#------------------------------------------------------------------------------
#$Date: 2016-03-23 22:36:42 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179486 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/83/4338326.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4338326
loop_
_publ_author_name
'Wang, Genxiang'
'Luo, Min'
'Ye, Ning'
'Lin, Chensheng'
'Cheng, Wendan'
_publ_section_title
;
 Series of Lead Oxide Hydroxide Nitrates Obtained by Adjusting the pH
 Values of the Reaction Systems.
;
_journal_issue                   10
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5222
_journal_page_last               5228
_journal_paper_doi               10.1021/ic5004116
_journal_volume                  53
_journal_year                    2014
_chemical_formula_sum            'H0 N0.86 O4.14 Pb1.43'
_chemical_formula_weight         374.28
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                97.277(10)
_cell_angle_beta                 98.222(14)
_cell_angle_gamma                91.758(8)
_cell_formula_units_Z            28
_cell_length_a                   8.594(7)
_cell_length_b                   14.601(13)
_cell_length_c                   23.91(2)
_cell_measurement_reflns_used    6596
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.7003
_cell_measurement_theta_min      2.3761
_cell_volume                     2942(4)
_computing_cell_refinement       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_collection       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_reduction        'CrystalClear (Rigaku Inc., 2008)'
_computing_molecular_graphics    'SHELXL-97 (Sheldrick, 1997)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 14.6306
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device
;
Mercury70 (2x2 bin mode)
;
_diffrn_measurement_method       CCD_Profile_fitting
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1018
_diffrn_reflns_av_sigmaI/netI    0.1146
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            28686
_diffrn_reflns_theta_full        25.50
_diffrn_reflns_theta_max         25.50
_diffrn_reflns_theta_min         2.09
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count none
_diffrn_standards_interval_time  none
_exptl_absorpt_coefficient_mu    57.114
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.4683
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            White
_exptl_crystal_density_diffrn    5.915
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             4376
_exptl_crystal_size_max          0.2500
_exptl_crystal_size_mid          0.1500
_exptl_crystal_size_min          0.0500
_refine_diff_density_max         9.545
_refine_diff_density_min         -9.353
_refine_diff_density_rms         0.929
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.007
_refine_ls_matrix_type           full
_refine_ls_number_parameters     811
_refine_ls_number_reflns         10881
_refine_ls_number_restraints     1068
_refine_ls_restrained_S_all      1.026
_refine_ls_R_factor_all          0.1044
_refine_ls_R_factor_gt           0.0789
_refine_ls_shift/su_max          0.092
_refine_ls_shift/su_mean         0.004
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1257P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1932
_refine_ls_wR_factor_ref         0.2173
_reflns_number_gt                7692
_reflns_number_total             10881
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic5004116_si_005.cif
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 4338324--4338327.cif.
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4338326
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pb1 Pb 0.86349(14) 0.77621(8) 0.35154(5) 0.0225(3) Uani 1 1 d U
Pb2 Pb 0.57409(14) 0.83800(8) 0.44814(5) 0.0219(3) Uani 1 1 d U
Pb3 Pb 0.99841(14) 0.43621(8) 0.39965(5) 0.0251(3) Uani 1 1 d .
Pb4 Pb 1.32550(14) 0.22370(8) 0.40283(5) 0.0254(3) Uani 1 1 d U
Pb5 Pb 0.65020(14) 0.82181(9) 0.20924(5) 0.0263(3) Uani 1 1 d .
Pb6 Pb 1.14991(14) 0.32112(9) 0.27014(5) 0.0279(3) Uani 1 1 d .
Pb7 Pb 0.46968(14) 0.64611(8) 0.32477(5) 0.0246(3) Uani 1 1 d .
Pb8 Pb 0.77033(16) 0.42331(9) 0.24876(5) 0.0303(3) Uani 1 1 d .
Pb9 Pb 0.41102(16) 0.93778(8) 0.30445(5) 0.0274(3) Uani 1 1 d .
Pb10 Pb 0.99543(14) 0.84612(9) 0.51223(5) 0.0280(3) Uani 1 1 d .
