4) Uani 1 1 d . . . F 1
C52A C 0.2698(17) 0.673(3) -0.0070(16) 0.106(15) Uani 0.5 1 d . U P F 1
H52A H 0.2567 0.7166 0.0019 0.16 Uiso 0.5 1 calc R U P F 1
H52B H 0.2481 0.6619 -0.0391 0.16 Uiso 0.5 1 calc R U P F 1
H52C H 0.3051 0.6817 -0.0034 0.16 Uiso 0.5 1 calc R U P F 1
O53 O 0.2216(4) 0.6919(8) 0.0705(3) 0.072(4) Uani 1 1 d . . . G 1
C54 C 0.2180(7) 0.7552(13) 0.0962(6) 0.088(7) Uani 1 1 d . . . G 1
H54A H 0.1842 0.7775 0.0804 0.132 Uiso 0.5 1 calc R U P G 1
H54B H 0.2226 0.7407 0.127 0.132 Uiso 0.5 1 calc R U P G 1
H54C H 0.2448 0.7897 0.0984 0.132 Uiso 0.5 1 calc R U P G 1
H54D H 0.2502 0.7611 0.1235 0.132 Uiso 0.5 1 calc R U P G 1
H54E H 0.2118 0.7979 0.0769 0.132 Uiso 0.5 1 calc R U P G 1
H54F H 0.1896 0.7489 0.1055 0.132 Uiso 0.5 1 calc R U P G 1
O55 O 0.2344(4) 0.5384(7) 0.0730(4) 0.076(4) Uani 1 1 d D . . H 1
C56A C 0.2480(17) 0.475(3) 0.1078(14) 0.144(17) Uani 0.6 1 d . U P H 1
H56A H 0.2588 0.4338 0.0953 0.216 Uiso 1 1 calc R U . H 1
H56B H 0.2178 0.4628 0.1133 0.216 Uiso 1 1 calc R U . H 1
H56C H 0.2761 0.4899 0.1366 0.216 Uiso 1 1 calc R U . H 1
O61 O 0.6207(4) 0.9568(9) 0.1782(5) 0.088(4) Uani 1 1 d . . . I 1
C62 C 0.6076(8) 0.9119(16) 0.1376(7) 0.112(9) Uani 1 1 d . . . I 1
H62A H 0.6379 0.8843 0.1402 0.169 Uiso 1 1 calc R U . I 1
H62B H 0.5964 0.9423 0.1103 0.169 Uiso 1 1 calc R U . I 1
H62C H 0.5799 0.879 0.135 0.169 Uiso 1 1 calc R U . I 1
O63 O 0.6776(4) 0.9587(8) 0.2745(4) 0.082(4) Uani 1 1 d . . . J 1
C64 C 0.7115(7) 0.9255(14) 0.3134(6) 0.097(8) Uani 1 1 d . . . J 1
H64A H 0.7419 0.9559 0.3283 0.146 Uiso 1 1 calc R U . J 1
H64B H 0.7219 0.8794 0.3054 0.146 Uiso 1 1 calc R U . J 1
H64C H 0.695 0.9177 0.3344 0.146 Uiso 1 1 calc R U . J 1
O65 O 0.5849(5) 1.0283(7) 0.2377(5) 0.091(4) Uani 1 1 d . . . K 1
C66 C 0.5333(11) 1.0506(19) 0.2061(11) 0.172(13) Uani 1 1 d . U . K 1
H66A H 0.5123 1.0081 0.1927 0.258 Uiso 1 1 calc R U . K 1
H66B H 0.5355 1.0802 0.1818 0.258 Uiso 1 1 calc R U . K 1
H66C H 0.5174 1.0784 0.2228 0.258 Uiso 1 1 calc R U . K 1
O71 O 0.7067(4) 0.3694(7) 0.2944(4) 0.068(3) Uani 1 1 d . . . L 1
C72 C 0.7488(7) 0.4028(14) 0.2880(8) 0.106(7) Uani 1 1 d . U . L 1
H72A H 0.742 0.402 0.2555 0.16 Uiso 1 1 calc R U . L 1
H72B H 0.7806 0.3765 0.3055 0.16 Uiso 1 1 calc R U . L 1
H72C H 0.7525 0.4525 0.2987 0.16 Uiso 1 1 calc R U . L 1
