#------------------------------------------------------------------------------
#$Date: 2016-03-23 20:48:37 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179425 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/22/4332259.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_4332259
loop_
_publ_author_name
'Krivovichev, Sergey V.'
'Siidra, Oleg I.'
'Nazarchuk, Evgenii V.'
'Burns, Peter C.'
'Depmeier, Wulf'
_publ_section_title
;
 Particular Topological Complexity of Lead Oxide Blocks in Pb31O22X18(X =
 Br, Cl)
;
_journal_issue                   10
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              3846
_journal_page_last               3848
_journal_paper_doi               10.1021/ic060166m
_journal_volume                  45
_journal_year                    2006
_chemical_formula_moiety         Pb31O22Br10Cl8
_chemical_formula_sum            'Br1.25 Cl O2.75 Pb3.88'
_chemical_formula_weight         982.20
_chemical_melting_point          973.15
_chemical_name_common            'lead oxide bromide/chloride'
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                93.104(2)
_cell_angle_beta                 95.809(2)
_cell_angle_gamma                111.2520(10)
_cell_formula_units_Z            16
_cell_length_a                   12.1192(7)
_cell_length_b                   16.2489(10)
_cell_length_c                   18.3007(11)
_cell_measurement_reflns_used    4055
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      68.768
_cell_measurement_theta_min      5.281
_cell_volume                     3325.4(3)
_computing_cell_refinement       'SMART (Bruker, 2003)'
_computing_data_collection       'SMART (Bruker, 2003)'
_computing_data_reduction        'SAINT (Bruker, 2003)'
_computing_molecular_graphics    'Atoms 5.1 (Dowty, 2000)'
_computing_publication_material  'WINGX (Farrugia, 2005)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 0.2
_diffrn_measured_fraction_theta_full 0.775
_diffrn_measured_fraction_theta_max 0.775
_diffrn_measurement_device_type  'SMART APEX diffractometer'
_diffrn_measurement_method       omega-scan
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0798
_diffrn_reflns_av_sigmaI/netI    0.1996
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            33290
_diffrn_reflns_theta_full        34.53
_diffrn_reflns_theta_max         34.53
_diffrn_reflns_theta_min         1.35
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count 100
_diffrn_standards_interval_time  10
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    84.502
_exptl_absorpt_correction_T_max  0.56242
_exptl_absorpt_correction_T_min  0.11855
_exptl_absorpt_correction_type   'semi-empirical (XPREP, Bruker 2003)'
_exptl_absorpt_process_details   'crystal modeled as (102) plate'
_exptl_crystal_colour            green
_exptl_crystal_density_diffrn    7.847
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             6408
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.01
_refine_diff_density_max         8.158
_refine_diff_density_min         -4.448
_refine_diff_density_rms         0.965
_refine_ls_extinction_coef       none
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.798
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     548
_refine_ls_number_reflns         21894
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.798
_refine_ls_R_factor_all          0.1604
_refine_ls_R_factor_gt           0.0655
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0241P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1211
_refine_ls_wR_factor_ref         0.1453
_reflns_number_gt                8416
_reflns_number_total             21894
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic060166msup1.cif
_cod_data_source_block           plate
_cod_depositor_comments
;
The following automatic conversions were performed:

'_chemical_melting_point' value '700oC' was changed to '973.15' - it
was converted from degrees Celsius(C) to Kelvins(K).

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4332259
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pb1 Pb 0.61446(12) 0.45159(7) 0.03075(7) 0.0180(3) Uani 1 1 d .
Pb2 Pb -0.00483(12) 0.02471(7) -0.34831(7) 0.0188(3) Uani 1 1 d .
Pb3 Pb 0.53736(12) 0.27575(6) -0.12757(7) 0.0184(3) Uani 1 1 d .
Pb4 Pb 0.62132(12) 0.52319(7) -0.15556(7) 0.0177(3) Uani 1 1 d .
Pb5 Pb 0.37988(12) 0.52336(7) 0.45660(8) 0.0219(3) Uani 1 1 d .
Pb6 Pb 0.75148(12) 0.04132(7) 0.28726(7) 0.0165(3) Uani 1 1 d .
Pb7 Pb 0.36486(12) 0.44799(7) 0.66475(7) 0.0194(3) Uani 1 1 d .
Pb8 Pb 0.87896(12) 0.53198(7) 0.21758(7) 0.0177(3) Uani 1 1 d .
Pb9 Pb 0.32969(12) 0.21018(7) -0.30889(7) 0.0190(3) Uani 1 1 d .
Pb10 Pb 0.49011(12) -0.03671(7) 0.09599(7) 0.0160(3) Uani 1 1 d .
Pb11 Pb 0.29582(12) 0.28417(6) 0.50836(7) 0.0183(3) Uani 1 1 d .
Pb12 Pb 0.30393(12) 0.29762(7) -0.01385(8) 0.0202(3) Uani 1 1 d .
Pb13 Pb 0.05764(11) 0.21822(6) 0.31983(7) 0.0162(3) Uani 1 1 d .
Pb14 Pb 0.26348(12) 0.04673(7) -0.47049(7) 0.0165(3) Uani 1 1 d .
Pb15 Pb 0.57854(11) 0.21295(6) 0.05576(7) 0.0177(3) Uani 1 1 d .
Pb16 Pb 0.12445(11) 0.45398(6) 0.27174(7) 0.0156(3) Uani 1 1 d .
Pb17 Pb 0.24411(11) -0.05561(6) 0.22513(7) 0.0175(3) Uani 1 1 d .
Pb18 Pb 0.17902(11) -0.20277(6) 0.05576(7) 0.0154(3) Uani 1 1 d .
Pb19 Pb 0.87556(12) 0.46924(7) -0.08663(7) 0.0173(3) Uani 1 1 d .
Pb20 Pb 1.17418(11) 0.70240(6) 0.26482(7) 0.0157(3) Uani 1 1 d .
Pb21 Pb 0.42529(12) -0.21303(6) 0.42053(8) 0.0186(3) Uani 1 1 d .
Pb22 Pb 0.49646(12) 0.03313(7) 0.40675(7) 0.0159(3) Uani 1 1 d .
Pb23 Pb -0.17247(12) 0.20291(6) 0.44875(7) 0.0167(3) Uani 1 1 d .
Pb24 Pb 0.95316(12) 0.71212(6) -0.10902(7) 0.0167(3) Uani 1 1 d .