Pb11 Pb 0.76667(15) 0.63248(8) 0.46192(5) 0.0241(3) Uani 1 1 d .
Pb12 Pb 0.29954(15) 0.94632(8) 0.14362(5) 0.0263(3) Uani 1 1 d .
Pb13 Pb -0.23277(16) 1.14169(9) 0.17008(6) 0.0319(3) Uani 1 1 d .
Pb14 Pb 0.53739(16) 0.71965(10) 0.06009(5) 0.0323(3) Uani 1 1 d .
Pb15 Pb 0.22447(18) 0.86254(9) -0.01104(6) 0.0360(4) Uani 1 1 d .
Pb16 Pb 0.82580(15) 0.21694(9) 0.33403(6) 0.0335(4) Uani 1 1 d .
Pb17 Pb 0.23431(15) 0.72989(9) 0.19333(5) 0.0299(3) Uani 1 1 d .
Pb18 Pb 0.30750(18) 0.65019(10) -0.08885(6) 0.0371(4) Uani 1 1 d .
Pb19 Pb -0.09223(18) 0.72373(11) -0.11033(6) 0.0437(4) Uani 1 1 d .
Pb20 Pb 0.0927(2) 0.64818(11) 0.03248(6) 0.0440(4) Uani 1 1 d .
O1 O 0.822(3) 0.8875(14) 0.4291(9) 0.028(3) Uani 1 1 d U
O2 O 0.754(3) 0.7774(15) 0.5123(10) 0.033(3) Uani 1 1 d U
O3 O 0.625(3) 0.7012(16) 0.2621(10) 0.036(3) Uani 1 1 d U
O4 O 0.174(3) 0.7832(17) -0.0998(10) 0.042(4) Uani 1 1 d U
O5 O 0.394(3) 0.8594(16) 0.2144(10) 0.036(3) Uani 1 1 d U
O6 O 0.303(3) 0.7157(18) 0.0035(11) 0.045(3) Uani 1 1 d U
O7 O 0.052(3) 0.6121(18) -0.0703(11) 0.047(4) Uani 1 1 d U
O8 O 0.665(3) 0.8919(15) 0.3031(9) 0.031(3) Uani 1 1 d U
O9 O 0.925(3) 0.8216(17) 0.6458(11) 0.042(3) Uani 1 1 d U
O10 O 0.982(3) 0.7180(15) 0.4419(10) 0.032(3) Uani 1 1 d U
O11 O 0.774(3) 0.6330(16) 0.5982(10) 0.037(3) Uani 1 1 d U
O12 O 1.071(3) 0.6476(16) 0.6843(10) 0.037(3) Uani 1 1 d U
O13 O 0.156(3) 0.8026(17) 0.1152(11) 0.045(3) Uani 1 1 d U
O14 O 1.019(3) 0.6151(16) 0.7994(10) 0.038(3) Uani 1 1 d U
O15 O 1.322(3) 0.7206(17) 0.7880(11) 0.041(3) Uani 1 1 d U
O16 O 0.661(3) 0.7134(15) 0.3923(9) 0.031(2) Uani 1 1 d U
O17 O 1.095(3) 0.7020(16) 0.5745(10) 0.037(3) Uani 1 1 d U
O18 O 0.419(3) 0.6877(18) 0.1363(11) 0.044(3) Uani 1 1 d U
O19 O -0.015(3) 0.7739(18) -0.0107(11) 0.046(3) Uani 1 1 d U
O20 O 0.998(3) 0.8044(16) 0.7804(10) 0.039(3) Uani 1 1 d U
O21 O 0.384(3) 0.7959(15) 0.3349(10) 0.035(3) Uani 1 1 d U
O22 O 0.474(3) 0.8697(17) 0.0939(11) 0.041(3) Uani 1 1 d U
O23 O 1.521(3) 0.5200(16) 0.6010(11) 0.041(5) Uani 1 1 d U
O24 O 0.822(4) 1.126(2) 0.5920(13) 0.061(6) Uani 1 1 d U