O73 O 0.6515(4) 0.3564(7) 0.1955(4) 0.068(4) Uani 1 1 d . . . M 1
C74 C 0.6347(8) 0.3937(15) 0.1521(6) 0.111(10) Uani 1 1 d . . . M 1
H74A H 0.5974 0.3999 0.1392 0.166 Uiso 1 1 calc R U . M 1
H74B H 0.6441 0.3656 0.1309 0.166 Uiso 1 1 calc R U . M 1
H74C H 0.6514 0.4407 0.1569 0.166 Uiso 1 1 calc R U . M 1
O75 O 0.6213(5) 0.2776(8) 0.2568(4) 0.078(4) Uani 1 1 d . . . N 1
C76A C 0.6360(19) 0.222(3) 0.2526(18) 0.28(3) Uani 1 1 d . U . N 1
H76A H 0.6184 0.1854 0.2624 0.421 Uiso 0.25 1 calc R U P N 1
H76B H 0.6292 0.2148 0.2204 0.421 Uiso 0.25 1 calc R U P N 1
H76C H 0.6731 0.2195 0.2713 0.421 Uiso 0.25 1 calc R U P N 1
H76D H 0.662 0.2277 0.2403 0.421 Uiso 0.25 1 calc R U P N 1
H76E H 0.6513 0.1983 0.2824 0.421 Uiso 0.25 1 calc R U P N 1
H76F H 0.6074 0.1936 0.2314 0.421 Uiso 0.25 1 calc R U P N 1
C42B C 0.4164(14) 0.656(2) -0.0143(13) 0.062(10) Uiso 0.5 1 d . . P O 2
C46B C 0.587(2) 0.509(4) 0.0652(19) 0.122(19) Uiso 0.5 1 d . . P P 2
C52B C 0.3126(19) 0.608(3) -0.0008(16) 0.120(17) Uiso 0.5 1 d . . P Q 2
C56B C 0.186(2) 0.538(4) 0.078(2) 0.110(19) Uiso 0.4 1 d . . P R 2
C1 C 0.1474(18) 0.617(3) 0.137(2) 0.23(3) Uiso 0.7 1 d D . P . .
O1 O 0.1044(12) 0.580(2) 0.1389(10) 0.170(11) Uiso 0.7 1 d D . P . .
C2B C 0.332(2) 0.076(9) 0.152(4) 0.22(6) Uiso 0.3 1 d D . P . .
C2A C 0.3939(18) 0.071(3) 0.1453(13) 0.172(18) Uiso 0.7 1 d D . P . .
O2 O 0.3836(12) 0.0882(19) 0.1837(10) 0.242(12) Uiso 1 1 d D . . . .
C3 C 0.2891(19) 0.438(3) -0.1026(17) 0.16(2) Uiso 0.6 1 d D . P . .
O3 O 0.3322(18) 0.399(3) -0.0707(13) 0.26(2) Uiso 0.6 1 d D . P . .
C4A C 0.287(2) 0.313(4) 0.0964(18) 0.24(3) Uiso 0.7 1 d D . P S 1
O4A O 0.2618(10) 0.3122(17) 0.1269(9) 0.149(10) Uiso 0.7 1 d D . P S 1
C4B C 0.3074(17) 0.255(3) 0.1169(15) 0.052(13) Uiso 0.3 1 d D . P T 2
O4B O 0.343(2) 0.219(3) 0.1568(17) 0.14(2) Uiso 0.3 1 d D . P T 2
C5A C -0.028(2) 0.660(3) 0.0891(18) 0.20(2) Uiso 0.7 1 d D . P . .
O5 O -0.0019(15) 0.604(3) 0.0763(13) 0.228(16) Uiso 0.7 1 d D . P . .
C6 C 0.206(2) 0.441(4) -0.0250(19) 0.23(3) Uiso 0.6 1 d D . P U 1
O6A O 0.244(2) 0.432(3) 0.0203(18) 0.16(2) Uiso 0.3 1 d D . P U 1
O6B O 0.179(2) 0.477(4) -0.0016(19) 0.14(2) Uiso 0.3 1 d D . P V 2
O7 O 0.0180(14) 0.342(2) 0.0013(12) 0.258(16) Uiso 0.9 1 d D . P . .
C7 C -0.014(3) 0.397(3) 0.006(2) 0.35(4) Uiso 0.9 1 d D . P . .