Pb25 Pb -0.25626(12) -0.03538(7) -0.02074(7) 0.0195(3) Uani 1 1 d .
Pb26 Pb 0.81983(11) 0.28032(6) 0.23883(7) 0.0162(3) Uani 1 1 d .
Pb27 Pb 0.05618(11) 0.30245(6) 0.61475(7) 0.0173(3) Uani 1 1 d .
Pb28 Pb -0.10503(12) 0.45923(7) 0.40369(7) 0.0197(3) Uani 1 1 d .
Pb29 Pb -0.05066(11) -0.22237(6) 0.17747(7) 0.0159(3) Uani 1 1 d .
Pb30 Pb 0.01769(12) -0.01998(7) -0.16017(7) 0.0188(3) Uani 1 1 d .
Pb31 Pb 0.43880(13) 0.24886(7) 0.28102(8) 0.0259(3) Uani 1 1 d .
Br1 Br 0.3466(4) 0.3777(2) -0.1597(3) 0.0111(9) Uani 0.40 1 d P
Br2 Br 0.0153(4) 0.1222(2) 0.4768(3) 0.0179(10) Uani 0.50 1 d P
Br3 Br 0.4698(4) -0.1227(2) 0.2770(3) 0.0146(10) Uani 0.39 1 d P
Br4 Br 0.1077(5) 0.3801(3) 0.4555(3) 0.0467(14) Uani 0.80 1 d P
Br5 Br -0.1003(5) -0.3856(3) 0.0504(3) 0.0126(11) Uani 0.28 1 d P
Br6 Br -0.2270(5) 0.1113(3) 0.0985(3) 0.0428(12) Uani 0.87 1 d P
Br7 Br 0.2188(5) -0.1221(3) 0.3873(3) 0.0108(10) Uani 0.30 1 d P
Br8 Br 1.1336(5) 0.6273(3) -0.0871(3) 0.0242(12) Uani 0.42 1 d P
Br9 Br 0.5912(4) 0.3801(2) -0.2989(3) 0.0199(11) Uani 0.48 1 d P
Br10 Br 0.2577(5) 0.1127(3) -0.1481(3) 0.0242(12) Uani 0.46 1 d P
Br11 Br 0.6001(5) 0.3772(3) 0.2046(3) 0.0448(16) Uani 0.68 1 d P
Br12 Br -0.0110(6) -0.1121(3) 0.0305(4) 0.0425(17) Uani 0.44 1 d P
Br13 Br 0.5202(6) 0.1204(3) 0.2284(3) 0.0432(16) Uani 0.59 1 d P
Br14 Br 0.2645(6) 0.1190(3) 0.3544(4) 0.0331(16) Uani 0.37 1 d P
Br15 Br 0.1265(6) 0.5997(3) 0.4090(4) 0.0312(15) Uani 0.30 1 d P
Br16 Br 0.6184(4) 0.2933(3) 0.4177(3) 0.0558(12) Uani 1 1 d .
Br17 Br 0.2559(5) 0.2035(3) 0.1470(3) 0.0613(13) Uani 1 1 d .
Br18 Br 0.3636(8) 0.3897(4) 0.3494(5) 0.092(3) Uani 0.72 1 d P
Cl1 Cl 0.3466(4) 0.3777(2) -0.1597(3) 0.0111(9) Uani 0.60 1 d P
Cl2 Cl 0.0153(4) 0.1222(2) 0.4768(3) 0.0179(10) Uani 0.50 1 d P
Cl3 Cl 0.4698(4) -0.1227(2) 0.2770(3) 0.0146(10) Uani 0.61 1 d P
Cl4 Cl 0.1077(5) 0.3801(3) 0.4555(3) 0.0467(14) Uani 0.20 1 d P
Cl5 Cl -0.1003(5) -0.3856(3) 0.0504(3) 0.0126(11) Uani 0.72 1 d P
Cl6 Cl -0.2270(5) 0.1113(3) 0.0985(3) 0.0428(12) Uani 0.13 1 d P
Cl7 Cl 0.2188(5) -0.1221(3) 0.3873(3) 0.0108(10) Uani 0.70 1 d P
Cl8 Cl 1.1336(5) 0.6273(3) -0.0871(3) 0.0242(12) Uani 0.58 1 d P
Cl9 Cl 0.5912(4) 0.3801(2) -0.2989(3) 0.0199(11) Uani 0.52 1 d P
Cl10 Cl 0.2577(5) 0.1127(3) -0.1481(3) 0.0242(12) Uani 0.54 1 d P
Cl11 Cl 0.6001(5) 0.3772(3) 0.2046(3) 0.0448(16) Uani 0.32 1 d P
Cl12 Cl -0.0110(6) -0.1121(3) 0.0305(4) 0.0425(17) Uani 0.56 1 d P
Cl13 Cl 0.5202(6) 0.1204(3) 0.2284(3) 0.0432(16) Uani 0.41 1 d P
Cl14 Cl 0.2645(6) 0.1190(3) 0.3544(4) 0.0331(16) Uani 0.63 1 d P
Cl15 Cl 0.1265(6) 0.5997(3) 0.4090(4) 0.0312(15) Uani 0.70 1 d P
Cl16 Cl 0.3636(8) 0.3897(4) 0.3494(5) 0.092(3) Uani 0.28 1 d P
O1 O 0.4087(18) 0.4351(10) 0.0379(11) 0.016(4) Uiso 1 1 d .
O2 O 0.4155(18) 0.4348(10) 0.5410(11) 0.016(4) Uiso 1 1 d .
O3 O 1.085(2) 0.5608(11) 0.2073(12) 0.022(4) Uiso 1 1 d .
O4 O -0.0393(19) 0.0703(11) -0.2241(12) 0.021(4) Uiso 1 1 d .
O5 O 0.830(2) 0.5757(11) -0.1498(12) 0.023(5) Uiso 1 1 d .
O6 O 0.2109(19) 0.0688(11) -0.3502(12) 0.017(4) Uiso 1 1 d .
O7 O -0.0812(18) 0.4230(10) 0.2904(11) 0.017(4) Uiso 1 1 d .
O8 O 0.4580(16) 0.0686(9) 0.0197(10) 0.008(3) Uiso 1 1 d .
O9 O 0.152(2) -0.2011(11) 0.1787(12) 0.023(5) Uiso 1 1 d .