O25 O 1.730(3) 0.0639(17) 0.3977(11) 0.044(6) Uani 1 1 d U
O26 O 0.309(3) 0.6677(18) 0.4260(11) 0.044(5) Uani 1 1 d U
O27 O 1.314(3) 0.5102(16) 0.6395(10) 0.036(4) Uani 1 1 d U
O28 O 0.252(3) 0.5921(18) 0.4909(12) 0.045(5) Uani 1 1 d U
O29 O 1.519(4) 0.0385(19) 0.4332(12) 0.055(6) Uani 1 1 d U
O30 O 0.486(3) 0.6509(16) 0.4966(10) 0.038(3) Uani 1 1 d U
O31 O 1.437(3) 0.6445(16) 0.6430(11) 0.040(4) Uani 1 1 d U
O32 O 1.070(3) 0.4224(17) 0.6755(11) 0.041(5) Uani 1 1 d U
O33 O -0.159(4) 0.859(2) 0.0846(13) 0.059(5) Uani 1 1 d U
O34 O 0.121(4) 1.0108(19) 0.2371(12) 0.055(5) Uani 1 1 d U
O35 O 0.883(3) 0.3353(18) 0.6992(13) 0.054(6) Uani 1 1 d U
O36 O 0.021(4) 0.8784(19) 0.2451(13) 0.055(5) Uani 1 1 d U
O37 O -0.015(4) 0.571(2) 0.1429(14) 0.067(6) Uani 1 1 d U
O38 O 0.847(3) 0.4792(18) 0.6832(12) 0.048(5) Uani 1 1 d U
O39 O -0.113(4) 1.000(2) 0.2564(14) 0.064(6) Uani 1 1 d U
O40 O 0.409(4) 0.520(2) 0.0560(14) 0.071(5) Uani 1 1 d U
O41 O -0.027(4) 0.984(2) 0.0722(13) 0.061(5) Uani 1 1 d U
O42 O -0.273(4) 0.985(2) 0.0805(13) 0.058(6) Uani 1 1 d U
O43 O -0.246(4) 0.570(2) 0.1644(14) 0.072(7) Uani 1 1 d U
O44 O 1.648(3) 0.1700(17) 0.4497(11) 0.045(6) Uani 1 1 d U
O45 O 0.506(4) 1.0646(19) 0.2323(12) 0.049(5) Uani 1 1 d U
O46 O -0.130(4) 0.698(2) 0.1493(14) 0.064(5) Uani 1 1 d U
O47 O 0.363(4) 1.173(2) 0.2014(14) 0.066(6) Uani 1 1 d U
O48 O 0.458(4) 0.534(2) 0.2050(13) 0.063(5) Uani 1 1 d U
O49 O 0.252(4) 0.478(2) 0.1539(14) 0.070(5) Uani 1 1 d U
O50 O 0.611(4) 0.616(2) 0.7996(15) 0.070(8) Uani 1 1 d U
O51 O -0.256(4) 0.896(2) -0.0630(15) 0.072(5) Uani 1 1 d U
O52 O 0.209(4) 0.479(2) -0.0018(13) 0.060(4) Uani 1 1 d U
O53 O 0.341(4) 0.377(2) 0.0380(14) 0.078(6) Uani 1 1 d U
O54 O 0.815(4) 1.002(2) 0.5354(12) 0.056(5) Uani 1 1 d U
O55 O 0.413(4) 1.164(2) 0.2898(15) 0.073(6) Uani 1 1 d U
O56 O 0.860(4) 0.999(2) 0.6231(14) 0.069(6) Uani 1 1 d U
O57 O -0.480(5) 0.916(3) -0.0765(18) 0.100(8) Uani 1 1 d U
O58 O -0.458(5) 0.805(3) -0.0431(17) 0.094(7) Uani 1 1 d U
N1 N 0.838(3) 1.045(2) 0.5849(12) 0.029(6) Uani 1 1 d .
N2 N 1.428(4) 0.5582(19) 0.6295(13) 0.037(8) Uani 1 1 d .