O8 O 0.5 0.260(3) 0.25 0.247(18) Uiso 1 2 d DS . P . .
C8 C 0.5455(12) 0.220(2) 0.2749(12) 0.080(11) Uiso 0.5 1 d D . P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.849 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C18A W1 C13 68.6(7) . .
C18A W1 C16 73.0(13) . .
C13 W1 C16 125.6(11) . .
C18A W1 C14 98.6(10) . .
C13 W1 C14 81.3(6) . .
C16 W1 C14 142.3(7) . .
C18A W1 C15 144.5(7) . .
C13 W1 C15 146.9(6) . .
C16 W1 C15 77.8(11) . .
C14 W1 C15 92.2(6) . .
C18A W1 C17 75.9(8) . .
C13 W1 C17 130.9(6) . .
C16 W1 C17 70.7(8) . .
C14 W1 C17 71.5(6) . .
C15 W1 C17 75.7(6) . .
C18A W1 C12 97.5(10) . .
C13 W1 C12 76.1(6) . .
C16 W1 C12 72.3(7) . .
C14 W1 C12 145.1(5) . .
C15 W1 C12 92.4(6) . .
C17 W1 C12 142.8(6) . .
C18A W1 C11 142.1(7) . .
C13 W1 C11 73.5(6) . .
C16 W1 C11 134.1(8) . .
C14 W1 C11 74.4(5) . .
C15 W1 C11 73.4(5) . .
C17 W1 C11 132.4(6) . .
C12 W1 C11 74.0(6) . .
C22 W2 C25 99.1(6) . .
C22 W2 C26 144.5(6) . .
C25 W2 C26 89.2(6) . .
C22 W2 C23 143.7(5) . .
C25 W2 C23 77.8(6) . .
C26 W2 C23 71.8(6) . .
C22 W2 C27 78.7(9) . .
C25 W2 C27 142.8(6) . .
C26 W2 C27 74.2(8) . .
C23 W2 C27 125.2(9) . .
C22 W2 C24 85.5(6) . .
C25 W2 C24 146.9(5) . .
C26 W2 C24 106.1(7) . .
C23 W2 C24 79.4(6) . .
C27 W2 C24 70.3(7) . .
C22 W2 C28 73.8(6) . .
C25 W2 C28 71.2(6) . .
C26 W2 C28 76.4(7) . .
C23 W2 C28 135.4(6) . .
C27 W2 C28 72.5(8) . .
C24 W2 C28 140.3(6) . .
C22 W2 C21 72.3(6) . .
C25 W2 C21 74.6(5) . .
C26 W2 C21 142.7(7) . .
C23 W2 C21 72.0(6) . .
C27 W2 C21 136.5(6) . .
C24 W2 C21 75.7(5) . .
C28 W2 C21 126.5(6) . .
C36B W3 C36A 19.0(17) . .
C36B W3 C37B 73(2) . .
C36A W3 C37B 88.1(19) . .
C36B W3 C37A 57.3(19) . .
C36A W3 C37A 75.4(14) . .
C37B W3 C37A 24.7(13) . .
C36B W3 C32 94.9(18) . .
C36A W3 C32 76.0(12) . .
C37B W3 C32 138.1(14) . .
C37A W3 C32 146.4(10) . .
C36B W3 C38 73.5(16) . .
C36A W3 C38 69.2(11) . .
C37B W3 C38 63.2(14) . .
C37A W3 C38 78.8(8) . .
C32 W3 C38 74.9(5) . .
C36B W3 C33 71.9(16) . .
C36A W3 C33 71.7(11) . .
C37B W3 C33 122.7(14) . .
C37A W3 C33 98.3(9) . .
C32 W3 C33 89.0(5) . .
C38 W3 C33 140.2(8) . .
C36B W3 C35 107.8(17) . .
C36A W3 C35 124.6(11) . .
C37B W3 C35 73.4(14) . .
C37A W3 C35 66.3(9) . .
C32 W3 C35 146.6(6) . .
C38 W3 C35 134.4(6) . .
C33 W3 C35 75.7(6) . .
C36B W3 C34 140.8(16) . .
C36A W3 C34 141.3(10) . .
C37B W3 C34 74.9(15) . .
C37A W3 C34 97.8(10) . .
C32 W3 C34 93.7(6) . .