O10 O -0.299(2) 0.0661(12) 0.4058(13) 0.024(5) Uiso 1 1 d .
O11 O 0.519(2) -0.0757(11) 0.4723(12) 0.023(5) Uiso 1 1 d .
O12 O 0.043(2) -0.0684(11) -0.2678(12) 0.022(4) Uiso 1 1 d .
O13 O 0.2806(17) -0.0564(9) 0.0964(10) 0.010(3) Uiso 1 1 d .
O14 O 0.6611(19) 0.4170(11) -0.0948(12) 0.018(4) Uiso 1 1 d .
O15 O 0.173(2) 0.4485(12) 0.6486(13) 0.031(5) Uiso 1 1 d .
O16 O 1.006(2) 0.2895(11) 0.2227(12) 0.024(5) Uiso 1 1 d .
O17 O 0.9787(18) 0.6867(10) 0.2664(11) 0.016(4) Uiso 1 1 d .
O18 O 0.393(2) 0.2081(12) -0.4219(13) 0.029(5) Uiso 1 1 d .
O19 O 0.250(2) 0.3008(11) 0.6249(12) 0.023(5) Uiso 1 1 d .
O20 O -0.1337(18) 0.2022(10) 0.3330(11) 0.017(4) Uiso 1 1 d .
O21 O 0.479(2) 0.2894(11) -0.0138(12) 0.023(4) Uiso 1 1 d .
O22 O 0.6316(19) 0.1975(11) -0.0568(12) 0.019(4) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Pb1 O1 76.6(6) 2_665 .
O1 Pb1 O14 75.8(6) 2_665 .
O1 Pb1 O14 115.6(7) . .
O1 Pb1 O21 118.1(7) 2_665 .
O1 Pb1 O21 71.7(6) . .
O14 Pb1 O21 72.5(6) . .
O1 Pb1 Pb4 38.3(5) 2_665 .
O1 Pb1 Pb4 95.3(5) . .
O14 Pb1 Pb4 37.6(4) . .
O21 Pb1 Pb4 93.9(5) . .
O1 Pb1 Pb12 95.7(5) 2_665 .
O1 Pb1 Pb12 36.3(4) . .
O14 Pb1 Pb12 91.6(5) . .
O21 Pb1 Pb12 35.8(5) . .
Pb4 Pb1 Pb12 92.06(4) . .
O12 Pb2 O6 77.8(6) . .
O12 Pb2 O4 73.4(6) . .
O6 Pb2 O4 108.5(7) . .
O12 Pb2 Br14 82.6(5) . 2
O6 Pb2 Br14 152.3(4) . 2
O4 Pb2 Br14 83.9(5) . 2
O12 Pb2 Br2 85.0(5) . 2
O6 Pb2 Br2 82.4(5) . 2
O4 Pb2 Br2 152.6(4) . 2
Br14 Pb2 Br2 76.65(14) 2 2
O12 Pb2 Pb30 36.3(5) . .
O6 Pb2 Pb30 92.3(5) . .
O4 Pb2 Pb30 37.1(4) . .
Br14 Pb2 Pb30 82.90(13) 2 .
Br2 Pb2 Pb30 120.02(8) 2 .
O12 Pb2 Pb6 40.2(5) . 2_655
O6 Pb2 Pb6 38.3(4) . 2_655
O4 Pb2 Pb6 96.9(5) . 2_655
Br14 Pb2 Pb6 117.50(11) 2 2_655
Br2 Pb2 Pb6 75.86(9) 2 2_655
Pb30 Pb2 Pb6 65.19(3) . 2_655
O14 Pb3 O21 83.0(7) . .
O14 Pb3 O22 101.7(7) . .
O21 Pb3 O22 77.4(7) . .
O14 Pb3 Pb15 92.6(5) . .
O21 Pb3 Pb15 39.9(5) . .
O22 Pb3 Pb15 37.5(5) . .
O14 Pb4 O1 81.3(6) . 2_665
O14 Pb4 O5 79.6(7) . .
O1 Pb4 O5 103.5(8) 2_665 .
O14 Pb4 Pb19 40.6(5) . .
O1 Pb4 Pb19 93.0(5) 2_665 .
O5 Pb4 Pb19 38.9(4) . .
O14 Pb4 Pb1 42.3(5) . .
O1 Pb4 Pb1 39.1(4) 2_665 .
O5 Pb4 Pb1 95.2(5) . .
Pb19 Pb4 Pb1 65.40(4) . .
O2 Pb5 O2 80.1(6) . 2_666
O2 Pb5 Br18 86.4(5) . .
O2 Pb5 Br18 85.4(5) 2_666 .
O2 Pb5 Pb5 40.4(5) . 2_666
O2 Pb5 Pb5 39.7(4) 2_666 2_666
Br18 Pb5 Pb5 84.67(19) . 2_666
O6 Pb6 O10 77.6(7) 2_655 1_655
O6 Pb6 O12 78.4(6) 2_655 2_655
O10 Pb6 O12 121.4(8) 1_655 2_655
O6 Pb6 O20 119.4(7) 2_655 1_655
O10 Pb6 O20 72.3(6) 1_655 1_655
O12 Pb6 O20 74.9(6) 2_655 1_655
O6 Pb6 Pb23 95.6(5) 2_655 1_655
O10 Pb6 Pb23 36.3(5) 1_655 1_655
O12 Pb6 Pb23 95.5(5) 2_655 1_655
O20 Pb6 Pb23 36.6(4) 1_655 1_655
O6 Pb6 Pb2 40.7(5) 2_655 2_655
O10 Pb6 Pb2 97.1(6) 1_655 2_655
O12 Pb6 Pb2 38.5(4) 2_655 2_655
O20 Pb6 Pb2 93.0(5) 1_655 2_655
Pb23 Pb6 Pb2 91.10(4) 1_655 2_655
O15 Pb7 O19 77.4(7) . .
O15 Pb7 O2 105.1(8) . .
O19 Pb7 O2 78.1(6) . .
O15 Pb7 Pb11 91.4(6) . .
O19 Pb7 Pb11 38.0(5) . .
O2 Pb7 Pb11 40.2(4) . .
O15 Pb7 Pb27 38.0(5) . .
O19 Pb7 Pb27 39.4(5) . .
O2 Pb7 Pb27 93.8(5) . .