N3 N 1.633(3) 0.0932(17) 0.4275(11) 0.024(6) Uani 1 1 d U
N4 N 0.349(4) 0.6338(18) 0.4714(12) 0.031(6) Uani 1 1 d U
N5 N 0.006(4) 0.961(2) 0.2462(13) 0.039(8) Uani 1 1 d .
N7 N 0.930(4) 0.413(2) 0.6851(13) 0.039(7) Uani 1 1 d U
N6 N -0.135(4) 0.607(2) 0.1534(13) 0.040(7) Uani 1 1 d U
N8 N -0.150(5) 0.945(2) 0.0857(15) 0.052(9) Uani 1 1 d U
N9 N -0.391(5) 0.866(2) -0.0589(15) 0.050(9) Uani 1 1 d U
N10 N 0.637(4) 0.537(2) 0.8116(15) 0.049(9) Uani 1 1 d .
N11 N 0.433(4) 1.131(2) 0.2440(13) 0.049(9) Uani 1 1 d .
N12 N 0.330(5) 0.460(2) 0.0279(19) 0.078(16) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O16 Pb1 O1 73.9(7) . .
O16 Pb1 O10 71.6(8) . .
O1 Pb1 O10 72.5(8) . .
O16 Pb1 O8 90.6(8) . .
O1 Pb1 O8 76.0(7) . .
O10 Pb1 O8 147.1(8) . .
O16 Pb1 Pb2 37.6(5) . .
O1 Pb1 Pb2 38.6(5) . .
O10 Pb1 Pb2 77.3(6) . .
O8 Pb1 Pb2 72.0(5) . .
O2 Pb2 O16 77.4(8) . .
O2 Pb2 O1 74.7(8) . .
O16 Pb2 O1 74.5(8) . .
O2 Pb2 Pb11 40.7(5) . .
O16 Pb2 Pb11 39.6(5) . .
O1 Pb2 Pb11 81.8(5) . .
O2 Pb2 Pb1 82.5(6) . .
O16 Pb2 Pb1 37.7(6) . .
O1 Pb2 Pb1 39.1(5) . .
Pb11 Pb2 Pb1 62.66(4) . .
O12 Pb3 O11 86.0(9) 2_766 2_766
O12 Pb3 O17 78.3(8) 2_766 2_766
O11 Pb3 O17 84.2(9) 2_766 2_766
O12 Pb3 Pb16 37.7(6) 2_766 .
O11 Pb3 Pb16 85.1(6) 2_766 .
O17 Pb3 Pb16 40.7(6) 2_766 .
O2 Pb4 O11 87.1(9) 2_766 2_766
O2 Pb4 O9 92.3(9) 2_766 2_766
O11 Pb4 O9 81.7(9) 2_766 2_766
O5 Pb5 O3 91.1(9) . .
O5 Pb5 O8 77.6(8) . .
O3 Pb5 O8 74.9(8) . .
O5 Pb5 Pb9 38.6(6) . .
O3 Pb5 Pb9 83.6(6) . .
O8 Pb5 Pb9 39.2(6) . .
O5 Pb5 Pb14 90.3(6) . .
O3 Pb5 Pb14 105.2(6) . .
O8 Pb5 Pb14 167.9(6) . .
Pb9 Pb5 Pb14 128.76(6) . .
O20 Pb6 O12 86.1(9) 2_766 2_766
O20 Pb6 O14 76.0(8) 2_766 2_766
O12 Pb6 O14 77.6(9) 2_766 2_766
O20 Pb6 Pb8 80.6(7) 2_766 .
O12 Pb6 Pb8 38.8(6) 2_766 .
O14 Pb6 Pb8 38.9(7) 2_766 .
O16 Pb7 O21 80.3(8) . .
O16 Pb7 O3 84.0(8) . .
O21 Pb7 O3 84.3(9) . .
O15 Pb8 O12 85.4(8) 2_766 2_766
O15 Pb8 O14 83.5(9) 2_766 2_766
O12 Pb8 O14 78.7(9) 2_766 2_766
O15 Pb8 Pb6 84.9(7) 2_766 .
O12 Pb8 Pb6 39.3(7) 2_766 .