C38 W3 C34 72.1(7) . .
C33 W3 C34 146.4(7) . .
C35 W3 C34 84.1(6) . .
C36B W3 C31 144.3(16) . .
C36A W3 C31 133.8(11) . .
C37B W3 C31 137.2(16) . .
C37A W3 C31 140.5(9) . .
C32 W3 C31 73.0(5) . .
C38 W3 C31 131.3(5) . .
C33 W3 C31 74.4(6) . .
C35 W3 C31 74.3(5) . .
C34 W3 C31 74.5(6) . .
N31 Co1 N31 89.6(7) . 2_655
N31 Co1 N21 91.3(4) . 2_655
N31 Co1 N21 90.5(5) 2_655 2_655
N31 Co1 N21 90.5(5) . .
N31 Co1 N21 91.3(4) 2_655 .
N21 Co1 N21 177.4(7) 2_655 .
N31 Co1 N11 178.1(4) . 2_655
N31 Co1 N11 89.8(5) 2_655 2_655
N21 Co1 N11 90.5(4) 2_655 2_655
N21 Co1 N11 87.7(5) . 2_655
N31 Co1 N11 89.8(5) . .
N31 Co1 N11 178.1(4) 2_655 .
N21 Co1 N11 87.7(5) 2_655 .
N21 Co1 N11 90.5(4) . .
N11 Co1 N11 90.8(7) 2_655 .
N12 Co2 O63 89.1(5) 2_655 .
N12 Co2 N13 93.2(5) 2_655 .
O63 Co2 N13 176.1(6) . .
N12 Co2 O61 175.4(7) 2_655 .
O63 Co2 O61 88.0(5) . .
N13 Co2 O61 89.6(5) . .
N12 Co2 N22 91.0(6) 2_655 .
O63 Co2 N22 91.5(6) . .
N13 Co2 N22 91.6(6) . .
O61 Co2 N22 92.6(6) . .
N12 Co2 O65 89.3(6) 2_655 .
O63 Co2 O65 83.9(5) . .
N13 Co2 O65 93.0(5) . .
O61 Co2 O65 86.9(6) . .
N22 Co2 O65 175.4(5) . .
N35 Fe5 N25 93.6(5) . 2_655
N35 Fe5 N15 90.6(6) . .
N25 Fe5 N15 89.3(6) 2_655 .
N35 Fe5 O55 89.9(6) . .
N25 Fe5 O55 93.6(5) 2_655 .
N15 Fe5 O55 177.1(5) . .
N35 Fe5 O53 176.7(5) . .
N25 Fe5 O53 89.5(5) 2_655 .
N15 Fe5 O53 90.6(6) . .
O55 Fe5 O53 88.7(5) . .
N35 Fe5 O51 89.2(5) . .
N25 Fe5 O51 176.7(5) 2_655 .
N15 Fe5 O51 92.4(6) . .
O55 Fe5 O51 84.7(5) . .
O53 Fe5 O51 87.7(5) . .
O75 Fe3 N33 87.1(6) . 2_655
O75 Fe3 N32 93.2(5) . .
N33 Fe3 N32 90.1(4) 2_655 .
O75 Fe3 N23 174.1(5) . .
N33 Fe3 N23 96.5(5) 2_655 .
N32 Fe3 N23 91.5(5) . .
O75 Fe3 O73 88.0(5) . .
N33 Fe3 O73 175.1(6) 2_655 .
N32 Fe3 O73 90.2(4) . .
N23 Fe3 O73 88.3(5) . .
O75 Fe3 O71 85.7(5) . .
N33 Fe3 O71 91.2(4) 2_655 .
N32 Fe3 O71 178.2(5) . .
N23 Fe3 O71 89.6(5) . .
O73 Fe3 O71 88.4(4) . .
N24 Co4 N14 93.4(5) . .
N24 Co4 O41 174.3(5) . .
N14 Co4 O41 91.8(4) . .
N24 Co4 O43 92.6(5) . .
N14 Co4 O43 91.2(5) . .
O41 Co4 O43 84.8(5) . .
N24 Co4 O45 89.3(5) . .
N14 Co4 O45 175.2(5) . .
O41 Co4 O45 85.3(4) . .
O43 Co4 O45 84.7(5) . .
N24 Co4 N34 90.8(5) . .
N14 Co4 N34 91.0(5) . .