Pb11 Pb7 Pb27 62.39(4) . .
O3 Pb8 O7 77.4(6) . 1_655
O3 Pb8 O17 76.6(6) . .
O7 Pb8 O17 116.6(7) 1_655 .
O3 Pb8 O15 115.9(8) . 2_666
O7 Pb8 O15 70.5(6) 1_655 2_666
O17 Pb8 O15 71.0(6) . 2_666
O3 Pb8 Pb20 38.4(5) . .
O7 Pb8 Pb20 95.6(5) 1_655 .
O17 Pb8 Pb20 38.5(5) . .
O15 Pb8 Pb20 91.5(5) 2_666 .
O3 Pb8 Pb28 94.1(5) . 1_655
O7 Pb8 Pb28 35.3(5) 1_655 1_655
O17 Pb8 Pb28 91.2(4) . 1_655
O15 Pb8 Pb28 35.7(5) 2_666 1_655
Pb20 Pb8 Pb28 90.01(4) . 1_655
O6 Pb9 O18 82.6(7) . .
O6 Pb9 O19 105.8(7) . 1_554
O18 Pb9 O19 75.4(7) . 1_554
O6 Pb9 Pb11 91.7(5) . 1_554
O18 Pb9 Pb11 38.2(5) . 1_554
O19 Pb9 Pb11 37.5(5) 1_554 1_554
O6 Pb9 Pb14 39.0(5) . .
O18 Pb9 Pb14 43.6(5) . .
O19 Pb9 Pb14 92.5(5) 1_554 .
Pb11 Pb9 Pb14 62.05(3) 1_554 .
O8 Pb10 O8 74.2(6) 2_655 .
O8 Pb10 O13 115.0(7) 2_655 .
O8 Pb10 O13 74.3(5) . .
O8 Pb10 O22 73.5(6) 2_655 2_655
O8 Pb10 O22 117.0(6) . 2_655
O13 Pb10 O22 72.9(6) . 2_655
O8 Pb10 Pb25 94.7(4) 2_655 2
O8 Pb10 Pb25 38.7(4) . 2
O13 Pb10 Pb25 35.6(4) . 2
O22 Pb10 Pb25 93.2(5) 2_655 2
O8 Pb10 Pb15 36.8(4) 2_655 2_655
O8 Pb10 Pb15 95.1(4) . 2_655
O13 Pb10 Pb15 93.1(4) . 2_655
O22 Pb10 Pb15 36.8(4) 2_655 2_655
Pb25 Pb10 Pb15 93.06(4) 2 2_655
O19 Pb11 O18 75.7(7) . 1_556
O19 Pb11 O2 80.3(6) . .
O18 Pb11 O2 104.1(7) 1_556 .
O19 Pb11 Pb7 38.7(5) . .
O18 Pb11 Pb7 89.0(6) 1_556 .
O2 Pb11 Pb7 41.6(5) . .
O19 Pb11 Pb9 38.9(5) . 1_556
O18 Pb11 Pb9 37.2(5) 1_556 1_556
O2 Pb11 Pb9 96.7(5) . 1_556
Pb7 Pb11 Pb9 62.99(3) . 1_556
O21 Pb12 O1 83.6(7) . .
O21 Pb12 Br1 85.7(5) . .
O1 Pb12 Br1 85.2(5) . .
O21 Pb12 Pb1 43.9(5) . .
O1 Pb12 Pb1 40.1(5) . .
Br1 Pb12 Pb1 79.36(10) . .
O20 Pb13 O16 77.0(7) . 1_455
O20 Pb13 O12 80.5(7) . 2
O16 Pb13 O12 98.9(7) 1_455 2
O20 Pb13 Pb26 39.4(4) . 1_455
O16 Pb13 Pb26 37.7(5) 1_455 1_455
O12 Pb13 Pb26 91.5(5) 2 1_455
O10 Pb14 O6 76.1(7) 2 .
O10 Pb14 O11 74.7(6) 2 2_655
O6 Pb14 O11 114.2(8) . 2_655
O10 Pb14 O18 116.8(8) 2 .
O6 Pb14 O18 74.2(6) . .
O11 Pb14 O18 69.1(7) 2_655 .
O10 Pb14 Pb9 96.6(5) 2 .
O6 Pb14 Pb9 36.5(4) . .
O11 Pb14 Pb9 91.7(5) 2_655 .
O18 Pb14 Pb9 37.7(5) . .
O22 Pb15 O8 80.0(6) . .
O22 Pb15 O21 78.1(7) . .
O8 Pb15 O21 101.4(7) . .
O22 Pb15 Pb3 39.6(5) . .
O8 Pb15 Pb3 91.8(4) . .
O21 Pb15 Pb3 38.6(5) . .
O22 Pb15 Pb10 42.0(4) . 2_655
O8 Pb15 Pb10 38.1(4) . 2_655
O21 Pb15 Pb10 92.3(5) . 2_655
Pb3 Pb15 Pb10 63.98(3) . 2_655
O3 Pb16 O5 77.3(7) 1_455 2_665
O3 Pb16 O7 79.2(6) 1_455 .
O5 Pb16 O7 119.4(8) 2_665 .
O3 Pb16 O16 117.4(8) 1_455 1_455
O5 Pb16 O16 69.8(6) 2_665 1_455
O7 Pb16 O16 73.5(6) . 1_455
O3 Pb16 Pb19 38.8(5) 1_455 2_665
O5 Pb16 Pb19 38.4(4) 2_665 2_665
O7 Pb16 Pb19 100.5(5) . 2_665
O16 Pb16 Pb19 93.4(5) 1_455 2_665
O9 Pb17 O4 80.5(7) . 2
O9 Pb17 O13 75.7(6) . .
O4 Pb17 O13 106.3(7) 2 .
O9 Pb17 Br7 87.5(5) . .
O4 Pb17 Br7 84.5(5) 2 .
O13 Pb17 Br7 158.0(4) . .
O9 Pb17 Pb29 39.6(5) . .
O4 Pb17 Pb29 40.9(4) 2 .
O13 Pb17 Pb29 91.5(4) . .
Br7 Pb17 Pb29 84.23(10) . .
O9 Pb17 Pb18 37.7(5) . .
O4 Pb17 Pb18 93.0(5) 2 .
O13 Pb17 Pb18 38.0(4) . .
Br7 Pb17 Pb18 124.26(9) . .
