#------------------------------------------------------------------------------
#$Date: 2024-01-11 10:34:38 +0200 (Thu, 11 Jan 2024) $
#$Revision: 289031 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/33/15/4331589.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_4331589
loop_
_publ_author_name
'Nyman, May'
'Celestian, Aaron J.'
'Parise, John B.'
'Holland, Gregory P.'
'Alam, Todd M.'
_publ_section_title
;
 Solid-State Structural Characterization of a Rigid Framework of Lacunary
 Heteropolyniobates
;
_journal_issue                   3
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1043
_journal_page_last               1052
_journal_paper_doi               10.1021/ic051155g
_journal_volume                  45
_journal_year                    2006
_chemical_formula_moiety         '15(Na+), Nb9 O40 P4, 22(H2 O)'
_chemical_formula_sum            'Na15 Nb9 O62 P4'
_chemical_formula_weight         2296.92
_chemical_melting_point          ?
_chemical_name_common            'A-type trivacant alpha-Keggin ion'
_chemical_name_systematic
; 
 Lacunary Keggin Ion 
;
_space_group_IT_number           2
_symmetry_cell_setting           1
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   none
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                93.12(3)
_cell_angle_beta                 99.78(3)
_cell_angle_gamma                119.84(3)
_cell_formula_units_Z            2
_cell_length_a                   12.242(2)
_cell_length_b                   12.291(3)
_cell_length_c                   22.056(4)
_cell_measurement_reflns_used    7522
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      31.19
_cell_measurement_theta_min      2.61
_cell_volume                     2799.1(14)
_computing_cell_refinement       DENZO
_computing_data_reduction        DENZO
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.905
_diffrn_measured_fraction_theta_max 0.905
_diffrn_measurement_device_type  MAR345
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.92200
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0211
_diffrn_reflns_limit_h_max       0
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            7522
_diffrn_reflns_theta_full        31.19
_diffrn_reflns_theta_max         31.19
_diffrn_reflns_theta_min         2.61
_exptl_absorpt_coefficient_mu    2.141
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.725
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             2180
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.0015
_refine_diff_density_max         2.301
_refine_diff_density_min         -1.681
_refine_diff_density_rms         0.218
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.100
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_parameters     787
_refine_ls_number_reflns         7522
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.100
_refine_ls_R_factor_all          0.0474
_refine_ls_R_factor_gt           0.0471
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0724P)²+37.0798P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1327
_refine_ls_wR_factor_ref         0.1329
_reflns_number_gt                7418
_reflns_number_total             7522
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic051155gsup1.cif
_cod_data_source_block           NaNbPO_Lacunary
_cod_depositor_comments
;
The following automatic conversions were performed:

'_chemical_melting_point' value 'not measured' was changed to '?' -
the value is undefined or not given.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 

2024-01-11
Z value and formula fixed to values more according to usual
chemical conventions.                 miguel
;
_cod_original_formula_weight         1148.46
_cod_original_formula_moiety         'Na7.50 Nb4.50 O31 P2'
_cod_original_formula_units_Z            4
_cod_original_cell_volume        2799.2(10)
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'Na7.50 Nb4.50 O31 P2'
_cod_database_code               4331589
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Na1 Na 0.4668(4) 0.8182(4) 0.41489(16) 0.0353(9) Uani 1 1 d .
Na2 Na 0.9544(3) 0.6824(3) 1.05276(15) 0.0263(8) Uani 1 1 d .
Na3 Na 0.8832(4) 0.8672(4) 0.58558(16) 0.0363(9) Uani 1 1 d .
Na4 Na 0.2753(4) 0.3900(4) 0.72485(17) 0.0336(9) Uani 1 1 d .
Na5 Na 0.5672(4) 0.5493(4) 0.64411(18) 0.0446(10) Uani 1 1 d .
Na6 Na 0.6337(3) 0.5926(3) 0.79036(15) 0.0285(8) Uani 1 1 d .
Na7 Na 0.7084(3) 0.6457(3) 0.94456(15) 0.0261(8) Uani 1 1 d .
Na8 Na 0.7524(3) 0.9050(4) 0.72869(17) 0.0331(9) Uani 1 1 d .
Na9 Na 0.7887(3) 0.4301(3) 0.72416(16) 0.0324(9) Uani 1 1 d .
Na10 Na 0.2037(4) 0.5359(4) 0.58496(16) 0.0344(9) Uani 1 1 d .
Na11 Na 0.9010(3) 0.2148(3) 0.64545(14) 0.0239(8) Uani 1 1 d .
Na12 Na 0.9698(3) 0.2672(3) 0.79136(15) 0.0297(8) Uani 1 1 d .
Na13 Na 0.3359(7) 1.0906(8) 0.8415(5) 0.121(3) Uani 1 1 d .
Na14 Na 0.1924(9) 0.8046(10) 0.8437(6) 0.146(4) Uani 1 1 d .
Na15 Na 0.5808(15) 1.1594(9) 0.9998(5) 0.111(7) Uani 1 1 d .
P1 P 0.32639(18) 0.6119(2) 0.84424(9) 0.0144(4) Uani 1 1 d .
P2 P 0.00039(18) 0.95008(19) 0.84553(9) 0.0139(4) Uani 1 1 d .
P3 P 0.66530(18) 1.28173(19) 0.84395(9) 0.0141(4) Uani 1 1 d .
P4 P 0.26610(17) 0.90327(18) 0.71121(8) 0.0092(4) Uani 1 1 d .
Nb1 Nb 0.03549(6) 0.69448(6) 0.57261(3) 0.01107(18) Uani 1 1 d .
Nb2 Nb 0.20190(6) 1.02202(6) 0.57264(3) 0.01140(19) Uani 1 1 d .
Nb3 Nb 0.42713(6) 0.73052(6) 0.71877(3) 0.00844(18) Uani 1 1 d .
Nb4 Nb 0.36464(6) 0.85590(6) 0.57304(3) 0.01113(18) Uani 1 1 d .
Nb5 Nb -0.06438(6) 0.74880(6) 0.71838(3) 0.00842(18) Uani 1 1 d .
Nb6 Nb 0.10509(6) 0.57101(6) 0.71846(3) 0.00859(18) Uani 1 1 d .
Nb7 Nb 0.09897(6) 1.06999(6) 0.71910(3) 0.00838(18) Uani 1 1 d .
Nb8 Nb 0.60378(6) 1.07554(6) 0.71958(3) 0.00849(18) Uani 1 1 d .
Nb9 Nb 0.44556(6) 1.23961(6) 0.71782(3) 0.00916(18) Uani 1 1 d .
O1 O -0.0087(5) 0.4088(5) 0.7177(2) 0.0189(12) Uani 1 1 d .
O2 O 0.0104(5) 0.6470(5) 0.7459(2) 0.0147(11) Uani 1 1 d .
O3 O 0.0605(5) 0.5849(5) 0.6323(2) 0.0171(12) Uani 1 1 d .
O4 O -0.0590(5) 0.7186(5) 0.6333(2) 0.0195(13) Uani 1 1 d .
O5 O 0.1845(5) 0.7133(5) 0.5417(2) 0.0174(12) Uani 1 1 d .
O6 O 0.3206(5) 0.9792(5) 0.5415(2) 0.0189(12) Uani 1 1 d .
O7 O 0.1035(5) 1.0447(5) 0.6326(2) 0.0171(12) Uani 1 1 d .
O8 O 0.0507(5) 1.1835(5) 0.7188(2) 0.0179(12) Uani 1 1 d .
O9 O 0.5212(5) 1.0009(5) 0.6332(2) 0.0167(12) Uani 1 1 d .
O10 O 0.5516(5) 0.9117(5) 0.7468(2) 0.0144(11) Uani 1 1 d .
O11 O 0.3904(5) 0.7496(5) 0.6337(2) 0.0180(12) Uani 1 1 d .
O12 O 0.2748(5) 0.7926(5) 0.7341(2) 0.0145(11) Uani 1 1 d .
O13 O 0.3963(5) 1.0280(5) 0.7345(2) 0.0142(11) Uani 1 1 d .
O14 O 0.0525(5) 0.8491(5) 0.5413(2) 0.0175(12) Uani 1 1 d .
O15 O 0.4347(5) 0.8302(6) 0.5154(3) 0.0242(14) Uani 1 1 d .
O16 O 0.2312(5) 0.8795(5) 0.6392(2) 0.0134(11) Uani 1 1 d .
O17 O -0.0956(5) 0.5797(5) 0.5147(2) 0.0231(13) Uani 1 1 d .
O18 O 0.5375(5) 0.6778(6) 0.7178(3) 0.0229(13) Uani 1 1 d .
O19 O 0.1603(5) 0.9136(5) 0.7351(2) 0.0167(12) Uani 1 1 d .
O20 O 0.1949(5) 0.6019(5) 0.8158(2) 0.0168(12) Uani 1 1 d .
O21 O 0.4296(5) 0.7203(5) 0.8160(2) 0.0183(12) Uani 1 1 d .
O22 O 0.2855(5) 1.1864(5) 0.7465(2) 0.0154(12) Uani 1 1 d .
O23 O -0.1278(5) 0.9458(6) 0.8304(3) 0.0223(13) Uani 1 1 d .
O24 O 0.1023(5) 1.0577(5) 0.8165(2) 0.0178(12) Uani 1 1 d .
O25 O 0.0548(5) 0.9732(5) 0.9153(2) 0.0236(14) Uani 1 1 d .
O26 O 0.1818(6) 1.1064(6) 0.5149(3) 0.0268(14) Uani 1 1 d .
O27 O -0.2284(5) 0.6384(5) 0.7168(3) 0.0220(13) Uani 1 1 d .
O28 O 0.3574(5) 1.1671(5) 0.6328(2) 0.0189(12) Uani 1 1 d .
O29 O 0.5343(5) 1.2729(5) 0.8156(2) 0.0179(12) Uani 1 1 d .
O30 O 0.6494(5) 1.1529(5) 0.8167(2) 0.0159(12) Uani 1 1 d .
O31 O 0.6856(6) 1.2930(6) 0.9144(3) 0.0254(14) Uani 1 1 d .
O32 O 0.3597(5) 0.6494(6) 0.9145(3) 0.0262(14) Uani 1 1 d .
O33 O -0.0166(5) 0.8228(5) 0.8157(2) 0.0178(12) Uani 1 1 d .
O34 O 0.7768(5) 1.3934(5) 0.8246(3) 0.0244(14) Uani 1 1 d .
O35 O 0.4966(5) 1.4010(5) 0.7161(3) 0.0243(14) Uani 1 1 d .
O36 O 0.5966(5) 1.2301(5) 0.7051(2) 0.0136(11) Uani 1 1 d .
O37 O 0.7657(5) 1.1243(5) 0.7190(2) 0.0178(12) Uani 1 1 d .
O38 O -0.0668(5) 0.9055(5) 0.7058(2) 0.0145(12) Uani 1 1 d .
O39 O 0.2592(5) 0.5685(5) 0.7049(2) 0.0155(12) Uani 1 1 d .
O40 O 0.3201(6) 0.4879(6) 0.8258(3) 0.0253(14) Uani 1 1 d .
O50 O 0.8211(7) 0.6227(6) 0.8704(3) 0.0359(16) Uani 1 1 d .
O51 O 0.7499(6) 0.5022(5) 0.9992(3) 0.0263(15) Uani 1 1 d .
O52 O 0.9142(6) 0.8304(5) 0.9988(3) 0.0280(15) Uani 1 1 d .
O53 O 0.5614(9) 0.6498(8) 1.0025(4) 0.058(2) Uani 1 1 d .
O54 O 0.6725(6) 0.7695(7) 0.8735(3) 0.0373(17) Uani 1 1 d .
O55 O 0.8442(7) 0.7101(6) 1.1268(3) 0.0399(18) Uani 1 1 d .
O56 O 1.1386(6) 0.8549(7) 1.1232(3) 0.0419(18) Uani 1 1 d .
O57 O 0.9841(6) 0.5468(7) 1.1185(4) 0.0436(19) Uani 1 1 d .
O58 O 1.0898(7) 0.6493(7) 0.9968(4) 0.050(2) Uani 1 1 d .
O59 O 1.0504(12) 0.2278(12) 0.5855(4) 0.085(4) Uani 1 1 d .
O60 O 0.7328(8) 0.0198(10) 0.5853(4) 0.075(3) Uani 1 1 d .
O61 O 0.8389(11) 0.3364(8) 0.5852(4) 0.082(4) Uani 1 1 d .