O41 Co4 N34 91.5(5) . .
O43 Co4 N34 175.8(5) . .
O45 Co4 N34 93.0(6) . .
N11 C11 W1 175.2(14) . .
C11 N11 Co1 172.1(12) . .
N12 C12 W1 177.6(13) . .
C12 N12 Fe2 171.9(16) . 2_655
C12 N12 Co2 171.9(16) . 2_655
N13 C13 W1 176.5(14) . .
C13 N13 Co2 177.2(15) . .
N14 C14 W1 175.7(13) . .
C14 N14 Co4 174.8(12) . .
N15 C15 W1 177.3(13) . .
C15 N15 Fe5 173.0(15) . .
N16 C16 W1 172(3) . .
N17 C17 W1 177.1(16) . .
N18A C18A W1 176(4) . .
N21 C21 W2 176.2(15) . .
C21 N21 Co1 175.8(13) . .
N22 C22 W2 178.9(17) . .
C22 N22 Co2 175.3(13) . .
N23 C23 W2 175.5(14) . .
C23 N23 Fe3 177.1(13) . .
N24 C24 W2 177.0(15) . .
C24 N24 Co4 173.0(15) . .
N25 C25 W2 176.8(12) . .
C25 N25 Fe5 171.8(13) . 2_655
N26 C26 W2 179(2) . .
N27A C27 W2 162(3) . .
N28 C28 W2 175.5(17) . .
N31 C31 W3 176.6(10) . .
C31 N31 Co1 175.4(11) . .
N32 C32 W3 176.3(11) . .
C32 N32 Fe3 169.7(13) . .
N33 C33 W3 178.1(13) . .
C33 N33 Fe3 172.8(12) . 2_655
N34 C34 W3 178.6(15) . .
C34 N34 Co4 171.6(12) . .
N35 C35 W3 175.9(14) . .
C35 N35 Fe5 178.1(16) . .
C36B C36A N36A 109(8) . .
C36B C36A N36B 63(7) . .
N36A C36A N36B 46(3) . .
C36B C36A W3 77(8) . .
N36A C36A W3 168(3) . .
N36B C36A W3 140(4) . .
N36B N36A C36A 72(4) . .
N36B N36A C36B 49(4) . .
C36A C36B N36B 86(8) . .
C36A C36B N36A 47(7) . .
C36A C36B C37A 142(9) . .
N36B C36B C37A 127(6) . .
N36A C36B C37A 165(5) . .
C36A C36B W3 84(8) . .
N36B C36B W3 170(6) . .
N36A C36B W3 130(4) . .
C37A C36B W3 63(2) . .
N36A N36B C36B 91(5) . .
N36A N36B C36A 61(3) . .
C37B C37A N37A 92(4) . .
C37B C37A N37B 45(4) . .
N37A C37A N37B 48(2) . .
C37B C37A C36B 112(5) . .
N37A C37A C36B 124(4) . .
N37B C37A C36B 139(3) . .
C37B C37A W3 78(4) . .
N37A C37A W3 170(3) . .
N37B C37A W3 122(3) . .
C36B C37A W3 60(2) . .
N37B N37A C37A 83(3) . .
N37B N37A C37B 47(3) . .
C37A C37B N37B 101(6) . .
C37A C37B N37A 52(3) . .
N37B C37B N37A 50(4) . .
C37A C37B W3 78(4) . .
N37B C37B W3 172(5) . .
N37A C37B W3 129(4) . .
C37B N37B N37A 83(5) . .
N37A N37B C37A 49(3) . .
N38 C38 W3 177.5(19) . .
C42A O41 Co4 126.0(15) . .
O41 C42A H42A 109.5 . .
O41 C42A H42B 109.5 . .
H42A C42A H42B 109.5 . .
O41 C42A H42C 109.5 . .
H42A C42A H42C 109.5 . .
H42B C42A H42C 109.5 . .
C44 O43 Co4 131(2) . .
O43 C44 H44A 109.5 . .
O43 C44 H44B 109.5 . .
H44A C44 H44B 109.5 . .
O43 C44 H44C 109.5 . .
H44A C44 H44C 109.5 . .
H44B C44 H44C 109.5 . .
O43 C44 H44D 109.5 . .
H44A C44 H44D 141.1 . .
H44B C44 H44D 56.3 . .