O14 Pb8 Pb6 39.4(6) 2_766 .
O5 Pb9 O21 86.7(8) . .
O5 Pb9 O8 78.2(8) . .
O21 Pb9 O8 81.1(9) . .
O5 Pb9 Pb5 38.7(6) . .
O21 Pb9 Pb5 84.7(6) . .
O8 Pb9 Pb5 39.6(5) . .
O2 Pb10 O10 76.1(8) . .
O2 Pb10 O1 73.0(8) . .
O10 Pb10 O1 74.2(8) . .
O2 Pb10 Pb11 38.4(6) . .
O10 Pb10 Pb11 39.5(6) . .
O1 Pb10 Pb11 78.2(5) . .
O16 Pb11 O2 78.4(8) . .
O16 Pb11 O10 76.0(8) . .
O2 Pb11 O10 75.4(8) . .
O16 Pb11 O30 83.5(8) . .
O2 Pb11 O30 69.7(8) . .
O10 Pb11 O30 142.3(8) . .
O16 Pb11 Pb2 40.9(6) . .
O2 Pb11 Pb2 40.4(6) . .
O10 Pb11 Pb2 83.4(6) . .
O30 Pb11 Pb2 60.9(5) . .
O16 Pb11 Pb10 82.8(5) . .
O2 Pb11 Pb10 37.7(6) . .
O10 Pb11 Pb10 39.5(6) . .
O30 Pb11 Pb10 107.3(5) . .
Pb2 Pb11 Pb10 63.00(7) . .
O22 Pb12 O5 84.1(9) . .
O22 Pb12 O13 80.6(9) . .
O5 Pb12 O13 77.0(8) . .
O22 Pb12 Pb17 84.7(6) . .
O5 Pb12 Pb17 38.2(6) . .
O13 Pb12 Pb17 39.2(6) . .
O4 Pb13 O20 87.5(9) 2_575 2_676
O4 Pb13 O15 88.2(9) 2_575 2_676
O20 Pb13 O15 83.8(9) 2_676 2_676
O6 Pb14 O18 91.8(10) . .
O6 Pb14 O22 84.4(9) . .
O18 Pb14 O22 80.8(9) . .
O6 Pb14 Pb5 129.6(7) . .
O18 Pb14 Pb5 53.5(6) . .
O22 Pb14 Pb5 57.6(6) . .
O4 Pb15 O6 77.3(9) . .
O4 Pb15 O19 75.9(9) . .
O6 Pb15 O19 74.9(10) . .
O4 Pb15 Pb18 39.5(7) . .
O6 Pb15 Pb18 39.5(7) . .
O19 Pb15 Pb18 79.7(7) . .
O4 Pb15 Pb20 83.9(6) . .
O6 Pb15 Pb20 37.3(7) . .
O19 Pb15 Pb20 40.2(7) . .
Pb18 Pb15 Pb20 61.28(7) . .
O9 Pb16 O12 85.6(9) 2_766 2_766
O9 Pb16 O17 77.4(9) 2_766 2_766
O12 Pb16 O17 77.0(8) 2_766 2_766
O9 Pb16 Pb3 80.7(6) 2_766 .
O12 Pb16 Pb3 36.6(6) 2_766 .
O17 Pb16 Pb3 40.4(6) 2_766 .
O5 Pb17 O18 81.2(9) . .
O5 Pb17 O13 79.7(8) . .
O18 Pb17 O13 78.0(10) . .
O5 Pb17 Pb12 39.2(6) . .
O18 Pb17 Pb12 81.2(6) . .
O13 Pb17 Pb12 40.9(6) . .
O6 Pb18 O4 76.8(9) . .
O6 Pb18 O7 75.1(9) . .
O4 Pb18 O7 76.2(9) . .
O6 Pb18 Pb15 39.9(7) . .
O4 Pb18 Pb15 38.5(6) . .
O7 Pb18 Pb15 80.1(6) . .
O6 Pb18 Pb19 83.3(7) . .
O4 Pb18 Pb19 40.5(6) . .
O7 Pb18 Pb19 38.5(7) . .