O62 O 0.5217(6) 0.4668(7) 0.8788(4) 0.0450(19) Uani 1 1 d .
O63 O 0.7046(17) 0.4290(17) 0.6102(8) 0.152(6) Uiso 1 1 d .
O64 O 0.2896(18) 0.3800(18) 0.6100(9) 0.158(6) Uiso 1 1 d .
O65 O 0.6621(19) 0.8053(19) 0.6132(9) 0.166(7) Uiso 1 1 d .
O66 O 0.3133(18) 1.1248(18) 0.9394(8) 0.103(5) Uiso 0.70 1 d P
O67 O 0.4469(12) 0.9492(13) 0.8513(6) 0.060(3) Uiso 0.70 1 d P
O68 O 0.1752(17) 0.8387(17) 0.9400(8) 0.097(5) Uiso 0.70 1 d P
O69 O 0.691(3) 0.582(3) 0.5487(17) 0.186(13) Uiso 0.60 1 d P
O70 O 0.432(4) 0.360(4) 0.5521(19) 0.142(14) Uiso 0.40 1 d P
O71 O 0.467(4) 0.616(4) 0.5515(19) 0.181(15) Uiso 0.50 1 d P
O72 O 0.523(3) 0.952(3) 0.8814(14) 0.059(7) Uiso 0.30 1 d P
O73 O 0.4012(10) 0.9893(11) 0.9679(5) 0.081(3) Uiso 1 1 d .
O74 O 0.407(2) 1.153(2) 1.0352(10) 0.063(6) Uiso 0.40 1 d P
O75 O 0.630(3) 0.978(3) 0.9259(12) 0.082(7) Uiso 0.40 1 d P
O76 O 0.756(3) 1.041(3) 0.9879(13) 0.060(7) Uiso 0.30 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Nb Nb -2.0727 0.6215 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O15 Na1 O9 110.9(3) . 2_676
O15 Na1 O28 136.1(3) . 2_676
O9 Na1 O28 90.1(2) 2_676 2_676
O15 Na1 O6 84.6(2) . 2_676
O9 Na1 O6 68.2(2) 2_676 2_676
O28 Na1 O6 67.6(2) 2_676 2_676
O15 Na1 O36 156.7(3) . 2_676
O9 Na1 O36 66.96(19) 2_676 2_676
O28 Na1 O36 66.67(19) 2_676 2_676
O6 Na1 O36 113.9(2) 2_676 2_676
O15 Na1 O63 91.5(4) . 2_666
O9 Na1 O63 132.5(4) 2_676 2_666
O28 Na1 O63 102.1(4) 2_676 2_666
O6 Na1 O63 158.4(5) 2_676 2_666
O36 Na1 O63 76.2(4) 2_676 2_666
O15 Na1 Nb9 165.0(2) . 2_676
O9 Na1 Nb9 82.39(15) 2_676 2_676
O28 Na1 Nb9 32.89(13) 2_676 2_676
O6 Na1 Nb9 94.29(16) 2_676 2_676
O36 Na1 Nb9 34.71(13) 2_676 2_676
O63 Na1 Nb9 83.9(4) 2_666 2_676
O15 Na1 Nb4 91.75(19) . 2_676
O9 Na1 Nb4 35.38(13) 2_676 2_676
O28 Na1 Nb4 83.90(17) 2_676 2_676
O6 Na1 Nb4 34.34(14) 2_676 2_676
O36 Na1 Nb4 96.34(16) 2_676 2_676
O63 Na1 Nb4 167.2(4) 2_666 2_676
Nb9 Na1 Nb4 95.79(9) 2_676 2_676
O15 Na1 Nb8 135.5(2) . 2_676
O9 Na1 Nb8 33.04(13) 2_676 2_676
O28 Na1 Nb8 81.89(16) 2_676 2_676
O6 Na1 Nb8 94.52(17) 2_676 2_676
O36 Na1 Nb8 34.75(13) 2_676 2_676
O63 Na1 Nb8 102.9(4) 2_666 2_676
Nb9 Na1 Nb8 59.49(6) 2_676 2_676
Nb4 Na1 Nb8 66.46(8) 2_676 2_676
O15 Na1 Nb2 106.99(19) . 2_676
O9 Na1 Nb2 84.34(16) 2_676 2_676
O28 Na1 Nb2 34.94(13) 2_676 2_676
O6 Na1 Nb2 34.20(14) 2_676 2_676
O36 Na1 Nb2 95.98(15) 2_676 2_676
O63 Na1 Nb2 129.7(4) 2_666 2_676
Nb9 Na1 Nb2 66.10(8) 2_676 2_676
Nb4 Na1 Nb2 60.69(7) 2_676 2_676
Nb8 Na1 Nb2 95.58(9) 2_676 2_676
O15 Na1 Na9 124.2(2) . 2_666
O9 Na1 Na9 93.67(17) 2_676 2_666
O28 Na1 Na9 90.54(17) 2_676 2_666
O6 Na1 Na9 150.64(18) 2_676 2_666
O36 Na1 Na9 36.89(13) 2_676 2_666
O63 Na1 Na9 41.3(4) 2_666 2_666
Nb9 Na1 Na9 59.43(8) 2_676 2_666
Nb4 Na1 Na9 128.38(12) 2_676 2_666
Nb8 Na1 Na9 61.95(8) 2_676 2_666
Nb2 Na1 Na9 125.23(12) 2_676 2_666
O56 Na2 O57 86.5(3) . .
O56 Na2 O55 82.2(3) . .
O57 Na2 O55 85.2(3) . .
O56 Na2 O58 91.2(3) . .
O57 Na2 O58 84.7(3) . .
O55 Na2 O58 168.3(3) . .
O56 Na2 O51 168.7(3) . .
O57 Na2 O51 88.5(3) . .
O55 Na2 O51 87.3(2) . .
O58 Na2 O51 98.4(3) . .
O56 Na2 O52 90.5(3) . .
O57 Na2 O52 171.3(3) . .
O55 Na2 O52 86.4(3) . .
O58 Na2 O52 103.5(3) . .
O51 Na2 O52 92.9(2) . .
O56 Na2 Na7 136.5(2) . .
O57 Na2 Na7 134.0(2) . .
O55 Na2 Na7 85.7(2) . .
O58 Na2 Na7 105.6(2) . .
O51 Na2 Na7 46.02(17) . .
O52 Na2 Na7 46.92(16) . .
O56 Na2 Na12 50.6(2) . 2_767
O57 Na2 Na12 53.3(2) . 2_767
O55 Na2 Na12 49.2(2) . 2_767
O58 Na2 Na12 119.4(2) . 2_767
O51 Na2 Na12 118.76(19) . 2_767
O52 Na2 Na12 119.0(2) . 2_767
Na7 Na2 Na12 134.85(14) . 2_767
O26 Na3 O7 109.5(2) 2_676 1_655
O26 Na3 O4 136.1(3) 2_676 1_655
O7 Na3 O4 89.4(2) 1_655 1_655
O26 Na3 O14 83.6(2) 2_676 1_655
O7 Na3 O14 67.8(2) 1_655 1_655
O4 Na3 O14 67.0(2) 1_655 1_655
O26 Na3 O38 157.3(3) 2_676 1_655
O7 Na3 O38 67.15(19) 1_655 1_655
O4 Na3 O38 66.4(2) 1_655 1_655
O14 Na3 O38 113.6(2) 1_655 1_655
O26 Na3 O65 93.3(5) 2_676 .
O7 Na3 O65 130.8(5) 1_655 .
O4 Na3 O65 103.9(5) 1_655 .
O14 Na3 O65 160.5(5) 1_655 .
O38 Na3 O65 75.3(5) 1_655 .
O26 Na3 Nb5 165.6(2) 2_676 1_655
O7 Na3 Nb5 82.37(16) 1_655 1_655
O4 Na3 Nb5 32.83(13) 1_655 1_655
O14 Na3 Nb5 93.98(17) 1_655 1_655
O38 Na3 Nb5 34.64(13) 1_655 1_655
O65 Na3 Nb5 84.3(4) . 1_655
O26 Na3 Nb7 134.6(2) 2_676 1_655
O7 Na3 Nb7 33.18(13) 1_655 1_655
O4 Na3 Nb7 81.53(15) 1_655 1_655
O14 Na3 Nb7 94.38(16) 1_655 1_655
O38 Na3 Nb7 34.88(12) 1_655 1_655
O65 Na3 Nb7 101.4(4) . 1_655
Nb5 Na3 Nb7 59.57(6) 1_655 1_655
O26 Na3 Nb2 90.47(19) 2_676 1_655
O7 Na3 Nb2 35.18(13) 1_655 1_655
O4 Na3 Nb2 82.95(16) 1_655 1_655
O14 Na3 Nb2 34.16(13) 1_655 1_655
O38 Na3 Nb2 96.19(16) 1_655 1_655
O65 Na3 Nb2 165.3(5) . 1_655
Nb5 Na3 Nb2 95.41(10) 1_655 1_655
Nb7 Na3 Nb2 66.38(8) 1_655 1_655
O26 Na3 Nb1 106.3(2) 2_676 1_655
O7 Na3 Nb1 84.10(17) 1_655 1_655
O4 Na3 Nb1 34.56(14) 1_655 1_655
O14 Na3 Nb1 34.11(14) 1_655 1_655
O38 Na3 Nb1 95.77(17) 1_655 1_655
O65 Na3 Nb1 131.4(5) . 1_655
Nb5 Na3 Nb1 65.91(8) 1_655 1_655
Nb7 Na3 Nb1 95.54(10) 1_655 1_655
Nb2 Na3 Nb1 60.42(7) 1_655 1_655
O26 Na3 Na8 126.1(2) 2_676 .
O7 Na3 Na8 92.91(17) 1_655 .
O4 Na3 Na8 90.49(17) 1_655 .
O14 Na3 Na8 149.60(18) 1_655 .
O38 Na3 Na8 36.06(14) 1_655 .
O65 Na3 Na8 41.0(4) . .
Nb5 Na3 Na8 59.08(8) 1_655 .
Nb7 Na3 Na8 60.98(8) 1_655 .
Nb2 Na3 Na8 127.34(12) 1_655 .
Nb1 Na3 Na8 124.79(12) 1_655 .
O40 Na4 O39 79.9(2) . .
O40 Na4 O64 155.7(5) . .
O39 Na4 O64 82.1(5) . .
O40 Na4 O8 100.9(2) . 1_545
O39 Na4 O8 113.5(2) . 1_545
O64 Na4 O8 101.2(5) . 1_545
O40 Na4 O22 100.3(2) . 1_545
O39 Na4 O22 178.2(2) . 1_545
O64 Na4 O22 98.1(5) . 1_545
O8 Na4 O22 64.74(19) 1_545 1_545
O40 Na4 O35 103.5(2) . 1_545
O39 Na4 O35 117.0(2) . 1_545
O64 Na4 O35 70.6(4) . 1_545
O8 Na4 O35 126.7(2) 1_545 1_545
O22 Na4 O35 64.66(19) 1_545 1_545
O40 Na4 Nb7 108.7(2) . 1_545
O39 Na4 Nb7 143.3(2) . 1_545
O64 Na4 Nb7 95.5(4) . 1_545
O8 Na4 Nb7 30.82(13) 1_545 1_545
O22 Na4 Nb7 34.94(12) 1_545 1_545
O35 Na4 Nb7 96.06(17) 1_545 1_545
O40 Na4 Nb9 110.1(2) . 1_545
O39 Na4 Nb9 146.6(2) . 1_545
O64 Na4 Nb9 77.4(4) . 1_545
O8 Na4 Nb9 96.23(17) 1_545 1_545
O22 Na4 Nb9 34.90(12) 1_545 1_545
O35 Na4 Nb9 30.68(13) 1_545 1_545
Nb7 Na4 Nb9 65.47(7) 1_545 1_545
O40 Na4 P1 21.09(16) . .
O39 Na4 P1 58.86(15) . .
O64 Na4 P1 137.8(5) . .
O8 Na4 P1 108.39(18) 1_545 .
O22 Na4 P1 121.42(17) 1_545 .
O35 Na4 P1 111.35(17) 1_545 .
Nb7 Na4 P1 125.12(12) 1_545 .
Nb9 Na4 P1 126.88(12) 1_545 .
O40 Na4 Nb3 74.13(17) . .
O39 Na4 Nb3 29.48(13) . .
O64 Na4 Nb3 82.2(4) . .
O8 Na4 Nb3 142.65(19) 1_545 .