H44C C44 H44D 56.3 . .
O43 C44 H44E 109.5 . .
H44A C44 H44E 56.3 . .
H44B C44 H44E 141.1 . .
H44C C44 H44E 56.3 . .
H44D C44 H44E 109.5 . .
O43 C44 H44F 109.5 . .
H44A C44 H44F 56.3 . .
H44B C44 H44F 56.3 . .
H44C C44 H44F 141.1 . .
H44D C44 H44F 109.5 . .
H44E C44 H44F 109.5 . .
C46A O45 Co4 129.4(18) . .
O45 C46A H46A 109.5 . .
O45 C46A H46B 109.5 . .
H46A C46A H46B 109.5 . .
O45 C46A H46C 109.5 . .
H46A C46A H46C 109.5 . .
H46B C46A H46C 109.5 . .
C52A O51 Fe5 127(2) . .
O51 C52A H52A 109.5 . .
O51 C52A H52B 109.5 . .
H52A C52A H52B 109.5 . .
O51 C52A H52C 109.5 . .
H52A C52A H52C 109.5 . .
H52B C52A H52C 109.5 . .
C54 O53 Fe5 126.4(9) . .
O53 C54 H54A 109.5 . .
O53 C54 H54B 109.5 . .
H54A C54 H54B 109.5 . .
O53 C54 H54C 109.5 . .
H54A C54 H54C 109.5 . .
H54B C54 H54C 109.5 . .
O53 C54 H54D 109.5 . .
H54A C54 H54D 141.1 . .
H54B C54 H54D 56.3 . .
H54C C54 H54D 56.3 . .
O53 C54 H54E 109.5 . .
H54A C54 H54E 56.3 . .
H54B C54 H54E 141.1 . .
H54C C54 H54E 56.3 . .
H54D C54 H54E 109.5 . .
O53 C54 H54F 109.5 . .
H54A C54 H54F 56.3 . .
H54B C54 H54F 56.3 . .
H54C C54 H54F 141.1 . .
H54D C54 H54F 109.5 . .
H54E C54 H54F 109.5 . .
C56A O55 Fe5 118.6(18) . .
O55 C56A H56A 109.5 . .
O55 C56A H56B 109.5 . .
H56A C56A H56B 109.5 . .
O55 C56A H56C 109.5 . .
H56A C56A H56C 109.5 . .
H56B C56A H56C 109.5 . .
C62 O61 Co2 121.4(14) . .
O61 C62 H62A 109.5 . .
O61 C62 H62B 109.5 . .
H62A C62 H62B 109.5 . .
O61 C62 H62C 109.5 . .
H62A C62 H62C 109.5 . .
H62B C62 H62C 109.5 . .
C64 O63 Co2 126.2(13) . .
O63 C64 H64A 109.5 . .
O63 C64 H64B 109.5 . .
H64A C64 H64B 109.5 . .
O63 C64 H64C 109.5 . .
H64A C64 H64C 109.5 . .
H64B C64 H64C 109.5 . .
C66 O65 Co2 117.6(16) . .
O65 C66 H66A 109.5 . .
O65 C66 H66B 109.5 . .
H66A C66 H66B 109.5 . .
O65 C66 H66C 109.5 . .
H66A C66 H66C 109.5 . .
H66B C66 H66C 109.5 . .
C72 O71 Fe3 122.0(11) . .
O71 C72 H72A 109.5 . .
O71 C72 H72B 109.5 . .
H72A C72 H72B 109.5 . .
O71 C72 H72C 109.5 . .
H72A C72 H72C 109.5 . .
H72B C72 H72C 109.5 . .
C74 O73 Fe3 124.4(10) . .
O73 C74 H74A 109.5 . .
O73 C74 H74B 109.5 . .
H74A C74 H74B 109.5 . .
O73 C74 H74C 109.5 . .
H74A C74 H74C 109.5 . .
H74B C74 H74C 109.5 . .
C76A O75 Fe3 142(3) . .
O75 C76A H76A 109.5 . .
O75 C76A H76B 109.5 . .
H76A C76A H76B 109.5 . .
O75 C76A H76C 109.5 . .
H76A C76A H76C 109.5 . .
H76B C76A H76C 109.5 . .
O75 C76A H76D 109.5 . .
H76A C76A H76D 141.1 . .
H76B C76A H76D 56.3 . .