Pb15 Pb18 Pb19 62.25(4) . .
O6 Pb18 Pb20 36.5(7) . .
O4 Pb18 Pb20 82.5(7) . .
O7 Pb18 Pb20 40.7(6) . .
Pb15 Pb18 Pb20 60.24(5) . .
Pb19 Pb18 Pb20 64.13(6) . .
O7 Pb19 O4 76.0(9) . .
O7 Pb19 O19 70.8(9) . .
O4 Pb19 O19 73.7(9) . .
O7 Pb19 Pb18 39.8(7) . .
O4 Pb19 Pb18 38.9(6) . .
O19 Pb19 Pb18 78.5(7) . .
O6 Pb20 O19 76.5(10) . .
O6 Pb20 O7 74.6(9) . .
O19 Pb20 O7 69.3(9) . .
O6 Pb20 O52 87.7(10) . .
O19 Pb20 O52 137.5(9) . .
O7 Pb20 O52 68.6(9) . .
O6 Pb20 Pb15 38.4(7) . .
O19 Pb20 Pb15 40.8(7) . .
O7 Pb20 Pb15 78.0(6) . .
O52 Pb20 Pb15 123.1(7) . .
O6 Pb20 Pb18 37.1(6) . .
O19 Pb20 Pb18 77.9(7) . .
O7 Pb20 Pb18 39.6(7) . .
O52 Pb20 Pb18 66.5(7) . .
Pb15 Pb20 Pb18 58.48(5) . .
Pb2 O1 Pb1 102.3(8) . .
Pb2 O1 Pb10 101.1(8) . .
Pb1 O1 Pb10 105.2(9) . .
Pb4 O2 Pb10 116.6(9) 2_766 .
Pb4 O2 Pb2 112.7(11) 2_766 .
Pb10 O2 Pb2 108.8(9) . .
Pb4 O2 Pb11 114.4(10) 2_766 .
Pb10 O2 Pb11 103.9(10) . .
Pb2 O2 Pb11 98.8(8) . .
Pb5 O3 Pb7 142.1(12) . .
Pb13 O4 Pb15 116.0(10) 2_575 .
Pb13 O4 Pb18 115.2(12) 2_575 .
Pb15 O4 Pb18 102.1(10) . .
Pb13 O4 Pb19 115.3(10) 2_575 .
Pb15 O4 Pb19 105.7(11) . .
Pb18 O4 Pb19 100.6(9) . .
Pb17 O5 Pb9 117.2(11) . .
Pb17 O5 Pb5 109.7(10) . .
Pb9 O5 Pb5 102.7(9) . .
Pb17 O5 Pb12 102.5(9) . .
Pb9 O5 Pb12 113.3(10) . .
Pb5 O5 Pb12 111.6(10) . .
Pb14 O6 Pb20 117.8(11) . .
Pb14 O6 Pb18 113.8(12) . .
Pb20 O6 Pb18 106.5(10) . .
Pb14 O6 Pb15 112.1(10) . .
Pb20 O6 Pb15 104.3(12) . .
Pb18 O6 Pb15 100.6(10) . .
Pb19 O7 Pb18 101.6(10) . .
Pb19 O7 Pb20 109.8(11) . .
Pb18 O7 Pb20 99.7(9) . .
Pb9 O8 Pb5 101.2(8) . .
Pb9 O8 Pb1 139.4(10) . .
Pb5 O8 Pb1 97.4(8) . .
Pb16 O9 Pb4 146.4(12) 2_766 2_766
Pb10 O10 Pb11 101.0(9) . .
Pb10 O10 Pb1 104.7(9) . .
Pb11 O10 Pb1 100.8(8) . .
Pb3 O11 Pb4 140.9(11) 2_766 2_766
Pb3 O12 Pb16 105.7(10) 2_766 2_766
Pb3 O12 Pb8 115.6(10) 2_766 2_766
Pb16 O12 Pb8 114.4(10) 2_766 2_766
Pb3 O12 Pb6 110.9(10) 2_766 2_766
Pb16 O12 Pb6 108.3(10) 2_766 2_766
Pb8 O12 Pb6 101.9(9) 2_766 2_766
Pb17 O13 Pb12 99.9(9) . .