O22 Na4 Nb3 152.29(18) 1_545 .
O35 Na4 Nb3 89.83(16) 1_545 .
Nb7 Na4 Nb3 172.56(13) 1_545 .
Nb9 Na4 Nb3 120.52(11) 1_545 .
P1 Na4 Nb3 56.03(7) . .
O40 Na4 Nb6 73.79(19) . .
O39 Na4 Nb6 27.83(13) . .
O64 Na4 Nb6 97.1(4) . .
O8 Na4 Nb6 87.67(16) 1_545 .
O22 Na4 Nb6 150.55(18) 1_545 .
O35 Na4 Nb6 144.65(18) 1_545 .
Nb7 Na4 Nb6 118.48(11) 1_545 .
Nb9 Na4 Nb6 173.79(12) 1_545 .
P1 Na4 Nb6 55.73(7) . .
Nb3 Na4 Nb6 55.15(6) . .
O40 Na4 Na6 68.94(18) . .
O39 Na4 Na6 92.08(18) . .
O64 Na4 Na6 95.6(4) . .
O8 Na4 Na6 150.9(2) 1_545 .
O22 Na4 Na6 89.66(17) 1_545 .
O35 Na4 Na6 39.50(14) 1_545 .
Nb7 Na4 Na6 124.52(13) 1_545 .
Nb9 Na4 Na6 64.46(9) 1_545 .
P1 Na4 Na6 72.25(10) . .
Nb3 Na4 Na6 62.85(9) . .
Nb6 Na4 Na6 113.69(11) . .
O27 Na5 O18 81.7(2) 1_655 .
O27 Na5 O35 82.5(2) 1_655 1_545
O18 Na5 O35 82.8(2) . 1_545
O27 Na5 O71 137.2(10) 1_655 .
O18 Na5 O71 91.4(10) . .
O35 Na5 O71 138.7(10) 1_545 .
O27 Na5 O70 136.3(10) 1_655 .
O18 Na5 O70 139.8(10) . .
O35 Na5 O70 89.2(10) 1_545 .
O71 Na5 O70 69.4(14) . .
O27 Na5 O69 89.1(8) 1_655 .
O18 Na5 O69 137.9(8) . .
O35 Na5 O69 136.8(8) 1_545 .
O71 Na5 O69 68.2(12) . .
O70 Na5 O69 68.3(12) . .
O27 Na5 O64 151.1(4) 1_655 .
O18 Na5 O64 88.7(4) . .
O35 Na5 O64 69.2(4) 1_545 .
O71 Na5 O64 69.8(10) . .
O70 Na5 O64 51.9(10) . .
O69 Na5 O64 115.4(9) . .
O27 Na5 O63 70.2(4) 1_655 .
O18 Na5 O63 151.0(4) . .
O35 Na5 O63 86.4(4) 1_545 .
O71 Na5 O63 114.0(10) . .
O70 Na5 O63 66.5(10) . .
O69 Na5 O63 51.2(9) . .
O64 Na5 O63 112.5(5) . .
O27 Na5 O65 86.4(4) 1_655 .
O18 Na5 O65 69.1(4) . .
O35 Na5 O65 151.0(4) 1_545 .
O71 Na5 O65 52.3(10) . .
O70 Na5 O65 116.8(10) . .
O69 Na5 O65 69.3(9) . .
O64 Na5 O65 115.6(6) . .
O63 Na5 O65 114.8(6) . .
O27 Na5 Na6 49.82(16) 1_655 .
O18 Na5 Na6 49.47(17) . .
O35 Na5 Na6 49.15(17) 1_545 .
O71 Na5 Na6 140.8(10) . .
O70 Na5 Na6 138.3(10) . .
O69 Na5 Na6 138.9(8) . .
O64 Na5 Na6 104.1(4) . .
O63 Na5 Na6 104.1(4) . .
O65 Na5 Na6 104.1(4) . .
O27 Na5 Na9 42.56(17) 1_655 .
O18 Na5 Na9 111.9(2) . .
O35 Na5 Na9 59.37(18) 1_545 .
O71 Na5 Na9 154.1(10) . .
O70 Na5 Na9 97.1(10) . .
O69 Na5 Na9 86.4(8) . .
O64 Na5 Na9 120.1(4) . .
O63 Na5 Na9 40.7(4) . .
O65 Na5 Na9 124.4(4) . .
Na6 Na5 Na9 63.42(12) . .
O27 Na5 Na4 112.30(19) 1_655 .
O18 Na5 Na4 60.22(17) . .
O35 Na5 Na4 42.37(17) 1_545 .
O71 Na5 Na4 100.0(9) . .
O70 Na5 Na4 87.8(10) . .
O69 Na5 Na4 155.7(8) . .
O64 Na5 Na4 40.9(4) . .
O63 Na5 Na4 124.0(4) . .
O65 Na5 Na4 121.2(4) . .
Na6 Na5 Na4 63.23(12) . .
Na9 Na5 Na4 101.53(13) . .
O35 Na6 O18 82.7(2) 1_545 .
O35 Na6 O27 82.1(2) 1_545 1_655
O18 Na6 O27 80.9(2) . 1_655
O35 Na6 O50 122.5(3) 1_545 .
O18 Na6 O50 150.0(3) . .
O27 Na6 O50 86.5(2) 1_655 .
O35 Na6 O54 152.7(3) 1_545 .
O18 Na6 O54 86.4(2) . .
O27 Na6 O54 120.7(2) 1_655 .
O50 Na6 O54 76.8(2) . .
O35 Na6 O62 88.8(2) 1_545 .
O18 Na6 O62 123.2(2) . .
O27 Na6 O62 153.0(3) 1_655 .
O50 Na6 O62 77.0(2) . .
O54 Na6 O62 76.5(2) . .
O35 Na6 Na5 49.41(17) 1_545 .
O18 Na6 Na5 49.16(17) . .
O27 Na6 Na5 49.04(16) 1_655 .
O50 Na6 Na5 133.5(2) . .
O54 Na6 Na5 133.2(2) . .
O62 Na6 Na5 135.8(2) . .
O35 Na6 Na7 132.0(2) 1_545 .
O18 Na6 Na7 130.1(2) . .
O27 Na6 Na7 130.26(19) 1_655 .
O50 Na6 Na7 46.31(17) . .
O54 Na6 Na7 45.66(17) . .
O62 Na6 Na7 45.45(16) . .
Na5 Na6 Na7 178.61(17) . .
O35 Na6 Na9 62.16(18) 1_545 .
O18 Na6 Na9 116.33(18) . .
O27 Na6 Na9 45.37(17) 1_655 .
O50 Na6 Na9 70.12(19) . .
O54 Na6 Na9 144.19(19) . .
O62 Na6 Na9 108.2(2) . .
Na5 Na6 Na9 68.27(12) . .
Na7 Na6 Na9 112.18(13) . .
O35 Na6 Na4 45.37(17) 1_545 .
O18 Na6 Na4 63.22(17) . .
O27 Na6 Na4 116.83(18) 1_655 .
O50 Na6 Na4 145.6(2) . .
O54 Na6 Na4 107.58(19) . .
O62 Na6 Na4 71.29(17) . .
Na5 Na6 Na4 68.59(12) . .
Na7 Na6 Na4 112.31(13) . .
Na9 Na6 Na4 107.43(12) . .
O35 Na6 Na8 117.18(19) 1_545 .
O18 Na6 Na8 44.59(16) . .
O27 Na6 Na8 61.71(17) 1_655 .
O50 Na6 Na8 105.6(2) . .
O54 Na6 Na8 68.89(18) . .
O62 Na6 Na8 143.3(2) . .
Na5 Na6 Na8 68.58(13) . .
Na7 Na6 Na8 110.06(13) . .
Na9 Na6 Na8 106.94(11) . .
Na4 Na6 Na8 107.67(12) . .
O54 Na7 O62 86.0(3) . .
O54 Na7 O53 92.5(3) . .
O62 Na7 O53 85.5(3) . .
O54 Na7 O51 169.0(3) . .
O62 Na7 O51 88.8(3) . .
O53 Na7 O51 96.8(3) . .
O54 Na7 O50 82.2(3) . .
O62 Na7 O50 84.8(3) . .
O53 Na7 O50 169.3(3) . .
O51 Na7 O50 87.7(3) . .
O54 Na7 O52 90.8(2) . .
O62 Na7 O52 171.5(3) . .
O53 Na7 O52 102.5(3) . .
O51 Na7 O52 92.9(2) . .
O50 Na7 O52 86.9(2) . .
O54 Na7 Na6 50.4(2) . .
O62 Na7 Na6 53.3(2) . .
O53 Na7 Na6 121.0(3) . .
O51 Na7 Na6 119.1(2) . .
O50 Na7 Na6 48.71(19) . .
O52 Na7 Na6 118.94(19) . .
O54 Na7 Na2 136.5(2) . .
O62 Na7 Na2 134.3(2) . .
O53 Na7 Na2 104.4(3) . .
O51 Na7 Na2 46.15(16) . .
O50 Na7 Na2 85.7(2) . .
O52 Na7 Na2 46.80(17) . .
Na6 Na7 Na2 134.45(14) . .
O23 Na8 O38 81.0(2) 1_655 1_655
O23 Na8 O65 156.8(5) 1_655 .
O38 Na8 O65 80.3(5) 1_655 .
O23 Na8 O10 102.4(2) 1_655 .
O38 Na8 O10 175.9(2) 1_655 .
O65 Na8 O10 96.9(5) . .
O23 Na8 O37 101.5(2) 1_655 .
O38 Na8 O37 111.9(2) 1_655 .
O65 Na8 O37 98.2(5) . .
O10 Na8 O37 65.27(18) . .
O23 Na8 O18 105.7(2) 1_655 .
O38 Na8 O18 116.9(2) 1_655 .
O65 Na8 O18 71.2(5) . .
O10 Na8 O18 64.67(19) . .
O37 Na8 O18 126.8(2) . .
O23 Na8 Nb8 109.6(2) 1_655 .
O38 Na8 Nb8 141.7(2) 1_655 .
O65 Na8 Nb8 93.6(5) . .
O10 Na8 Nb8 35.03(13) . .
O37 Na8 Nb8 31.04(12) . .
O18 Na8 Nb8 96.13(16) . .
O23 Na8 Nb3 112.14(19) 1_655 .
O38 Na8 Nb3 146.1(2) 1_655 .
O65 Na8 Nb3 77.4(4) . .
O10 Na8 Nb3 34.65(13) . .
O37 Na8 Nb3 96.36(15) . .
O18 Na8 Nb3 30.82(13) . .
Nb8 Na8 Nb3 65.45(7) . .
O23 Na8 P2 21.84(14) 1_655 1_655
O38 Na8 P2 59.23(15) 1_655 1_655
O65 Na8 P2 136.9(5) . 1_655
O10 Na8 P2 124.23(17) . 1_655
O37 Na8 P2 109.50(17) . 1_655
O18 Na8 P2 112.71(18) . 1_655
Nb8 Na8 P2 126.82(12) . 1_655
Nb3 Na8 P2 128.98(12) . 1_655
O23 Na8 Nb5 75.65(17) 1_655 1_655
O38 Na8 Nb5 29.82(14) 1_655 1_655
O65 Na8 Nb5 81.3(5) . 1_655
O10 Na8 Nb5 153.11(19) . 1_655
O37 Na8 Nb5 141.62(17) . 1_655
O18 Na8 Nb5 89.72(17) . 1_655
Nb8 Na8 Nb5 170.61(13) . 1_655
Nb3 Na8 Nb5 120.51(12) . 1_655
P2 Na8 Nb5 56.47(7) 1_655 1_655
O23 Na8 Nb7 73.90(16) 1_655 1_655
O38 Na8 Nb7 27.79(14) 1_655 1_655
O65 Na8 Nb7 95.2(5) . 1_655
O10 Na8 Nb7 150.77(19) . 1_655
O37 Na8 Nb7 86.74(15) . 1_655
O18 Na8 Nb7 144.56(19) . 1_655
Nb8 Na8 Nb7 117.76(11) . 1_655
Nb3 Na8 Nb7 172.35(12) . 1_655
P2 Na8 Nb7 55.66(6) 1_655 1_655
Nb5 Na8 Nb7 55.35(6) 1_655 1_655
O23 Na8 Na6 71.54(19) 1_655 .
O38 Na8 Na6 92.79(19) 1_655 .
O65 Na8 Na6 95.7(5) . .
O10 Na8 Na6 90.55(17) . .
O37 Na8 Na6 153.31(18) . .