Pb29 Pb17 Pb18 60.95(3) . .
O22 Pb18 O13 80.6(6) 2_655 .
O22 Pb18 O9 104.0(8) 2_655 .
O13 Pb18 O9 78.4(6) . .
O22 Pb18 Br12 150.1(4) 2_655 .
O13 Pb18 Br12 74.9(5) . .
O9 Pb18 Br12 87.7(5) . .
O22 Pb18 Pb17 94.7(5) 2_655 .
O13 Pb18 Pb17 41.1(4) . .
O9 Pb18 Pb17 37.3(4) . .
Br12 Pb18 Pb17 77.89(13) . .
O22 Pb18 Pb29 141.9(5) 2_655 .
O13 Pb18 Pb29 92.2(4) . .
O9 Pb18 Pb29 38.2(6) . .
Br12 Pb18 Pb29 56.99(11) . .
Pb17 Pb18 Pb29 58.93(3) . .
O22 Pb18 Pb24 122.6(5) 2_655 1_445
O13 Pb18 Pb24 125.5(5) . 1_445
O9 Pb18 Pb24 129.0(6) . 1_445
Br12 Pb18 Pb24 62.77(13) . 1_445
Pb17 Pb18 Pb24 140.10(4) . 1_445
Pb29 Pb18 Pb24 92.05(4) . 1_445
O5 Pb19 O3 77.9(7) . 2_765
O5 Pb19 O14 77.1(6) . .
O3 Pb19 O14 105.1(8) 2_765 .
O5 Pb19 Pb4 39.3(5) . .
O3 Pb19 Pb4 92.5(5) 2_765 .
O14 Pb19 Pb4 37.8(4) . .
O5 Pb19 Pb16 40.2(5) . 2_665
O3 Pb19 Pb16 37.7(4) 2_765 2_665
O14 Pb19 Pb16 92.7(5) . 2_665
Pb4 Pb19 Pb16 63.46(3) . 2_665
O17 Pb20 O3 81.5(7) . .
O17 Pb20 O9 78.0(6) . 1_665
O3 Pb20 O9 107.0(7) . 1_665
O17 Pb20 Br15 81.7(5) . 1_655
O3 Pb20 Br15 82.1(5) . 1_655
O9 Pb20 Br15 156.1(5) 1_665 1_655
O17 Pb20 Pb8 41.3(4) . .
O3 Pb20 Pb8 40.4(5) . .
O9 Pb20 Pb8 96.8(5) 1_665 .
Br15 Pb20 Pb8 75.55(13) 1_655 .
O17 Pb20 Pb29 38.8(4) . 1_665
O3 Pb20 Pb29 93.9(6) . 1_665
O9 Pb20 Pb29 39.2(5) 1_665 1_665
Br15 Pb20 Pb29 119.79(13) 1_655 1_665
Pb8 Pb20 Pb29 64.88(3) . 1_665
O18 Pb21 O11 82.1(8) 2_655 .
O18 Pb21 Br3 84.5(6) 2_655 .
O11 Pb21 Br3 82.8(5) . .
O11 Pb22 O11 75.4(7) . 2_656
O11 Pb22 O10 80.3(7) . 1_655
O11 Pb22 O10 104.1(8) 2_656 1_655
O11 Pb22 Pb22 38.3(5) . 2_656
O11 Pb22 Pb22 37.2(4) 2_656 2_656
O10 Pb22 Pb22 92.9(5) 1_655 2_656
O20 Pb23 O10 80.8(7) . .
O20 Pb23 Br2 85.4(5) . .
O10 Pb23 Br2 86.7(6) . .
O20 Pb23 Pb6 42.8(4) . 1_455
O10 Pb23 Pb6 38.8(5) . 1_455
Br2 Pb23 Pb6 78.78(10) . 1_455
O16 Pb24 O5 81.4(7) 2_765 .
O16 Pb24 Br8 82.7(6) 2_765 .
O5 Pb24 Br8 83.8(6) . .
O16 Pb24 Pb18 124.7(6) 2_765 1_665
O5 Pb24 Pb18 131.2(6) . 1_665
Br8 Pb24 Pb18 63.16(11) . 1_665
O13 Pb25 O8 81.1(6) 2 2
O13 Pb25 Br6 84.7(5) 2 .
O8 Pb25 Br6 84.5(4) 2 .
O13 Pb25 Pb10 41.1(5) 2 2
O8 Pb25 Pb10 40.2(4) 2 2
Br6 Pb25 Pb10 80.60(10) . 2
O16 Pb26 O7 82.6(7) . 1_655
O16 Pb26 O20 77.2(7) . 1_655
O7 Pb26 O20 100.5(7) 1_655 1_655
O16 Pb26 Br8 76.1(5) . 2_765
O7 Pb26 Br8 82.5(5) 1_655 2_765
O20 Pb26 Br8 152.5(5) 1_655 2_765
O16 Pb26 Pb13 39.0(5) . 1_655
O7 Pb26 Pb13 90.4(5) 1_655 1_655
O20 Pb26 Pb13 38.2(5) 1_655 1_655
Br8 Pb26 Pb13 115.02(11) 2_765 1_655
O17 Pb27 O15 80.3(7) 2_666 .
O17 Pb27 O19 103.7(8) 2_666 .
O15 Pb27 O19 77.5(7) . .
O17 Pb27 Br15 82.5(5) 2_666 2_566
O15 Pb27 Br15 76.7(6) . 2_566
O19 Pb27 Br15 152.0(4) . 2_566
O17 Pb27 Pb7 90.9(5) 2_666 .
O15 Pb27 Pb7 38.6(6) . .
O19 Pb27 Pb7 38.9(4) . .
Br15 Pb27 Pb7 114.93(11) 2_566 .
O15 Pb28 O7 83.7(8) 2_566 .
O15 Pb28 Br15 84.8(6) 2_566 .
O7 Pb28 Br15 85.7(5) . .
O15 Pb28 Pb8 44.6(6) 2_566 1_455
O7 Pb28 Pb8 39.6(4) . 1_455
Br15 Pb28 Pb8 78.25(13) . 1_455
O17 Pb29 O9 77.0(6) 1_445 .
O17 Pb29 O4 110.7(7) 1_445 2
O9 Pb29 O4 79.9(7) . 2
O17 Pb29 Pb17 93.7(5) 1_445 .