Pb8 O14 Pb6 101.6(10) 2_766 2_766
Pb8 O15 Pb13 139.7(13) 2_766 2_676
Pb7 O16 Pb11 119.3(9) . .
Pb7 O16 Pb2 112.1(10) . .
Pb11 O16 Pb2 99.5(8) . .
Pb7 O16 Pb1 110.7(9) . .
Pb11 O16 Pb1 109.1(10) . .
Pb2 O16 Pb1 104.7(8) . .
Pb3 O17 Pb16 98.9(9) 2_766 2_766
Pb17 O18 Pb14 146.0(13) . .
Pb20 O19 Pb19 108.5(11) . .
Pb20 O19 Pb15 99.0(10) . .
Pb19 O19 Pb15 101.4(10) . .
Pb13 O20 Pb6 146.9(13) 2_676 2_766
Pb9 O21 Pb7 143.2(12) . .
Pb12 O22 Pb14 141.2(12) . .
N4 O30 Pb11 132(2) . .
N12 O52 Pb20 115(2) . .
O24 N1 O56 123(3) . .
O24 N1 O54 119(3) . .
O56 N1 O54 117(3) . .
O23 N2 O27 118(3) . .
O23 N2 O31 121(3) . .
O27 N2 O31 121(3) . .
O44 N3 O25 119(3) . .
O44 N3 O29 123(3) . .
O25 N3 O29 119(3) . .
O28 N4 O30 122(3) . .
O28 N4 O26 119(3) . .
O30 N4 O26 118(3) . .
O36 N5 O39 125(3) . .
O36 N5 O34 118(4) . .
O39 N5 O34 117(3) . .
O38 N7 O32 119(3) . .
O38 N7 O35 122(3) . .
O32 N7 O35 119(3) . .
O43 N6 O37 127(4) . .
O43 N6 O46 121(4) . .
O37 N6 O46 112(3) . .
O42 N8 O33 118(4) . .
O42 N8 O41 118(4) . .
O33 N8 O41 120(4) . .
O57 N9 O58 109(5) . .
O57 N9 O51 108(4) . .
O58 N9 O51 143(5) . .
O49 N10 O50 122(3) 2_666 .
O49 N10 O48 113(4) 2_666 2_666
O50 N10 O48 125(4) . 2_666
O55 N11 O45 127(4) . .
O55 N11 O47 115(4) . .
O45 N11 O47 118(3) . .
O40 N12 O52 119(3) . .
O40 N12 O53 121(4) . .
O52 N12 O53 118(4) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pb1 O16 2.33(2) .
Pb1 O1 2.38(2) .
Pb1 O10 2.51(2) .
Pb1 O8 2.68(2) .
Pb1 Pb2 3.686(3) .
Pb2 O2 2.30(2) .
Pb2 O16 2.32(2) .
Pb2 O1 2.35(2) .
Pb2 Pb11 3.500(3) .
Pb3 O12 2.21(2) 2_766
Pb3 O11 2.22(3) 2_766
Pb3 O17 2.34(2) 2_766
Pb3 Pb16 3.561(3) .
Pb4 O2 2.24(2) 2_766
Pb4 O11 2.29(2) 2_766
Pb4 O9 2.33(3) 2_766
Pb5 O5 2.30(3) .
Pb5 O3 2.32(2) .
Pb5 O8 2.33(2) .
Pb5 Pb9 3.585(3) .
Pb5 Pb14 3.669(3) .
Pb6 O20 2.30(2) 2_766
Pb6 O12 2.35(3) 2_766
Pb6 O14 2.35(2) 2_766
Pb6 Pb8 3.625(3) .
Pb7 O16 2.24(2) .
Pb7 O21 2.32(2) .
Pb7 O3 2.34(3) .
Pb8 O15 2.25(2) 2_766
Pb8 O12 2.32(2) 2_766
Pb8 O14 2.33(3) 2_766
Pb9 O5 2.29(2) .