O18 Na8 Na6 39.19(15) . .
Nb8 Na8 Na6 125.54(12) . .
Nb3 Na8 Na6 64.66(9) . .
P2 Na8 Na6 73.87(10) 1_655 .
Nb5 Na8 Na6 63.14(9) 1_655 .
Nb7 Na8 Na6 114.58(11) 1_655 .
O34 Na9 O36 79.6(2) 1_545 1_545
O34 Na9 O63 156.8(5) 1_545 .
O36 Na9 O63 82.1(4) 1_545 .
O34 Na9 O2 100.0(2) 1_545 1_655
O36 Na9 O2 176.9(3) 1_545 1_655
O63 Na9 O2 99.0(4) . 1_655
O34 Na9 O1 98.8(2) 1_545 1_655
O36 Na9 O1 111.7(2) 1_545 1_655
O63 Na9 O1 101.2(4) . 1_655
O2 Na9 O1 65.21(19) 1_655 1_655
O34 Na9 O27 104.9(2) 1_545 1_655
O36 Na9 O27 118.7(2) 1_545 1_655
O63 Na9 O27 71.8(5) . 1_655
O2 Na9 O27 64.40(18) 1_655 1_655
O1 Na9 O27 127.0(2) 1_655 1_655
O34 Na9 Nb6 107.15(19) 1_545 1_655
O36 Na9 Nb6 142.0(2) 1_545 1_655
O63 Na9 Nb6 96.1(4) . 1_655
O2 Na9 Nb6 35.12(13) 1_655 1_655
O1 Na9 Nb6 31.07(12) 1_655 1_655
O27 Na9 Nb6 96.14(15) 1_655 1_655
O34 Na9 Nb5 110.7(2) 1_545 1_655
O36 Na9 Nb5 148.4(2) 1_545 1_655
O63 Na9 Nb5 78.6(4) . 1_655
O2 Na9 Nb5 34.56(13) 1_655 1_655
O1 Na9 Nb5 96.46(15) 1_655 1_655
O27 Na9 Nb5 30.77(12) 1_655 1_655
Nb6 Na9 Nb5 65.45(7) 1_655 1_655
O34 Na9 P3 21.14(14) 1_545 1_545
O36 Na9 P3 58.60(15) 1_545 1_545
O63 Na9 P3 137.6(4) . 1_545
O2 Na9 P3 121.12(17) 1_655 1_545
O1 Na9 P3 107.48(17) 1_655 1_545
O27 Na9 P3 111.59(17) 1_655 1_545
Nb6 Na9 P3 124.34(12) 1_655 1_545
Nb5 Na9 P3 126.89(12) 1_655 1_545
O34 Na9 Nb9 75.38(17) 1_545 1_545
O36 Na9 Nb9 30.04(14) 1_545 1_545
O63 Na9 Nb9 81.6(4) . 1_545
O2 Na9 Nb9 152.92(19) 1_655 1_545
O1 Na9 Nb9 141.55(18) 1_655 1_545
O27 Na9 Nb9 90.63(15) 1_655 1_545
Nb6 Na9 Nb9 171.80(13) 1_655 1_545
Nb5 Na9 Nb9 121.39(12) 1_655 1_545
P3 Na9 Nb9 56.50(7) 1_545 1_545
O34 Na9 Na6 70.57(19) 1_545 .
O36 Na9 Na6 92.30(18) 1_545 .
O63 Na9 Na6 96.1(4) . .
O2 Na9 Na6 90.49(17) 1_655 .
O1 Na9 Na6 151.95(18) 1_655 .
O27 Na9 Na6 40.06(14) 1_655 .
Nb6 Na9 Na6 125.52(12) 1_655 .
Nb5 Na9 Na6 65.41(9) 1_655 .
P3 Na9 Na6 72.14(10) 1_545 .
Nb9 Na9 Na6 62.65(8) 1_545 .
O34 Na9 Nb8 72.38(17) 1_545 1_545
O36 Na9 Nb8 27.14(14) 1_545 1_545
O63 Na9 Nb8 97.1(4) . 1_545
O2 Na9 Nb8 149.80(19) 1_655 1_545
O1 Na9 Nb8 86.69(16) 1_655 1_545
O27 Na9 Nb8 145.54(17) 1_655 1_545
Nb6 Na9 Nb8 117.76(12) 1_655 1_545
Nb5 Na9 Nb8 175.10(12) 1_655 1_545
P3 Na9 Nb8 55.11(7) 1_545 1_545
Nb9 Na9 Nb8 55.09(6) 1_545 1_545
Na6 Na9 Nb8 113.03(10) . 1_545
O17 Na10 O3 109.7(2) 2_566 .
O17 Na10 O11 137.9(3) 2_566 .
O3 Na10 O11 89.7(2) . .
O17 Na10 O5 85.5(2) 2_566 .
O3 Na10 O5 67.8(2) . .
O11 Na10 O5 67.3(2) . .
O17 Na10 O39 155.3(3) 2_566 .
O3 Na10 O39 66.73(19) . .
O11 Na10 O39 66.47(19) . .
O5 Na10 O39 113.4(2) . .
O17 Na10 O64 90.6(4) 2_566 .
O3 Na10 O64 131.4(5) . .
O11 Na10 O64 104.1(4) . .
O5 Na10 O64 160.2(5) . .
O39 Na10 O64 76.7(4) . .
O17 Na10 Nb3 166.6(2) 2_566 .
O3 Na10 Nb3 82.23(15) . .
O11 Na10 Nb3 32.70(13) . .
O5 Na10 Nb3 93.92(16) . .
O39 Na10 Nb3 34.76(12) . .
O64 Na10 Nb3 85.4(4) . .
O17 Na10 Nb6 133.9(2) 2_566 .
O3 Na10 Nb6 33.06(13) . .
O11 Na10 Nb6 81.58(15) . .
O5 Na10 Nb6 94.16(16) . .
O39 Na10 Nb6 34.53(13) . .
O64 Na10 Nb6 102.4(4) . .
Nb3 Na10 Nb6 59.41(6) . .
O17 Na10 Nb1 91.69(19) 2_566 .
O3 Na10 Nb1 35.23(14) . .
O11 Na10 Nb1 83.32(17) . .
O5 Na10 Nb1 34.03(13) . .
O39 Na10 Nb1 95.82(17) . .
O64 Na10 Nb1 165.8(4) . .
Nb3 Na10 Nb1 95.27(10) . .
Nb6 Na10 Nb1 66.26(7) . .
O17 Na10 Nb4 108.2(2) 2_566 .
O3 Na10 Nb4 84.40(17) . .
O11 Na10 Nb4 34.88(14) . .
O5 Na10 Nb4 34.26(13) . .
O39 Na10 Nb4 95.93(17) . .
O64 Na10 Nb4 131.5(4) . .
Nb3 Na10 Nb4 66.00(8) . .
Nb6 Na10 Nb4 95.68(10) . .
Nb1 Na10 Nb4 60.60(7) . .
O17 Na10 Na4 123.3(2) 2_566 .
O3 Na10 Na4 92.76(17) . .
O11 Na10 Na4 91.16(17) . .
O5 Na10 Na4 150.16(18) . .
O39 Na10 Na4 36.84(15) . .
O64 Na10 Na4 41.8(4) . .
Nb3 Na10 Na4 59.99(8) . .
Nb6 Na10 Na4 61.14(8) . .
Nb1 Na10 Na4 127.35(12) . .
Nb4 Na10 Na4 125.77(11) . .
O60 Na11 O61 93.4(4) . .
O60 Na11 O59 92.7(4) . .
O61 Na11 O59 93.4(4) . .
O60 Na11 O1 155.1(3) . 1_655
O61 Na11 O1 78.0(3) . 1_655
O59 Na11 O1 110.9(4) . 1_655
O60 Na11 O8 110.9(3) . 1_645
O61 Na11 O8 154.3(3) . 1_645
O59 Na11 O8 77.8(3) . 1_645
O1 Na11 O8 82.7(2) 1_655 1_645
O60 Na11 O37 78.6(2) . 1_545
O61 Na11 O37 111.7(4) . 1_545
O59 Na11 O37 153.6(3) . 1_545
O1 Na11 O37 83.1(2) 1_655 1_545
O8 Na11 O37 82.2(2) 1_645 1_545
O60 Na11 Na12 123.8(3) . .
O61 Na11 Na12 122.2(3) . .
O59 Na11 Na12 123.0(3) . .
O1 Na11 Na12 49.16(16) 1_655 .
O8 Na11 Na12 50.25(16) 1_645 .
O37 Na11 Na12 49.65(15) 1_545 .
O60 Na11 Na4 140.5(3) . 1_655
O61 Na11 Na4 114.7(3) . 1_655
O59 Na11 Na4 60.1(3) . 1_655
O1 Na11 Na4 62.72(16) 1_655 1_655
O8 Na11 Na4 40.18(15) 1_645 1_655
O37 Na11 Na4 112.53(17) 1_545 1_655
Na12 Na11 Na4 64.66(11) . 1_655
O60 Na11 Na9 115.4(3) . .
O61 Na11 Na9 60.1(3) . .
O59 Na11 Na9 140.9(3) . .
O1 Na11 Na9 40.23(15) 1_655 .
O8 Na11 Na9 112.93(17) 1_645 .
O37 Na11 Na9 63.50(16) 1_545 .
Na12 Na11 Na9 64.08(11) . .
Na4 Na11 Na9 102.89(11) 1_655 .
O60 Na11 Na8 61.3(3) . 1_545
O61 Na11 Na8 141.5(3) . 1_545
O59 Na11 Na8 114.8(3) . 1_545
O1 Na11 Na8 112.27(17) 1_655 1_545
O8 Na11 Na8 62.34(15) 1_645 1_545
O37 Na11 Na8 39.36(16) 1_545 1_545
Na12 Na11 Na8 64.41(11) . 1_545
Na4 Na11 Na8 102.42(11) 1_655 1_545
Na9 Na11 Na8 102.76(10) . 1_545
O1 Na12 O37 83.6(2) 1_655 1_545
O1 Na12 O8 82.6(2) 1_655 1_645
O37 Na12 O8 82.0(2) 1_545 1_645
O1 Na12 O55 124.7(2) 1_655 2_767
O37 Na12 O55 146.9(3) 1_545 2_767
O8 Na12 O55 84.9(2) 1_645 2_767
O1 Na12 O56 151.0(3) 1_655 2_767
O37 Na12 O56 86.2(2) 1_545 2_767
O8 Na12 O56 122.7(3) 1_645 2_767
O55 Na12 O56 75.6(2) 2_767 2_767
O1 Na12 O57 88.3(2) 1_655 2_767
O37 Na12 O57 126.3(2) 1_545 2_767
O8 Na12 O57 149.2(2) 1_645 2_767
O55 Na12 O57 76.2(2) 2_767 2_767
O56 Na12 O57 76.1(2) 2_767 2_767
O1 Na12 Na11 49.57(16) 1_655 .
O37 Na12 Na11 49.89(15) 1_545 .
O8 Na12 Na11 49.77(16) 1_645 .
O55 Na12 Na11 133.3(2) 2_767 .
O56 Na12 Na11 134.4(2) 2_767 .
O57 Na12 Na11 136.4(2) 2_767 .
O1 Na12 Na2 131.6(2) 1_655 2_767
O37 Na12 Na2 130.19(19) 1_545 2_767
O8 Na12 Na2 128.89(19) 1_645 2_767
O55 Na12 Na2 45.62(17) 2_767 2_767
O56 Na12 Na2 45.22(17) 2_767 2_767
O57 Na12 Na2 44.97(17) 2_767 2_767
Na11 Na12 Na2 178.53(17) . 2_767
O1 Na12 Na9 42.88(16) 1_655 .
O37 Na12 Na9 66.24(17) 1_545 .
O8 Na12 Na9 117.06(18) 1_645 .
O55 Na12 Na9 145.7(2) 2_767 .
O56 Na12 Na9 108.4(2) 2_767 .
O57 Na12 Na9 72.09(17) 2_767 .
Na11 Na12 Na9 68.78(11) . .
Na2 Na12 Na9 112.67(13) 2_767 .