H76C C76A H76D 56.3 . .
O75 C76A H76E 109.5 . .
H76A C76A H76E 56.3 . .
H76B C76A H76E 141.1 . .
H76C C76A H76E 56.3 . .
H76D C76A H76E 109.5 . .
O75 C76A H76F 109.5 . .
H76A C76A H76F 56.3 . .
H76B C76A H76F 56.3 . .
H76C C76A H76F 141.1 . .
H76D C76A H76F 109.5 . .
H76E C76A H76F 109.5 . .
O2 C2B C2A 48(3) . .
O2 C2A C2B 49(3) . .
C2A O2 C2B 83(6) . .
C8 O8 C8 117(5) 2_655 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 C18A 2.06(3) .
W1 C13 2.100(15) .
W1 C16 2.12(3) .
W1 C14 2.121(16) .
W1 C15 2.16(2) .
W1 C17 2.18(2) .
W1 C12 2.186(19) .
W1 C11 2.202(18) .
W2 C22 2.07(2) .
W2 C25 2.096(18) .
W2 C26 2.097(18) .
W2 C23 2.11(2) .
W2 C27 2.14(2) .
W2 C24 2.155(18) .
W2 C28 2.161(18) .
W2 C21 2.187(14) .
W3 C36B 2.01(7) .
W3 C36A 2.05(4) .
W3 C37B 2.08(5) .
W3 C37A 2.08(3) .
W3 C32 2.092(15) .
W3 C38 2.095(17) .
W3 C33 2.111(16) .
W3 C35 2.122(18) .
W3 C34 2.13(2) .
W3 C31 2.196(18) .
Co1 N31 1.900(12) .
Co1 N31 1.900(12) 2_655
Co1 N21 1.900(10) 2_655
Co1 N21 1.900(10) .
Co1 N11 1.908(12) 2_655
Co1 N11 1.908(12) .
Co2 N12 2.008(13) 2_655
Co2 O63 2.024(12) .
Co2 N13 2.054(13) .
Co2 O61 2.062(12) .
Co2 N22 2.065(17) .
Co2 O65 2.077(14) .
Fe5 N35 2.030(15) .
Fe5 N25 2.049(13) 2_655
Fe5 N15 2.059(16) .
Fe5 O55 2.062(13) .
Fe5 O53 2.067(12) .
Fe5 O51 2.078(11) .
Fe3 O75 2.039(14) .
Fe3 N33 2.044(12) 2_655
Fe3 N32 2.045(12) .
Fe3 N23 2.065(17) .
Fe3 O73 2.081(10) .
Fe3 O71 2.100(10) .
Co4 N24 2.038(14) .
Co4 N14 2.040(14) .
Co4 O41 2.058(11) .
Co4 O43 2.069(12) .
Co4 O45 2.079(12) .
Co4 N34 2.081(16) .
C11 N11 1.131(18) .
C12 N12 1.156(19) .
N12 Fe2 2.008(13) 2_655
N12 Co2 2.008(13) 2_655
C13 N13 1.172(17) .
C14 N14 1.170(18) .
C15 N15 1.13(2) .
C16 N16 1.17(3) .
C17 N17 1.14(2) .
C18A N18A 1.12(3) .
C21 N21 1.141(15) .
C22 N22 1.17(2) .
C23 N23 1.18(2) .
C24 N24 1.136(18) .
C25 N25 1.185(18) .
N25 Fe5 2.049(13) 2_655
C26 N26 1.18(2) .
C27 N27A 1.29(4) .
C28 N28 1.14(2) .
C31 N31 1.143(18) .
C32 N32 1.211(17) .
C33 N33 1.213(17) .
N33 Fe3 2.044(12) 2_655
C34 N34 1.16(2) .
C35 N35 1.179(19) .
C38 N38 1.194(19) .
O41 C42A 1.43(3) .
C42A H42A 0.98 .
C42A H42B 0.98 .
C42A H42C 0.98 .
O43 C44 1.43(4) .
C44 H44A 0.98 .
C44 H44B 0.98 .
C44 H44C 0.98 .
C44 H44D 0.98 .
C44 H44E 0.98 .
C44 H44F 0.98 .
O45 C46A 1.28(4) .
C46A H46A 0.98 .
C46A H46B 0.98 .
C46A H46C 0.98 .