Pb9 O21 2.30(2) .
Pb9 O8 2.31(3) .
Pb10 O2 2.27(2) .
Pb10 O10 2.34(2) .
Pb10 O1 2.46(2) .
Pb10 Pb11 3.611(3) .
Pb11 O16 2.26(2) .
Pb11 O2 2.31(2) .
Pb11 O10 2.34(2) .
Pb11 O30 2.67(3) .
Pb12 O22 2.28(3) .
Pb12 O5 2.31(2) .
Pb12 O13 2.37(2) .
Pb12 Pb17 3.570(3) .
Pb13 O4 2.23(3) 2_575
Pb13 O20 2.25(2) 2_676
Pb13 O15 2.33(3) 2_676
Pb14 O6 2.26(3) .
Pb14 O18 2.30(3) .
Pb14 O22 2.34(3) .
Pb15 O4 2.26(2) .
Pb15 O6 2.32(3) .
Pb15 O19 2.40(3) .
Pb15 Pb18 3.555(3) .
Pb15 Pb20 3.620(3) .
Pb16 O9 2.23(3) 2_766
Pb16 O12 2.26(2) 2_766
Pb16 O17 2.35(2) 2_766
Pb17 O5 2.26(2) .
Pb17 O18 2.29(3) .
Pb17 O13 2.29(3) .
Pb18 O6 2.30(3) .
Pb18 O4 2.31(3) .
Pb18 O7 2.37(3) .
Pb18 Pb19 3.616(3) .
Pb18 Pb20 3.657(3) .
Pb19 O7 2.30(3) .
Pb19 O4 2.39(3) .
Pb19 O19 2.39(3) .
Pb20 O6 2.27(3) .
Pb20 O19 2.37(3) .
Pb20 O7 2.42(3) .
Pb20 O52 2.76(3) .
O2 Pb4 2.24(2) 2_766
O4 Pb13 2.23(3) 2_575
O9 Pb16 2.23(3) 2_766
O9 Pb4 2.33(3) 2_766
O11 Pb3 2.22(3) 2_766
O11 Pb4 2.29(2) 2_766
O12 Pb3 2.21(2) 2_766
O12 Pb16 2.26(2) 2_766
O12 Pb8 2.32(2) 2_766
O12 Pb6 2.35(3) 2_766
O14 Pb8 2.33(3) 2_766
O14 Pb6 2.35(2) 2_766
O15 Pb8 2.25(2) 2_766
O15 Pb13 2.33(3) 2_676
O17 Pb3 2.34(2) 2_766
O17 Pb16 2.35(2) 2_766
O20 Pb13 2.25(2) 2_676
O20 Pb6 2.30(2) 2_766
O23 N2 1.23(4) .
O24 N1 1.20(4) .
O25 N3 1.23(4) .
O26 N4 1.26(4) .
O27 N2 1.25(4) .
O28 N4 1.20(4) .
O29 N3 1.28(4) .
O30 N4 1.24(4) .
O31 N2 1.26(4) .
O32 N7 1.26(4) .
O33 N8 1.24(4) .
O34 N5 1.27(4) .
O35 N7 1.30(4) .
O36 N5 1.21(4) .
O37 N6 1.22(5) .
O38 N7 1.22(4) .
O39 N5 1.23(5) .
O40 N12 1.16(4) .
O41 N8 1.29(5) .
O42 N8 1.22(5) .
O43 N6 1.15(4) .
O44 N3 1.17(3) .
O45 N11 1.20(4) .
O46 N6 1.35(4) .
O47 N11 1.33(4) .
O48 N10 1.28(4) 2_666
O49 N10 1.21(5) 2_666
O50 N10 1.25(5) .
O51 N9 1.25(5) .
O52 N12 1.23(4) .
O53 N12 1.26(5) .
O54 N1 1.25(4) .
O55 N11 1.18(4) .
O56 N1 1.20(4) .
O57 N9 1.15(5) .
O58 N9 1.17(5) .
N10 O49 1.21(5) 2_666
N10 O48 1.28(4) 2_666