O1 Na12 Na4 64.86(17) 1_655 1_655
O37 Na12 Na4 116.24(17) 1_545 1_655
O8 Na12 Na4 42.29(15) 1_645 1_655
O55 Na12 Na4 69.98(17) 2_767 1_655
O56 Na12 Na4 143.0(2) 2_767 1_655
O57 Na12 Na4 107.46(18) 2_767 1_655
Na11 Na12 Na4 68.24(11) . 1_655
Na2 Na12 Na4 111.24(12) 2_767 1_655
Na9 Na12 Na4 107.61(12) . 1_655
O1 Na12 Na8 117.16(18) 1_655 1_545
O37 Na12 Na8 41.96(16) 1_545 1_545
O8 Na12 Na8 64.87(16) 1_645 1_545
O55 Na12 Na8 105.1(2) 2_767 1_545
O56 Na12 Na8 69.29(18) 2_767 1_545
O57 Na12 Na8 143.52(19) 2_767 1_545
Na11 Na12 Na8 69.01(11) . 1_545
Na2 Na12 Na8 110.04(13) 2_767 1_545
Na9 Na12 Na8 108.04(11) . 1_545
Na4 Na12 Na8 107.01(12) 1_655 1_545
O66 Na13 O29 113.9(6) . .
O66 Na13 O22 127.0(6) . .
O29 Na13 O22 65.8(3) . .
O66 Na13 O24 79.8(5) . .
O29 Na13 O24 125.2(4) . .
O22 Na13 O24 64.8(3) . .
O66 Na13 O67 103.8(7) . .
O29 Na13 O67 91.4(4) . .
O22 Na13 O67 129.0(5) . .
O24 Na13 O67 138.8(4) . .
O66 Na13 O13 167.3(7) . .
O29 Na13 O13 66.2(3) . .
O22 Na13 O13 65.3(3) . .
O24 Na13 O13 110.9(4) . .
O67 Na13 O13 63.7(3) . .
O66 Na13 O19 131.7(6) . .
O29 Na13 O19 112.6(4) . .
O22 Na13 O19 64.3(3) . .
O24 Na13 O19 63.3(2) . .
O67 Na13 O19 87.1(4) . .
O13 Na13 O19 53.4(2) . .
O66 Na13 Na14 89.5(6) . .
O29 Na13 Na14 143.9(4) . .
O22 Na13 Na14 122.3(4) . .
O24 Na13 Na14 84.2(3) . .
O67 Na13 Na14 55.2(4) . .
O13 Na13 Na14 84.9(3) . .
O19 Na13 Na14 58.3(3) . .
O66 Na13 P4 151.9(6) . .
O29 Na13 P4 93.3(3) . .
O22 Na13 P4 69.7(3) . .
O24 Na13 P4 90.6(3) . .
O67 Na13 P4 66.7(3) . .
O13 Na13 P4 27.78(14) . .
O19 Na13 P4 27.86(14) . .
Na14 Na13 P4 63.0(3) . .
O66 Na13 Nb9 143.5(6) . .
O29 Na13 Nb9 38.57(18) . .
O22 Na13 Nb9 34.28(16) . .
O24 Na13 Nb9 98.9(3) . .
O67 Na13 Nb9 100.7(4) . .
O13 Na13 Nb9 44.16(18) . .
O19 Na13 Nb9 75.8(3) . .
Na14 Na13 Nb9 126.8(4) . .
P4 Na13 Nb9 63.87(18) . .
O66 Na13 Nb7 116.4(6) . .
O29 Na13 Nb7 98.9(3) . .
O22 Na13 Nb7 33.24(16) . .
O24 Na13 Nb7 37.87(17) . .
O67 Na13 Nb7 129.1(4) . .
O13 Na13 Nb7 75.5(3) . .
O19 Na13 Nb7 43.07(18) . .
Na14 Na13 Nb7 94.0(3) . .
P4 Na13 Nb7 63.13(18) . .
Nb9 Na13 Nb7 63.94(19) . .
O66 Na13 Na15 52.4(6) . .
O29 Na13 Na15 82.7(3) . .
O22 Na13 Na15 145.1(3) . .
O24 Na13 Na15 132.1(4) . .
O67 Na13 Na15 63.1(4) . .
O13 Na13 Na15 116.3(3) . .
O19 Na13 Na15 147.4(4) . .
Na14 Na13 Na15 91.9(4) . .
P4 Na13 Na15 129.4(3) . .
Nb9 Na13 Na15 120.4(2) . .
Nb7 Na13 Na15 167.4(3) . .
O68 Na14 O20 114.8(6) . .
O68 Na14 O2 128.9(6) . .
O20 Na14 O2 65.7(3) . .
O68 Na14 O33 82.5(6) . .
O20 Na14 O33 123.9(5) . .
O2 Na14 O33 63.1(3) . .
O68 Na14 O67 103.2(7) . .
O20 Na14 O67 91.6(4) . .
O2 Na14 O67 127.8(5) . .
O33 Na14 O67 138.3(5) . .
O68 Na14 O12 166.9(7) . .
O20 Na14 O12 65.8(3) . .
O2 Na14 O12 64.0(3) . .
O33 Na14 O12 108.4(4) . .
O67 Na14 O12 63.8(3) . .
O68 Na14 O19 132.3(6) . .
O20 Na14 O19 111.6(5) . .
O2 Na14 O19 63.3(3) . .
O33 Na14 O19 62.4(3) . .
O67 Na14 O19 86.0(4) . .
O12 Na14 O19 52.4(3) . .
O68 Na14 Na13 90.3(6) . .
O20 Na14 Na13 143.3(4) . .
O2 Na14 Na13 119.6(4) . .
O33 Na14 Na13 83.8(3) . .
O67 Na14 Na13 55.3(4) . .
O12 Na14 Na13 83.8(3) . .
O19 Na14 Na13 56.6(3) . .
O68 Na14 P4 151.7(6) . .
O20 Na14 P4 92.3(3) . .
O2 Na14 P4 68.5(3) . .
O33 Na14 P4 89.3(3) . .
O67 Na14 P4 66.1(3) . .
O12 Na14 P4 27.13(15) . .
O19 Na14 P4 27.53(15) . .
Na13 Na14 P4 61.8(3) . .
O68 Na14 Nb6 144.4(6) . .
O20 Na14 Nb6 38.2(2) . .
O2 Na14 Nb6 33.98(19) . .
O33 Na14 Nb6 96.9(4) . .
O67 Na14 Nb6 100.6(4) . .
O12 Na14 Nb6 43.8(2) . .
O19 Na14 Nb6 75.2(3) . .
Na13 Na14 Nb6 125.1(4) . .
P4 Na14 Nb6 63.3(2) . .
O68 Na14 Nb5 118.4(6) . .
O20 Na14 Nb5 98.1(4) . .
O2 Na14 Nb5 32.57(17) . .
O33 Na14 Nb5 36.87(19) . .
O67 Na14 Nb5 127.4(4) . .
O12 Na14 Nb5 73.7(3) . .
O19 Na14 Nb5 42.42(18) . .
Na13 Na14 Nb5 92.0(3) . .
P4 Na14 Nb5 62.0(2) . .
Nb6 Na14 Nb5 63.1(2) . .
O68 Na14 Na15 51.2(6) . 2_677
O20 Na14 Na15 83.9(3) . 2_677
O2 Na14 Na15 146.5(4) . 2_677
O33 Na14 Na15 133.6(4) . 2_677
O67 Na14 Na15 63.7(4) . 2_677
O12 Na14 Na15 117.3(3) . 2_677
O19 Na14 Na15 146.9(4) . 2_677
Na13 Na14 Na15 93.1(4) . 2_677
P4 Na14 Na15 129.5(3) . 2_677
Nb6 Na14 Na15 121.3(3) . 2_677
Nb5 Na14 Na15 168.4(3) . 2_677
O73 Na15 O73 71.9(6) . 2_677
O73 Na15 O74 64.7(8) . .
O73 Na15 O74 106.2(8) 2_677 .
O73 Na15 O31 116.8(6) . .
O73 Na15 O31 128.1(7) 2_677 .
O74 Na15 O31 124.1(8) . .
O73 Na15 O32 127.9(7) . 2_677
O73 Na15 O32 116.2(6) 2_677 2_677
O74 Na15 O32 63.8(7) . 2_677
O31 Na15 O32 98.0(4) . 2_677
O73 Na15 Na15 35.8(4) . 2_677
O73 Na15 Na15 36.1(4) 2_677 2_677
O74 Na15 Na15 84.7(8) . 2_677
O31 Na15 Na15 131.2(6) . 2_677
O32 Na15 Na15 130.8(5) 2_677 2_677
O73 Na15 Na14 119.6(5) . 2_677
O73 Na15 Na14 55.7(5) 2_677 2_677
O74 Na15 Na14 101.2(7) . 2_677
O31 Na15 Na14 118.4(5) . 2_677
O32 Na15 Na14 64.8(3) 2_677 2_677
Na15 Na15 Na14 87.6(5) 2_677 2_677
O73 Na15 Na13 55.7(5) . .
O73 Na15 Na13 119.5(5) 2_677 .
O74 Na15 Na13 78.5(7) . .
O31 Na15 Na13 65.2(3) . .
O32 Na15 Na13 119.0(5) 2_677 .
Na15 Na15 Na13 87.3(5) 2_677 .
Na14 Na15 Na13 175.0(3) 2_677 .
O40 P1 O32 111.7(4) . .
O40 P1 O21 110.0(3) . .
O32 P1 O21 109.3(3) . .
O40 P1 O20 110.6(3) . .
O32 P1 O20 109.6(3) . .
O21 P1 O20 105.5(3) . .
O40 P1 Na4 33.3(2) . .
O32 P1 Na4 145.0(3) . .
O21 P1 Na4 90.6(2) . .
O20 P1 Na4 91.4(2) . .
O25 P2 O23 112.3(3) . .
O25 P2 O24 108.4(3) . .
O23 P2 O24 110.4(3) . .
O25 P2 O33 109.1(3) . .
O23 P2 O33 110.1(3) . .
O24 P2 O33 106.4(3) . .
O25 P2 Na8 147.1(3) . 1_455
O23 P2 Na8 34.9(2) . 1_455
O24 P2 Na8 91.6(2) . 1_455
O33 P2 Na8 88.9(2) . 1_455
O31 P3 O34 111.6(3) . .
O31 P3 O29 109.5(3) . .
O34 P3 O29 110.3(3) . .
O31 P3 O30 109.1(3) . .
O34 P3 O30 110.6(3) . .
O29 P3 O30 105.5(3) . .
O31 P3 Na9 144.4(3) . 1_565
O34 P3 Na9 32.9(2) . 1_565
O29 P3 Na9 89.4(2) . 1_565
O30 P3 Na9 93.5(2) . 1_565
O12 P4 O13 110.3(3) . .
O12 P4 O19 109.8(3) . .
O13 P4 O19 109.5(3) . .
O12 P4 O16 109.0(3) . .
O13 P4 O16 109.1(3) . .
O19 P4 O16 109.1(3) . .
O12 P4 Na13 102.8(3) . .
O13 P4 Na13 57.2(2) . .
O19 P4 Na13 59.0(2) . .
O16 P4 Na13 148.1(3) . .
O12 P4 Na14 56.9(3) . .
O13 P4 Na14 102.1(3) . .
O19 P4 Na14 59.8(3) . .
O16 P4 Na14 148.7(3) . .
Na13 P4 Na14 55.2(3) . .
O17 Nb1 O5 102.5(2) . .
O17 Nb1 O14 98.8(2) . .
O5 Nb1 O14 92.1(2) . .
O17 Nb1 O4 100.0(2) . .
O5 Nb1 O4 157.2(2) . .
O14 Nb1 O4 87.8(2) . .
O17 Nb1 O3 101.4(2) . .
O5 Nb1 O3 88.6(2) . .
O14 Nb1 O3 159.1(2) . .
O4 Nb1 O3 83.6(2) . .
O17 Nb1 O16 169.6(2) . .
O5 Nb1 O16 72.65(19) . .
O14 Nb1 O16 72.54(19) . .
O4 Nb1 O16 85.6(2) . .
O3 Nb1 O16 87.8(2) . .
O17 Nb1 Na10 95.8(2) . .
O5 Nb1 Na10 45.96(18) . .
O14 Nb1 Na10 137.75(17) . .
O4 Nb1 Na10 128.16(18) . .
O3 Nb1 Na10 44.80(16) . .
O16 Nb1 Na10 87.35(14) . .
O17 Nb1 Na3 91.3(2) . 1_455
O5 Nb1 Na3 137.49(18) . 1_455
O14 Nb1 Na3 45.77(17) . 1_455
O4 Nb1 Na3 44.56(18) . 1_455
O3 Nb1 Na3 128.13(16) . 1_455
O16 Nb1 Na3 86.65(14) . 1_455
Na10 Nb1 Na3 170.97(8) . 1_455
O26 Nb2 O14 102.1(3) . .