O51 C52A 1.30(5) .
C52A H52A 0.98 .
C52A H52B 0.98 .
C52A H52C 0.98 .
O53 C54 1.47(2) .
C54 H54A 0.98 .
C54 H54B 0.98 .
C54 H54C 0.98 .
C54 H54D 0.98 .
C54 H54E 0.98 .
C54 H54F 0.98 .
O55 C56A 1.56(5) .
C56A H56A 0.98 .
C56A H56B 0.98 .
C56A H56C 0.98 .
O61 C62 1.46(2) .
C62 H62A 0.98 .
C62 H62B 0.98 .
C62 H62C 0.98 .
O63 C64 1.37(2) .
C64 H64A 0.98 .
C64 H64B 0.98 .
C64 H64C 0.98 .
O65 C66 1.47(3) .
C66 H66A 0.98 .
C66 H66B 0.98 .
C66 H66C 0.98 .
O71 C72 1.44(2) .
C72 H72A 0.98 .
C72 H72B 0.98 .
C72 H72C 0.98 .
O73 C74 1.45(2) .
C74 H74A 0.98 .
C74 H74B 0.98 .
C74 H74C 0.98 .
O75 C76A 1.14(6) .
C76A H76A 0.98 .
C76A H76B 0.98 .
C76A H76C 0.98 .
C76A H76D 0.98 .
C76A H76E 0.98 .
C76A H76F 0.98 .
C1 O1 1.432(10) .
C2B O2 1.430(10) .
C2A O2 1.420(10) .
C3 O3 1.428(10) .
C4A O4A 1.433(10) .
C4B O4B 1.428(10) .
C5A O5 1.432(10) .
C6 O6A 1.425(10) .
O7 C7 1.435(10) .
O8 C8 1.420(10) 2_655
O8 C8 1.420(10) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C36B C36A N36A N36B 11(8)
W3 C36A N36A N36B 126(16)
N36B C36A N36A C36B -11(8)
N36A C36A C36B N36B -9(6)
W3 C36A C36B N36B -177(4)
N36B C36A C36B N36A 9(6)
W3 C36A C36B N36A -169(4)
N36A C36A C36B C37A -163(9)
N36B C36A C36B C37A -154(14)
W3 C36A C36B C37A 28(11)
N36A C36A C36B W3 169(4)
N36B C36A C36B W3 177(4)
N36B N36A C36B C36A -166(10)
C36A N36A C36B N36B 166(10)
N36B N36A C36B C37A -31(15)
N36B N36A C36B W3 179(7)
C36A N36A C36B W3 -15(5)
C36A N36A N36B C36B -6(4)
C36B N36A N36B C36A 6(4)
C36A C36B N36B N36A 10(7)
C37A C36B N36B N36A 171(4)
N36A C36B N36B C36A -10(7)
C37A C36B N36B C36A 161(10)
C36B C36A N36B N36A -169(8)
W3 C36A N36B N36A -165(5)
N36A C36A N36B C36B 169(8)
W3 C36A N36B C36B 4(6)
C37B C37A N37A N37B -9(6)
C36B C37A N37A N37B -128(4)
W3 C37A N37A N37B -19(19)
N37B C37A N37A C37B 9(6)
C36B C37A N37A C37B -119(6)
W3 C37A N37A C37B -10(16)
N37A C37A C37B N37B 10(6)
C36B C37A C37B N37B 138(5)
W3 C37A C37B N37B -172(5)
N37B C37A C37B N37A -10(6)
C36B C37A C37B N37A 129(5)
W3 C37A C37B N37A 178(3)
N37A C37A C37B W3 -178(3)
N37B C37A C37B W3 172(5)
C36B C37A C37B W3 -50(3)
N37B N37A C37B C37A 168(8)
C37A N37A C37B N37B -168(8)
N37B N37A C37B W3 170(7)
C37A N37A C37B W3 2(3)
C37A C37B N37B N37A -10(6)
N37A C37B N37B C37A 10(6)
C37A N37A N37B C37B 7(4)
C37B N37A N37B C37A -7(4)
N37A C37A N37B C37B -167(8)
C36B C37A N37B C37B -71(8)
W3 C37A N37B C37B 9(6)
C37B C37A N37B N37A 167(8)
C36B C37A N37B N37A 97(6)
W3 C37A N37B N37A 176(4)