O9 Pb29 Pb17 38.5(4) . .
O4 Pb29 Pb17 41.4(5) 2 .
O17 Pb29 Pb20 37.8(5) 1_445 1_445
O9 Pb29 Pb20 39.2(4) . 1_445
O4 Pb29 Pb20 98.1(5) 2 1_445
Pb17 Pb29 Pb20 64.05(3) . 1_445
O17 Pb29 Pb18 105.1(5) 1_445 .
O9 Pb29 Pb18 37.5(5) . .
O4 Pb29 Pb18 92.7(5) 2 .
Pb17 Pb29 Pb18 60.12(3) . .
Pb20 Pb29 Pb18 70.12(3) 1_445 .
O12 Pb30 O4 82.9(7) . .
O12 Pb30 Br10 88.5(6) . .
O4 Pb30 Br10 86.7(6) . .
O12 Pb30 Br12 160.0(4) . 2
O4 Pb30 Br12 80.7(6) . 2
Br10 Pb30 Br12 79.16(16) . 2
O12 Pb30 Pb2 39.7(5) . .
O4 Pb30 Pb2 43.2(5) . .
Br10 Pb30 Pb2 85.17(11) . .
Br12 Pb30 Pb2 122.55(11) 2 .
Br13 Pb31 Br11 90.49(14) . .
Br13 Pb31 Br14 90.80(15) . .
Br11 Pb31 Br14 177.1(2) . .
Br13 Pb31 Br17 89.90(18) . .
Br11 Pb31 Br17 88.99(16) . .
Br14 Pb31 Br17 88.44(18) . .
Br13 Pb31 Br18 175.4(3) . .
Br11 Pb31 Br18 90.24(16) . .
Br14 Pb31 Br18 88.67(17) . .
Br17 Pb31 Br18 94.7(2) . .
Br13 Pb31 Br16 90.66(17) . .
Br11 Pb31 Br16 92.08(16) . .
Br14 Pb31 Br16 90.48(17) . .
Br17 Pb31 Br16 178.79(15) . .
Br18 Pb31 Br16 84.8(2) . .
Pb23 Br2 Pb2 114.20(16) . 2
Pb24 Br8 Pb26 74.94(11) . 2_765
Pb30 Br12 Pb18 116.9(2) 2 .
Pb31 Br14 Pb2 148.7(3) . 2
Pb28 Br15 Pb27 75.99(16) . 2_566
Pb28 Br15 Pb20 116.1(2) . 1_455
Pb27 Br15 Pb20 71.39(13) 2_566 1_455
Pb5 Br18 Pb31 154.4(4) . .
Pb12 O1 Pb4 119.3(7) . 2_665
Pb12 O1 Pb1 114.5(9) . 2_665
Pb4 O1 Pb1 102.6(7) 2_665 2_665
Pb12 O1 Pb1 103.6(7) . .
Pb4 O1 Pb1 112.5(9) 2_665 .
Pb1 O1 Pb1 103.4(6) 2_665 .
Pb5 O2 Pb5 99.9(6) . 2_666
Pb5 O2 Pb11 112.0(9) . .
Pb5 O2 Pb11 117.9(8) 2_666 .
Pb5 O2 Pb7 119.5(8) . .
Pb5 O2 Pb7 110.5(9) 2_666 .
Pb11 O2 Pb7 98.2(6) . .
Pb20 O3 Pb16 114.3(10) . 1_655
Pb20 O3 Pb19 119.1(7) . 2_765
Pb16 O3 Pb19 103.4(7) 1_655 2_765
Pb20 O3 Pb8 101.1(7) . .
Pb16 O3 Pb8 103.7(7) 1_655 .
Pb19 O3 Pb8 114.6(10) 2_765 .
Pb30 O4 Pb29 115.0(10) . 2
Pb30 O4 Pb17 116.5(7) . 2
Pb29 O4 Pb17 97.7(7) 2 2
Pb30 O4 Pb2 99.6(7) . .
Pb29 O4 Pb2 118.9(7) 2 .
Pb17 O4 Pb2 110.1(9) 2 .
Pb24 O5 Pb19 112.0(10) . .
Pb24 O5 Pb4 125.4(9) . .
Pb19 O5 Pb4 101.8(7) . .
Pb24 O5 Pb16 106.3(7) . 2_665
Pb19 O5 Pb16 101.4(7) . 2_665
Pb4 O5 Pb16 107.4(9) . 2_665
Pb9 O6 Pb6 115.9(10) . 2_655
Pb9 O6 Pb14 104.5(7) . .
Pb6 O6 Pb14 103.4(7) 2_655 .
Pb9 O6 Pb2 118.1(8) . .
Pb6 O6 Pb2 101.0(6) 2_655 .
Pb14 O6 Pb2 113.3(9) . .
Pb28 O7 Pb26 119.1(7) . 1_455
Pb28 O7 Pb16 114.3(9) . .
Pb26 O7 Pb16 104.0(7) 1_455 .
Pb28 O7 Pb8 105.1(7) . 1_455
Pb26 O7 Pb8 113.2(9) 1_455 1_455
Pb16 O7 Pb8 99.6(6) . 1_455
Pb15 O8 Pb25 115.6(7) . 2
Pb15 O8 Pb10 105.0(6) . 2_655
Pb25 O8 Pb10 114.1(8) 2 2_655
Pb15 O8 Pb10 115.0(8) . .
Pb25 O8 Pb10 101.1(5) 2 .
Pb10 O8 Pb10 105.8(6) 2_655 .
Pb17 O9 Pb18 104.9(7) . .
Pb17 O9 Pb20 111.8(10) . 1_445
Pb18 O9 Pb20 128.9(8) . 1_445
Pb17 O9 Pb29 101.9(7) . .
Pb18 O9 Pb29 104.3(9) . .
Pb20 O9 Pb29 101.6(7) 1_445 .
Pb23 O10 Pb22 118.2(8) . 1_455
Pb23 O10 Pb6 104.9(7) . 1_455
Pb22 O10 Pb6 113.3(10) 1_455 1_455
Pb23 O10 Pb14 113.1(10) . 2
Pb22 O10 Pb14 103.5(7) 1_455 2
Pb6 O10 Pb14 102.9(7) 1_455 2
Pb21 O11 Pb22 116.2(10) . .