O26 Nb2 O6 99.2(3) . .
O14 Nb2 O6 92.2(2) . .
O26 Nb2 O28 99.1(3) . .
O14 Nb2 O28 158.4(2) . .
O6 Nb2 O28 88.2(2) . .
O26 Nb2 O7 101.4(3) . .
O14 Nb2 O7 88.4(2) . .
O6 Nb2 O7 158.7(2) . .
O28 Nb2 O7 83.6(2) . .
O26 Nb2 O16 169.9(2) . .
O14 Nb2 O16 72.8(2) . .
O6 Nb2 O16 72.70(19) . .
O28 Nb2 O16 86.8(2) . .
O7 Nb2 O16 87.2(2) . .
O26 Nb2 Na3 95.5(2) . 1_455
O14 Nb2 Na3 46.22(18) . 1_455
O6 Nb2 Na3 138.07(18) . 1_455
O28 Nb2 Na3 127.80(17) . 1_455
O7 Nb2 Na3 44.38(16) . 1_455
O16 Nb2 Na3 87.13(13) . 1_455
O26 Nb2 Na1 91.5(2) . 2_676
O14 Nb2 Na1 137.53(18) . 2_676
O6 Nb2 Na1 45.64(17) . 2_676
O28 Nb2 Na1 44.88(16) . 2_676
O7 Nb2 Na1 128.35(16) . 2_676
O16 Nb2 Na1 87.02(14) . 2_676
Na3 Nb2 Na1 170.94(8) 1_455 2_676
O18 Nb3 O11 101.2(3) . .
O18 Nb3 O10 98.6(2) . .
O11 Nb3 O10 93.8(2) . .
O18 Nb3 O39 102.5(3) . .
O11 Nb3 O39 90.8(2) . .
O10 Nb3 O39 157.1(2) . .
O18 Nb3 O21 93.7(2) . .
O11 Nb3 O21 165.0(2) . .
O10 Nb3 O21 85.4(2) . .
O39 Nb3 O21 84.4(2) . .
O18 Nb3 O12 172.0(2) . .
O11 Nb3 O12 86.6(2) . .
O10 Nb3 O12 82.7(2) . .
O39 Nb3 O12 75.2(2) . .
O21 Nb3 O12 78.4(2) . .
O18 Nb3 Na8 50.9(2) . .
O11 Nb3 Na8 91.57(17) . .
O10 Nb3 Na8 49.09(17) . .
O39 Nb3 Na8 153.19(18) . .
O21 Nb3 Na8 99.13(15) . .
O12 Nb3 Na8 131.57(15) . .
O18 Nb3 Na10 97.51(19) . .
O11 Nb3 Na10 44.62(18) . .
O10 Nb3 Na10 137.71(17) . .
O39 Nb3 Na10 47.73(16) . .
O21 Nb3 Na10 132.13(16) . .
O12 Nb3 Na10 86.65(14) . .
Na8 Nb3 Na10 123.73(9) . .
O18 Nb3 Na4 68.5(2) . .
O11 Nb3 Na4 107.75(18) . .
O10 Nb3 Na4 156.42(17) . .
O39 Nb3 Na4 35.80(17) . .
O21 Nb3 Na4 76.26(17) . .
O12 Nb3 Na4 107.47(14) . .
Na8 Nb3 Na4 119.00(10) . .
Na10 Nb3 Na4 65.34(10) . .
O15 Nb4 O6 101.9(3) . .
O15 Nb4 O5 99.4(2) . .
O6 Nb4 O5 91.9(2) . .
O15 Nb4 O11 99.9(3) . .
O6 Nb4 O11 157.9(2) . .
O5 Nb4 O11 88.2(2) . .
O15 Nb4 O9 101.4(2) . .
O6 Nb4 O9 88.8(2) . .
O5 Nb4 O9 158.6(2) . .
O11 Nb4 O9 83.3(2) . .
O15 Nb4 O16 169.7(2) . .
O6 Nb4 O16 72.7(2) . .
O5 Nb4 O16 72.3(2) . .
O11 Nb4 O16 86.3(2) . .
O9 Nb4 O16 87.47(19) . .
O15 Nb4 Na1 95.0(2) . 2_676
O6 Nb4 Na1 46.19(17) . 2_676
O5 Nb4 Na1 137.76(18) . 2_676
O11 Nb4 Na1 128.03(17) . 2_676
O9 Nb4 Na1 44.89(17) . 2_676
O16 Nb4 Na1 87.47(14) . 2_676
O15 Nb4 Na10 91.4(2) . .
O6 Nb4 Na10 137.55(17) . .
O5 Nb4 Na10 45.94(18) . .
O11 Nb4 Na10 44.85(16) . .
O9 Nb4 Na10 128.11(17) . .
O16 Nb4 Na10 87.19(14) . .
Na1 Nb4 Na10 171.43(8) 2_676 .
O27 Nb5 O4 101.4(2) . .
O27 Nb5 O2 99.0(2) . .
O4 Nb5 O2 93.6(2) . .
O27 Nb5 O38 102.4(2) . .
O4 Nb5 O38 91.2(2) . .
O2 Nb5 O38 156.6(2) . .
O27 Nb5 O33 94.3(2) . .
O4 Nb5 O33 164.3(2) . .
O2 Nb5 O33 84.9(2) . .
O38 Nb5 O33 84.3(2) . .
O27 Nb5 O19 171.6(2) . .
O4 Nb5 O19 86.7(2) . .
O2 Nb5 O19 82.5(2) . .
O38 Nb5 O19 75.0(2) . .
O33 Nb5 O19 77.61(19) . .
O27 Nb5 Na9 50.8(2) . 1_455
O4 Nb5 Na9 90.70(18) . 1_455
O2 Nb5 Na9 49.92(16) . 1_455
O38 Nb5 Na9 152.92(16) . 1_455
O33 Nb5 Na9 100.12(16) . 1_455
O19 Nb5 Na9 132.11(16) . 1_455
O27 Nb5 Na3 97.4(2) . 1_455
O4 Nb5 Na3 44.87(19) . 1_455
O2 Nb5 Na3 137.78(16) . 1_455
O38 Nb5 Na3 47.95(16) . 1_455
O33 Nb5 Na3 132.26(17) . 1_455
O19 Nb5 Na3 86.81(15) . 1_455
Na9 Nb5 Na3 122.79(10) 1_455 1_455
O27 Nb5 Na14 122.2(2) . .
O4 Nb5 Na14 121.7(2) . .
O2 Nb5 Na14 46.8(2) . .
O38 Nb5 Na14 112.2(2) . .
O33 Nb5 Na14 47.8(2) . .
O19 Nb5 Na14 53.3(2) . .
Na9 Nb5 Na14 89.46(18) 1_455 .
Na3 Nb5 Na14 140.13(17) 1_455 .
O27 Nb5 Na8 68.3(2) . 1_455
O4 Nb5 Na8 109.19(19) . 1_455
O2 Nb5 Na8 155.40(16) . 1_455
O38 Nb5 Na8 36.29(16) . 1_455
O33 Nb5 Na8 75.60(17) . 1_455
O19 Nb5 Na8 107.19(15) . 1_455
Na9 Nb5 Na8 118.65(9) 1_455 1_455
Na3 Nb5 Na8 66.43(9) 1_455 1_455
Na14 Nb5 Na8 121.24(18) . 1_455
O1 Nb6 O3 100.6(2) . .
O1 Nb6 O2 99.2(2) . .
O3 Nb6 O2 93.6(2) . .
O1 Nb6 O39 103.4(3) . .
O3 Nb6 O39 90.8(2) . .
O2 Nb6 O39 155.8(2) . .
O1 Nb6 O20 93.4(2) . .
O3 Nb6 O20 165.8(2) . .
O2 Nb6 O20 86.2(2) . .
O39 Nb6 O20 83.8(2) . .
O1 Nb6 O12 172.0(2) . .
O3 Nb6 O12 87.3(2) . .
O2 Nb6 O12 81.6(2) . .
O39 Nb6 O12 74.9(2) . .
O20 Nb6 O12 78.66(19) . .
O1 Nb6 Na9 50.4(2) . 1_455
O3 Nb6 Na9 89.84(17) . 1_455
O2 Nb6 Na9 50.60(16) . 1_455
O39 Nb6 Na9 153.31(17) . 1_455
O20 Nb6 Na9 100.83(15) . 1_455
O12 Nb6 Na9 131.79(15) . 1_455
O1 Nb6 Na10 98.33(19) . .
O3 Nb6 Na10 44.49(18) . .
O2 Nb6 Na10 136.93(16) . .
O39 Nb6 Na10 47.65(16) . .
O20 Nb6 Na10 131.47(16) . .
O12 Nb6 Na10 86.28(14) . .
Na9 Nb6 Na10 122.70(9) 1_455 .
O1 Nb6 Na14 121.8(2) . .
O3 Nb6 Na14 124.3(2) . .
O2 Nb6 Na14 48.9(2) . .
O39 Nb6 Na14 110.1(2) . .
O20 Nb6 Na14 46.9(2) . .
O12 Nb6 Na14 52.99(19) . .
Na9 Nb6 Na14 91.33(16) 1_455 .
Na10 Nb6 Na14 139.21(16) . .
O1 Nb6 Na4 71.4(2) . .
O3 Nb6 Na4 107.12(18) . .
O2 Nb6 Na4 158.38(16) . .
O39 Nb6 Na4 33.88(17) . .
O20 Nb6 Na4 75.27(16) . .
O12 Nb6 Na4 105.13(14) . .
Na9 Nb6 Na4 121.55(9) 1_455 .
Na10 Nb6 Na4 64.62(9) . .
Na14 Nb6 Na4 118.89(17) . .
O8 Nb7 O7 100.7(2) . .
O8 Nb7 O22 98.4(2) . .
O7 Nb7 O22 94.0(2) . .
O8 Nb7 O38 103.4(2) . .
O7 Nb7 O38 90.8(2) . .
O22 Nb7 O38 156.3(2) . .
O8 Nb7 O24 94.0(2) . .
O7 Nb7 O24 165.1(2) . .
O22 Nb7 O24 85.7(2) . .
O38 Nb7 O24 83.9(2) . .
O8 Nb7 O19 171.5(2) . .
O7 Nb7 O19 87.8(2) . .
O22 Nb7 O19 82.1(2) . .
O38 Nb7 O19 75.0(2) . .
O24 Nb7 O19 77.5(2) . .
O8 Nb7 Na4 49.78(19) . 1_565
O7 Nb7 Na4 90.08(18) . 1_565
O22 Nb7 Na4 50.51(18) . 1_565
O38 Nb7 Na4 152.77(18) . 1_565
O24 Nb7 Na4 101.02(16) . 1_565
O19 Nb7 Na4 132.28(14) . 1_565
O8 Nb7 Na3 98.26(19) . 1_455
O7 Nb7 Na3 44.19(17) . 1_455
O22 Nb7 Na3 137.25(16) . 1_455
O38 Nb7 Na3 47.98(16) . 1_455
O24 Nb7 Na3 131.82(16) . 1_455
O19 Nb7 Na3 86.90(14) . 1_455
Na4 Nb7 Na3 122.25(10) 1_565 1_455
O8 Nb7 Na13 121.6(2) . .
O7 Nb7 Na13 122.5(2) . .
O22 Nb7 Na13 46.7(2) . .
O38 Nb7 Na13 112.3(2) . .
O24 Nb7 Na13 48.5(2) . .
O19 Nb7 Na13 53.02(19) . .
Na4 Nb7 Na13 89.91(16) 1_565 .
Na3 Nb7 Na13 139.91(16) 1_455 .
O8 Nb7 Na8 72.08(19) . 1_455
O7 Nb7 Na8 107.71(17) . 1_455
O22 Nb7 Na8 157.43(16) . 1_455
O38 Nb7 Na8 33.50(17) . 1_455
O24 Nb7 Na8 74.92(16) . 1_455
O19 Nb7 Na8 104.31(14) . 1_455
Na4 Nb7 Na8 121.57(10) 1_565 1_455
Na3 Nb7 Na8 65.25(9) 1_455 1_455
Na13 Nb7 Na8 120.52(15) . 1_455
O37 Nb8 O9 100.5(2) . .
O37 Nb8 O10 98.8(2) . .
O9 Nb8 O10 93.6(2) . .
O37 Nb8 O36 102.5(2) . .