Pb21 O11 Pb22 122.4(8) . 2_656
Pb22 O11 Pb22 104.6(7) . 2_656
Pb21 O11 Pb14 104.7(8) . 2_655
Pb22 O11 Pb14 101.5(7) . 2_655
Pb22 O11 Pb14 105.0(9) 2_656 2_655
Pb30 O12 Pb2 103.9(7) . .
Pb30 O12 Pb13 123.0(8) . 2
Pb2 O12 Pb13 108.4(9) . 2
Pb30 O12 Pb6 116.1(10) . 2_655
Pb2 O12 Pb6 101.3(7) . 2_655
Pb13 O12 Pb6 102.0(7) 2 2_655
Pb25 O13 Pb18 114.6(9) 2 .
Pb25 O13 Pb17 125.3(7) 2 .
Pb18 O13 Pb17 100.8(5) . .
Pb25 O13 Pb10 103.3(6) 2 .
Pb18 O13 Pb10 104.0(6) . .
Pb17 O13 Pb10 107.0(8) . .
Pb3 O14 Pb4 117.0(10) . .
Pb3 O14 Pb19 124.7(8) . .
Pb4 O14 Pb19 101.5(6) . .
Pb3 O14 Pb1 104.1(7) . .
Pb4 O14 Pb1 100.1(7) . .
Pb19 O14 Pb1 106.5(8) . .
Pb28 O15 Pb27 113.8(11) 2_566 .
Pb28 O15 Pb7 130.1(9) 2_566 .
Pb27 O15 Pb7 103.4(8) . .
Pb28 O15 Pb8 99.7(8) 2_566 2_666
Pb27 O15 Pb8 100.8(7) . 2_666
Pb7 O15 Pb8 105.0(10) . 2_666
Pb24 O16 Pb26 116.8(10) 2_765 .
Pb24 O16 Pb13 129.5(9) 2_765 1_655
Pb26 O16 Pb13 103.2(7) . 1_655
Pb24 O16 Pb16 101.6(6) 2_765 1_655
Pb26 O16 Pb16 99.6(7) . 1_655
Pb13 O16 Pb16 100.7(9) 1_655 1_655
Pb27 O17 Pb20 108.9(9) 2_666 .
Pb27 O17 Pb29 124.8(8) 2_666 1_665
Pb20 O17 Pb29 103.4(6) . 1_665
Pb27 O17 Pb8 107.4(6) 2_666 .
Pb20 O17 Pb8 100.2(6) . .
Pb29 O17 Pb8 109.4(8) 1_665 .
Pb21 O18 Pb9 115.0(11) 2_655 .
Pb21 O18 Pb11 128.8(9) 2_655 1_554
Pb9 O18 Pb11 104.6(8) . 1_554
Pb21 O18 Pb14 103.8(8) 2_655 .
Pb9 O18 Pb14 98.7(7) . .
Pb11 O18 Pb14 100.7(9) 1_554 .
Pb11 O19 Pb7 103.4(7) . .
Pb11 O19 Pb27 107.9(9) . .
Pb7 O19 Pb27 101.6(7) . .
Pb11 O19 Pb9 103.6(7) . 1_556
Pb7 O19 Pb9 108.4(9) . 1_556
Pb27 O19 Pb9 129.4(8) . 1_556
Pb23 O20 Pb13 114.6(9) . .
Pb23 O20 Pb26 129.0(8) . 1_455
Pb13 O20 Pb26 102.4(7) . 1_455
Pb23 O20 Pb6 100.6(6) . 1_455
Pb13 O20 Pb6 102.4(7) . 1_455
Pb26 O20 Pb6 104.4(8) 1_455 1_455
Pb12 O21 Pb3 115.7(10) . .
Pb12 O21 Pb15 132.6(8) . .
Pb3 O21 Pb15 101.5(8) . .
Pb12 O21 Pb1 100.3(7) . .
Pb3 O21 Pb1 100.5(6) . .
Pb15 O21 Pb1 100.5(8) . .
Pb15 O22 Pb18 114.3(10) . 2_655
Pb15 O22 Pb3 103.0(7) . .
Pb18 O22 Pb3 127.6(8) 2_655 .
Pb15 O22 Pb10 101.2(6) . 2_655
Pb18 O22 Pb10 102.5(7) 2_655 2_655
Pb3 O22 Pb10 104.9(8) . 2_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pb1 O1 2.367(17) 2_665
Pb1 O1 2.43(2) .
Pb1 O14 2.50(2) .
Pb1 O21 2.582(19) .
Pb1 Pb4 3.6610(17) .
Pb1 Pb12 3.6633(18) .
Pb2 O12 2.346(19) .
Pb2 O6 2.45(2) .
Pb2 O4 2.47(2) .
Pb2 Br14 3.153(6) 2
Pb2 Br2 3.217(5) 2
Pb2 Pb30 3.5609(17) .
Pb2 Pb6 3.6946(18) 2_655
Pb3 O14 2.247(18) .
Pb3 O21 2.29(2) .
Pb3 O22 2.352(19) .
Pb3 Pb15 3.5983(18) .
Pb4 O14 2.269(17) .
Pb4 O1 2.32(2) 2_665
Pb4 O5 2.34(2) .
Pb4 Pb19 3.6255(19) .
Pb5 O2 2.280(18) .
Pb5 O2 2.32(2) 2_666
Pb5 Br18 2.785(8) .
Pb5 Pb5 3.517(3) 2_666
Pb6 O6 2.334(17) 2_655
Pb6 O10 2.37(2) 1_655
Pb6 O12 2.43(2) 2_655
Pb6 O20 2.522(17) 1_655
Pb6 Pb23 3.6512(18) 1_655
Pb6 Pb2 3.6946(18) 2_655
Pb7 O15 2.32(2) .
Pb7 O19 2.320(19) .
Pb7 O2 2.425(19) .
Pb7 Pb11 3.6129(18) .
Pb7 Pb27 3.6171(18) .
Pb8 O3 2.40(2) .
Pb8 O7 2.426(17) 1_655
Pb8 O17 2.432(17) .
Pb8 O15 2.62(2) 2_666
Pb8 Pb20 3.6261(17) .
Pb8 Pb28 3.6749(17) 1_655
Pb9 O6 2.261(18) .
Pb9 O18 2.28(2) .
Pb9 O19 2.36(2) 1_554
Pb9 Pb11 3.6490(18) 1_554
Pb9 Pb14 3.6834(18) .