O9 Nb8 O36 90.5(2) . .
O10 Nb8 O36 157.1(2) . .
O37 Nb8 O30 93.7(2) . .
O9 Nb8 O30 165.6(2) . .
O10 Nb8 O30 86.6(2) . .
O36 Nb8 O30 84.0(2) . .
O37 Nb8 O13 171.9(2) . .
O9 Nb8 O13 87.4(2) . .
O10 Nb8 O13 82.4(2) . .
O36 Nb8 O13 75.27(19) . .
O30 Nb8 O13 78.40(19) . .
O37 Nb8 Na8 50.5(2) . .
O9 Nb8 Na8 90.92(19) . .
O10 Nb8 Na8 49.79(17) . .
O36 Nb8 Na8 152.72(16) . .
O30 Nb8 Na8 100.05(16) . .
O13 Nb8 Na8 132.01(15) . .
O37 Nb8 Na1 97.81(19) . 2_676
O9 Nb8 Na1 44.10(18) . 2_676
O10 Nb8 Na1 136.78(16) . 2_676
O36 Nb8 Na1 47.67(16) . 2_676
O30 Nb8 Na1 131.68(16) . 2_676
O13 Nb8 Na1 86.48(14) . 2_676
Na8 Nb8 Na1 123.16(9) . 2_676
O37 Nb8 Na9 71.6(2) . 1_565
O9 Nb8 Na9 106.35(18) . 1_565
O10 Nb8 Na9 159.03(16) . 1_565
O36 Nb8 Na9 32.77(15) . 1_565
O30 Nb8 Na9 75.76(16) . 1_565
O13 Nb8 Na9 104.48(15) . 1_565
Na8 Nb8 Na9 121.83(9) . 1_565
Na1 Nb8 Na9 64.05(9) 2_676 1_565
O35 Nb9 O28 100.9(3) . .
O35 Nb9 O22 99.3(3) . .
O28 Nb9 O22 93.8(2) . .
O35 Nb9 O36 103.0(2) . .
O28 Nb9 O36 91.5(2) . .
O22 Nb9 O36 155.7(2) . .
O35 Nb9 O29 93.7(2) . .
O28 Nb9 O29 165.4(2) . .
O22 Nb9 O29 84.8(2) . .
O36 Nb9 O29 84.1(2) . .
O35 Nb9 O13 171.9(2) . .
O28 Nb9 O13 87.0(2) . .
O22 Nb9 O13 81.9(2) . .
O36 Nb9 O13 74.73(19) . .
O29 Nb9 O13 78.4(2) . .
O35 Nb9 Na4 51.0(2) . 1_565
O28 Nb9 Na4 90.52(19) . 1_565
O22 Nb9 Na4 50.04(18) . 1_565
O36 Nb9 Na4 153.70(17) . 1_565
O29 Nb9 Na4 99.62(16) . 1_565
O13 Nb9 Na4 131.57(14) . 1_565
O35 Nb9 Na1 97.9(2) . 2_676
O28 Nb9 Na1 44.96(17) . 2_676
O22 Nb9 Na1 137.79(16) . 2_676
O36 Nb9 Na1 47.96(16) . 2_676
O29 Nb9 Na1 132.07(16) . 2_676
O13 Nb9 Na1 86.33(14) . 2_676
Na4 Nb9 Na1 123.51(10) 1_565 2_676
O35 Nb9 Na13 122.6(2) . .
O28 Nb9 Na13 123.0(2) . .
O22 Nb9 Na13 48.0(2) . .
O36 Nb9 Na13 110.2(2) . .
O29 Nb9 Na13 47.1(2) . .
O13 Nb9 Na13 52.72(19) . .
Na4 Nb9 Na13 90.43(16) 1_565 .
Na1 Nb9 Na13 139.02(16) 2_676 .
O35 Nb9 Na9 68.0(2) . 1_565
O28 Nb9 Na9 108.14(17) . 1_565
O22 Nb9 Na9 156.08(16) . 1_565
O36 Nb9 Na9 36.68(17) . 1_565
O29 Nb9 Na9 76.26(16) . 1_565
O13 Nb9 Na9 107.96(14) . 1_565
Na4 Nb9 Na9 118.63(9) 1_565 1_565
Na1 Nb9 Na9 65.77(9) 2_676 1_565
Na13 Nb9 Na9 120.76(15) . 1_565
Nb6 O1 Na12 133.1(3) . 1_455
Nb6 O1 Na11 134.9(3) . 1_455
Na12 O1 Na11 81.3(2) 1_455 1_455
Nb6 O1 Na9 98.5(3) . 1_455
Na12 O1 Na9 99.1(2) 1_455 1_455
Na11 O1 Na9 103.7(2) 1_455 1_455
Nb5 O2 Nb6 141.1(3) . .
Nb5 O2 Na9 95.5(2) . 1_455
Nb6 O2 Na9 94.3(2) . 1_455
Nb5 O2 Na14 100.6(3) . .
Nb6 O2 Na14 97.1(3) . .
Na9 O2 Na14 137.6(3) 1_455 .
Nb6 O3 Nb1 145.6(3) . .
Nb6 O3 Na10 102.4(2) . .
Nb1 O3 Na10 100.0(2) . .
Nb5 O4 Nb1 147.7(3) . .
Nb5 O4 Na3 102.3(3) . 1_455
Nb1 O4 Na3 100.9(2) . 1_455
Nb1 O5 Nb4 124.6(3) . .
Nb1 O5 Na10 100.0(2) . .
Nb4 O5 Na10 99.8(2) . .
Nb4 O6 Nb2 124.3(3) . .
Nb4 O6 Na1 99.5(2) . 2_676
Nb2 O6 Na1 100.2(2) . 2_676
Nb7 O7 Nb2 145.4(3) . .
Nb7 O7 Na3 102.6(2) . 1_455
Nb2 O7 Na3 100.4(2) . 1_455
Nb7 O8 Na11 134.0(3) . 1_465
Nb7 O8 Na12 134.8(3) . 1_465
Na11 O8 Na12 80.0(2) 1_465 1_465
Nb7 O8 Na4 99.4(2) . 1_565
Na11 O8 Na4 103.3(2) 1_465 1_565
Na12 O8 Na4 99.0(2) 1_465 1_565
Nb8 O9 Nb4 145.8(3) . .
Nb8 O9 Na1 102.9(2) . 2_676
Nb4 O9 Na1 99.7(2) . 2_676
Nb8 O10 Nb3 140.7(3) . .
Nb8 O10 Na8 95.2(2) . .
Nb3 O10 Na8 96.3(2) . .
Nb3 O11 Nb4 147.3(3) . .
Nb3 O11 Na10 102.7(2) . .
Nb4 O11 Na10 100.3(2) . .
P4 O12 Nb3 127.2(3) . .
P4 O12 Nb6 128.2(3) . .
Nb3 O12 Nb6 90.15(19) . .
P4 O12 Na14 95.9(3) . .
Nb3 O12 Na14 127.1(3) . .
Nb6 O12 Na14 83.2(3) . .
P4 O13 Nb8 127.8(3) . .
P4 O13 Nb9 127.1(3) . .
Nb8 O13 Nb9 90.39(17) . .
P4 O13 Na13 95.0(3) . .
Nb8 O13 Na13 128.0(3) . .
Nb9 O13 Na13 83.1(3) . .
Nb2 O14 Nb1 124.1(3) . .
Nb2 O14 Na3 99.6(2) . 1_455
Nb1 O14 Na3 100.1(2) . 1_455
Nb4 O15 Na1 155.2(4) . .
P4 O16 Nb2 125.6(3) . .
P4 O16 Nb1 125.5(3) . .
Nb2 O16 Nb1 90.16(17) . .
P4 O16 Nb4 124.6(3) . .
Nb2 O16 Nb4 89.96(16) . .
Nb1 O16 Nb4 90.03(17) . .
Nb1 O17 Na10 156.4(3) . 2_566
Nb3 O18 Na5 135.8(3) . .
Nb3 O18 Na6 135.0(3) . .
Na5 O18 Na6 81.4(2) . .
Nb3 O18 Na8 98.2(3) . .
Na5 O18 Na8 101.7(2) . .
Na6 O18 Na8 96.2(2) . .
P4 O19 Nb7 127.5(3) . .
P4 O19 Nb5 126.5(3) . .
Nb7 O19 Nb5 90.37(18) . .
P4 O19 Na13 93.2(3) . .
Nb7 O19 Na13 83.9(3) . .
Nb5 O19 Na13 131.5(3) . .
P4 O19 Na14 92.7(3) . .
Nb7 O19 Na14 131.0(3) . .
Nb5 O19 Na14 84.3(3) . .
Na13 O19 Na14 65.0(3) . .
P1 O20 Nb6 127.5(3) . .
P1 O20 Na14 113.7(4) . .
Nb6 O20 Na14 94.9(3) . .
P1 O21 Nb3 127.0(3) . .
Nb7 O22 Nb9 140.6(3) . .
Nb7 O22 Na13 100.1(3) . .
Nb9 O22 Na13 97.7(3) . .
Nb7 O22 Na4 94.5(2) . 1_565
Nb9 O22 Na4 95.1(2) . 1_565
Na13 O22 Na4 138.3(3) . 1_565
P2 O23 Na8 123.3(3) . 1_455
P2 O24 Nb7 127.9(3) . .
P2 O24 Na13 115.8(4) . .
Nb7 O24 Na13 93.6(3) . .
Nb2 O26 Na3 155.5(4) . 2_676
Nb5 O27 Na5 136.9(3) . 1_455
Nb5 O27 Na6 135.4(3) . 1_455
Na5 O27 Na6 81.1(2) 1_455 1_455
Nb5 O27 Na9 98.4(3) . 1_455
Na5 O27 Na9 100.2(2) 1_455 1_455
Na6 O27 Na9 94.6(2) 1_455 1_455
Nb9 O28 Nb2 147.1(3) . .
Nb9 O28 Na1 102.2(2) . 2_676
Nb2 O28 Na1 100.2(2) . 2_676
P3 O29 Nb9 126.6(3) . .
P3 O29 Na13 115.1(4) . .
Nb9 O29 Na13 94.4(3) . .
P3 O30 Nb8 126.9(3) . .
P3 O31 Na15 139.8(4) . .
P1 O32 Na15 140.7(5) . 2_677
P2 O33 Nb5 127.7(3) . .
P2 O33 Na14 114.7(4) . .
Nb5 O33 Na14 95.3(3) . .
P3 O34 Na9 125.9(3) . 1_565
Nb9 O35 Na6 133.9(3) . 1_565
Nb9 O35 Na5 137.8(3) . 1_565
Na6 O35 Na5 81.4(2) 1_565 1_565
Nb9 O35 Na4 98.4(2) . 1_565
Na6 O35 Na4 95.1(2) 1_565 1_565
Na5 O35 Na4 100.4(3) 1_565 1_565
Nb9 O36 Nb8 119.4(2) . .
Nb9 O36 Na9 113.3(3) . 1_565
Nb8 O36 Na9 120.1(3) . 1_565
Nb9 O36 Na1 97.3(2) . 2_676
Nb8 O36 Na1 97.6(2) . 2_676
Na9 O36 Na1 102.1(2) 1_565 2_676
Nb8 O37 Na12 133.3(3) . 1_565
Nb8 O37 Na11 134.1(3) . 1_565
Na12 O37 Na11 80.46(19) 1_565 1_565
Nb8 O37 Na8 98.5(2) . .
Na12 O37 Na8 100.3(2) 1_565 .
Na11 O37 Na8 105.0(2) 1_565 .
Nb5 O38 Nb7 119.6(3) . .
Nb5 O38 Na8 113.9(2) . 1_455
Nb7 O38 Na8 118.7(3) . 1_455
Nb5 O38 Na3 97.4(2) . 1_455
Nb7 O38 Na3 97.1(2) . 1_455
Na8 O38 Na3 103.7(2) 1_455 1_455
Nb6 O39 Nb3 119.5(3) . .
Nb6 O39 Na4 118.3(3) . .
Nb3 O39 Na4 114.7(3) . .
Nb6 O39 Na10 97.8(2) . .
Nb3 O39 Na10 97.5(2) . .
Na4 O39 Na10 102.3(2) . .
P1 O40 Na4 125.6(4) . .
Na7 O50 Na6 85.0(2) . .
Na7 O51 Na2 87.8(2) . .
Na2 O52 Na7 86.3(2) . .
Na7 O54 Na6 84.0(3) . .
Na2 O55 Na12 85.2(3) . 2_767
Na2 O56 Na12 84.2(3) . 2_767
Na2 O57 Na12 81.7(3) . 2_767
Na7 O62 Na6 81.2(3) . .
Na9 O63 Na1 95.2(6) . 2_666
Na9 O63 Na5 91.5(6) . .
Na1 O63 Na5 105.9(6) 2_666 .
Na4 O64 Na10 94.8(6) . .
Na4 O64 Na5 91.5(6) . .
Na10 O64 Na5 102.9(6) . .
Na8 O65 Na3 97.0(7) . .
Na8 O65 Na5 91.5(6) . .
Na3 O65 Na5 103.9(7) . .
O72 O67 Na14 129(2) . .
O72 O67 Na13 137(2) . .
Na14 O67 Na13 69.5(4) . .
O67 O72 O75 169(4) . .
Na15 O73 Na15 108.1(6) . 2_677
O75 O74 Na15 96.7(14) 2_677 .
O72 O75 O76 165(3) . .
O72 O75 O74 110(2) . 2_677
O76 O75 O74 78.2(17) . 2_677
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Na1 O15 2.325(6) .
Na1 O9 2.464(7) 2_676
Na1 O28 2.486(6) 2_676
Na1 O6 2.518(7) 2_676
Na1 O36 2.575(6) 2_676
Na1 O63 2.650(19) 2_666
Na1 Nb9 3.439(4) 2_676
Na1 Nb4 3.442(4) 2_676
Na1 Nb8 3.452(4) 2_676
Na1 Nb2 3.467(4) 2_676
Na1 Na9 3.837(6) 2_666
Na2 O56 2.385(7) .
Na2 O57 2.387(8) .
Na2 O55 2.398(7) .
Na2 O58 2.397(8) .
Na2 O51 2.400(7) .
Na2 O52 2.429(7) .
Na2 Na7 3.325(5) .
Na2 Na12 3.343(5) 2_767
Na3 O26 2.321(7) 2_676
Na3 O7 2.461(6) 1_655
Na3 O4 2.487(7) 1_655
Na3 O14 2.534(7) 1_655
Na3 O38 2.579(6) 1_655
Na3 O65 2.62(2) .
Na3 Nb5 3.444(4) 1_655
Na3 Nb7 3.445(4) 1_655
Na3 Nb2 3.460(4) 1_655
Na3 Nb1 3.481(4) 1_655
Na3 Na8 3.879(5) .
Na4 O40 2.312(7) .
Na4 O39 2.357(7) .
Na4 O64 2.569(19) .
Na4 O8 2.630(7) 1_545
Na4 O22 2.631(7) 1_545
Na4 O35 2.685(7) 1_545
Na4 Nb7 3.399(4) 1_545
Na4 Nb9 3.420(4) 1_545
Na4 P1 3.424(4) .
Na4 Nb3 3.660(4) .
Na4 Nb6 3.723(4) .
Na4 Na6 3.758(5) .
Na5 O27 2.398(7) 1_655
Na5 O18 2.400(7) .
Na5 O35 2.409(7) 1_545
Na5 O71 2.59(4) .
Na5 O70 2.60(4) .
Na5 O69 2.73(4) .
Na5 O64 2.893(19) .
Na5 O63 2.891(19) .
Na5 O65 2.93(2) .
Na5 Na6 3.137(5) .
Na5 Na9 3.902(6) .
Na6 O35 2.400(7) 1_545
Na6 O18 2.412(7) .
Na6 O27 2.426(6) 1_655
Na6 O50 2.494(8) .
Na6 O54 2.562(9) .
Na6 O62 2.684(9) .
Na6 Na7 3.307(5) .
Na6 Na9 3.757(5) .
Na6 Na8 3.794(6) .
Na7 O54 2.378(8) .
Na7 O62 2.385(8) .
Na7 O53 2.396(9) .
Na7 O51 2.395(7) .
Na7 O50 2.400(7) .
Na7 O52 2.434(7) .
Na8 O23 2.337(7) 1_655
Na8 O38 2.350(6) 1_655
Na8 O65 2.56(2) .
Na8 O10 2.596(6) .
Na8 O37 2.641(7) .
Na8 O18 2.679(7) .
Na8 Nb8 3.385(4) .
Na8 Nb3 3.415(4) .
Na8 P2 3.417(4) 1_655
Na8 Nb5 3.630(4) 1_655
Na8 Nb7 3.734(4) 1_655
Na9 O34 2.299(7) 1_545
Na9 O36 2.356(6) 1_545
Na9 O63 2.545(18) .
Na9 O2 2.631(6) 1_655
Na9 O1 2.646(7) 1_655
Na9 O27 2.682(7) 1_655
Na9 Nb6 3.396(4) 1_655
Na9 Nb5 3.423(4) 1_655
Na9 P3 3.425(4) 1_545
Na9 Nb9 3.623(4) 1_545
Na9 Nb8 3.766(4) 1_545
Na10 O17 2.324(6) 2_566
Na10 O3 2.476(7) .
Na10 O11 2.482(7) .
Na10 O5 2.526(7) .
Na10 O39 2.574(6) .
Na10 O64 2.65(2) .
Na10 Nb3 3.448(4) .
Na10 Nb6 3.450(4) .
Na10 Nb1 3.460(4) .
Na10 Nb4 3.463(4) .
Na11 O60 2.358(9) .
Na11 O61 2.362(10) .
Na11 O59 2.382(10) .
Na11 O1 2.410(6) 1_655
Na11 O8 2.426(6) 1_645
Na11 O37 2.427(6) 1_545
Na11 Na12 3.130(5) .
Na11 Na4 3.968(5) 1_655
Na11 Na8 4.023(5) 1_545
Na12 O1 2.396(6) 1_655
Na12 O37 2.418(6) 1_545
Na12 O8 2.443(7) 1_645
Na12 O55 2.538(9) 2_767
Na12 O56 2.596(9) 2_767
Na12 O57 2.709(10) 2_767
Na12 Na2 3.343(5) 2_767
Na12 Na4 3.861(5) 1_655
Na12 Na8 3.886(6) 1_545
Na13 O66 2.27(2) .
Na13 O29 2.538(9) .
Na13 O22 2.591(12) .
Na13 O24 2.633(9) .
Na13 O67 2.683(17) .
Na13 O13 2.770(10) .
Na13 O19 2.817(10) .
Na13 Na14 3.057(13) .
Na13 P4 3.283(9) .
Na13 Nb9 3.456(10) .
Na13 Nb7 3.507(10) .
Na13 Na15 3.935(17) .
Na14 O68 2.21(2) .
Na14 O20 2.550(12) .
Na14 O2 2.643(14) .
Na14 O33 2.651(10) .
Na14 O67 2.679(16) .
Na14 O12 2.797(12) .
Na14 O19 2.871(12) .
Na14 P4 3.320(11) .
Na14 Nb6 3.478(12) .
Na14 Nb5 3.562(11) .
Na14 Na15 3.895(18) 2_677
Na15 O73 2.107(16) .
Na15 O73 2.095(17) 2_677
Na15 O74 2.35(3) .
Na15 O31 2.636(12) .
Na15 O32 2.640(12) 2_677
Na15 Na15 3.401(19) 2_677
Na15 Na14 3.895(18) 2_677
P1 O40 1.516(7) .
P1 O32 1.517(6) .
P1 O21 1.563(6) .
P1 O20 1.566(6) .
P2 O25 1.519(6) .
P2 O23 1.521(6) .
P2 O24 1.561(6) .
P2 O33 1.562(6) .
P2 Na8 3.417(4) 1_455
P3 O31 1.519(6) .
P3 O34 1.525(6) .
P3 O29 1.566(6) .
P3 O30 1.567(6) .
P3 Na9 3.425(4) 1_565
P4 O12 1.522(6) .
P4 O13 1.536(5) .
P4 O19 1.536(6) .
P4 O16 1.545(5) .
Nb1 O17 1.747(5) .
Nb1 O5 1.967(5) .
Nb1 O14 1.983(6) .
Nb1 O4 2.011(6) .
Nb1 O3 2.026(6) .
Nb1 O16 2.467(5) .
Nb1 Na3 3.481(4) 1_455
Nb2 O26 1.746(6) .
Nb2 O14 1.970(5) .
Nb2 O6 1.980(6) .
Nb2 O28 2.017(5) .
Nb2 O7 2.027(5) .
Nb2 O16 2.465(5) .
Nb2 Na3 3.460(4) 1_455
Nb2 Na1 3.467(4) 2_676
Nb3 O18 1.768(6) .
Nb3 O11 1.909(5) .
Nb3 O10 1.953(5) .
Nb3 O39 1.983(5) .
Nb3 O21 2.150(5) .
Nb3 O12 2.403(5) .
Nb4 O15 1.746(5) .
Nb4 O6 1.968(6) .
Nb4 O5 1.979(5) .
Nb4 O11 2.013(6) .
Nb4 O9 2.022(5) .
Nb4 O16 2.472(5) .
Nb4 Na1 3.442(4) 2_676
Nb5 O27 1.770(5) .
Nb5 O4 1.911(5) .
Nb5 O2 1.951(6) .
Nb5 O38 1.975(6) .
Nb5 O33 2.147(5) .
Nb5 O19 2.415(5) .
Nb5 Na9 3.423(4) 1_455
Nb5 Na3 3.444(4) 1_455
Nb5 Na8 3.630(4) 1_455
Nb6 O1 1.772(5) .
Nb6 O3 1.927(5) .
Nb6 O2 1.959(5) .
Nb6 O39 1.974(5) .
Nb6 O20 2.159(5) .
Nb6 O12 2.424(5) .
Nb6 Na9 3.396(4) 1_455
Nb7 O8 1.765(6) .
Nb7 O7 1.932(5) .
Nb7 O22 1.953(5) .
Nb7 O38 1.985(5) .
Nb7 O24 2.157(5) .
Nb7 O19 2.409(6) .
Nb7 Na4 3.399(4) 1_565
Nb7 Na3 3.445(4) 1_455
Nb7 Na8 3.734(4) 1_455
Nb8 O37 1.765(5) .
Nb8 O9 1.931(5) .
Nb8 O10 1.951(5) .
Nb8 O36 1.985(6) .
Nb8 O30 2.155(5) .
Nb8 O13 2.394(5) .
Nb8 Na1 3.452(4) 2_676
Nb8 Na9 3.766(4) 1_565
Nb9 O35 1.764(6) .
Nb9 O28 1.910(5) .
Nb9 O22 1.964(5) .
Nb9 O36 1.974(5) .
Nb9 O29 2.161(5) .
Nb9 O13 2.425(6) .
Nb9 Na4 3.420(4) 1_565
Nb9 Na1 3.439(4) 2_676
Nb9 Na9 3.623(4) 1_565
O1 Na12 2.395(6) 1_455
O1 Na11 2.410(6) 1_455
O1 Na9 2.646(7) 1_455
O2 Na9 2.631(6) 1_455
O4 Na3 2.487(7) 1_455
O6 Na1 2.518(7) 2_676
O7 Na3 2.461(6) 1_455
O8 Na11 2.426(6) 1_465
O8 Na12 2.443(7) 1_465
O8 Na4 2.630(7) 1_565
O9 Na1 2.464(7) 2_676
O14 Na3 2.534(7) 1_455
O17 Na10 2.324(6) 2_566
O22 Na4 2.631(7) 1_565
O23 Na8 2.337(7) 1_455
O26 Na3 2.321(7) 2_676
O27 Na5 2.397(7) 1_455
O27 Na6 2.426(6) 1_455
O27 Na9 2.682(7) 1_455
O28 Na1 2.486(6) 2_676
O32 Na15 2.640(12) 2_677
O34 Na9 2.299(7) 1_565
O35 Na6 2.400(7) 1_565
O35 Na5 2.409(7) 1_565
O35 Na4 2.685(7) 1_565
O36 Na9 2.356(6) 1_565
O36 Na1 2.575(6) 2_676
O37 Na12 2.418(6) 1_565
O37 Na11 2.427(6) 1_565
O38 Na8 2.350(6) 1_455
O38 Na3 2.579(6) 1_455
O55 Na12 2.538(9) 2_767
O56 Na12 2.596(9) 2_767
O57 Na12 2.709(9) 2_767
O63 Na1 2.650(19) 2_666
O67 O72 1.03(3) .
O72 O75 1.37(4) .
O73 Na15 2.095(17) 2_677
O74 O75 1.75(4) 2_677
O75 O76 1.68(4) .
O75 O74 1.75(4) 2_677