Pb10 O8 2.352(17) 2_655
Pb10 O8 2.379(15) .
Pb10 O13 2.442(19) .
Pb10 O22 2.512(18) 2_655
Pb10 Pb25 3.6183(19) 2
Pb10 Pb15 3.6810(17) 2_655
Pb11 O19 2.28(2) .
Pb11 O18 2.33(2) 1_556
Pb11 O2 2.354(18) .
Pb11 Pb9 3.6490(18) 1_556
Pb12 O21 2.18(2) .
Pb12 O1 2.230(18) .
Pb12 Br1 3.042(4) .
Pb13 O20 2.28(2) .
Pb13 O16 2.33(2) 1_455
Pb13 O12 2.384(19) 2
Pb13 Pb26 3.5954(16) 1_455
Pb14 O10 2.379(19) 2
Pb14 O6 2.40(2) .
Pb14 O11 2.51(2) 2_655
Pb14 O18 2.57(2) .
Pb15 O22 2.25(2) .
Pb15 O8 2.286(15) .
Pb15 O21 2.36(2) .
Pb15 Pb10 3.6810(17) 2_655
Pb16 O3 2.311(18) 1_455
Pb16 O5 2.42(2) 2_665
Pb16 O7 2.42(2) .
Pb16 O16 2.590(19) 1_455
Pb16 Pb19 3.6728(16) 2_665
Pb17 O9 2.288(19) .
Pb17 O4 2.40(2) 2
Pb17 O13 2.441(18) .
Pb17 Br7 3.220(5) .
Pb17 Pb29 3.6001(17) .
Pb17 Pb18 3.6444(18) .
Pb18 O22 2.26(2) 2_655
Pb18 O13 2.285(16) .
Pb18 O9 2.31(2) .
Pb18 Br12 3.163(7) .
Pb18 Pb29 3.6743(17) .
Pb18 Pb24 3.6922(19) 1_445
Pb19 O5 2.328(19) .
Pb19 O3 2.37(2) 2_765
Pb19 O14 2.41(2) .
Pb19 Pb16 3.6728(16) 2_665
Pb20 O17 2.29(2) .
Pb20 O3 2.30(2) .
Pb20 O9 2.346(19) 1_665
Pb20 Br15 3.188(6) 1_655
Pb20 Pb29 3.6358(16) 1_665
Pb21 O18 2.18(2) 2_655
Pb21 O11 2.21(2) .
Pb21 Br3 3.078(4) .
Pb22 O11 2.269(18) .
Pb22 O11 2.33(2) 2_656
Pb22 O10 2.34(2) 1_655
Pb22 Pb22 3.636(2) 2_656
Pb23 O20 2.215(19) .
Pb23 O10 2.24(2) .
Pb23 Br2 3.027(5) .
Pb23 Pb6 3.6512(18) 1_455
Pb24 O16 2.19(2) 2_765
Pb24 O5 2.21(2) .
Pb24 Br8 2.985(5) .
Pb24 Pb18 3.6922(19) 1_665
Pb25 O13 2.165(16) 2
Pb25 O8 2.308(18) 2
Pb25 Br6 3.039(5) .
Pb25 Pb10 3.6183(19) 2
Pb26 O16 2.26(2) .
Pb26 O7 2.286(18) 1_655
Pb26 O20 2.336(18) 1_655
Pb26 Br8 3.231(5) 2_765
Pb26 Pb13 3.5954(16) 1_655
Pb27 O17 2.267(19) 2_666
Pb27 O15 2.29(2) .
Pb27 O19 2.35(2) .
Pb27 Br15 3.170(6) 2_566
Pb28 O15 2.17(2) 2_566
Pb28 O7 2.20(2) .
Pb28 Br15 2.894(6) .
Pb28 Pb8 3.6749(17) 1_455
Pb29 O17 2.342(17) 1_445
Pb29 O9 2.35(2) .
Pb29 O4 2.378(18) 2
Pb29 Pb20 3.6358(16) 1_445
Pb30 O12 2.17(2) .
Pb30 O4 2.180(19) .
Pb30 Br10 2.903(5) .
Pb30 Br12 3.140(6) 2
Pb31 Br13 2.780(5) .
Pb31 Br11 2.836(4) .
Pb31 Br14 2.892(5) .
Pb31 Br17 2.999(6) .
Pb31 Br18 3.011(7) .
Pb31 Br16 3.014(5) .
Br2 Pb2 3.217(5) 2
Br8 Pb26 3.231(5) 2_765
Br12 Pb30 3.140(6) 2
Br14 Pb2 3.153(6) 2
Br15 Pb27 3.170(6) 2_566
Br15 Pb20 3.188(6) 1_455
O1 Pb4 2.32(2) 2_665
O1 Pb1 2.367(17) 2_665
O2 Pb5 2.32(2) 2_666
O3 Pb16 2.311(18) 1_655
O3 Pb19 2.37(2) 2_765
O4 Pb29 2.378(18) 2
O4 Pb17 2.40(2) 2
O5 Pb16 2.42(2) 2_665
O6 Pb6 2.334(17) 2_655
O7 Pb26 2.286(18) 1_455
O7 Pb8 2.426(17) 1_455
O8 Pb25 2.308(18) 2
O8 Pb10 2.352(17) 2_655
O9 Pb20 2.346(19) 1_445
O10 Pb22 2.34(2) 1_455
O10 Pb6 2.37(2) 1_455
O10 Pb14 2.379(19) 2
O11 Pb22 2.33(2) 2_656
O11 Pb14 2.51(2) 2_655
O12 Pb13 2.384(19) 2
O12 Pb6 2.43(2) 2_655
O13 Pb25 2.165(16) 2
O15 Pb28 2.17(2) 2_566
O15 Pb8 2.62(2) 2_666
O16 Pb24 2.19(2) 2_765
O16 Pb13 2.33(2) 1_655
O16 Pb16 2.590(19) 1_655
O17 Pb27 2.267(19) 2_666
O17 Pb29 2.342(17) 1_665
O18 Pb21 2.18(2) 2_655
O18 Pb11 2.33(2) 1_554
O19 Pb9 2.36(2) 1_556
O20 Pb26 2.336(18) 1_455
O20 Pb6 2.522(17) 1_455
O22 Pb18 2.26(2) 2_655
O22 Pb10 2.512(18) 2_655
