#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/89/4338924.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4338924
loop_
_publ_author_name
'Brylev, Konstantin A.'
'Mironov, Yuri V.'
'Yarovoi, Spartak S.'
'Naumov, Nikolai G.'
'Fedorov, Vladimir E.'
'Kim, Sung-Jin'
'Kitamura, Noboru'
'Kuwahara, Yusuke'
'Yamada, Konatsu'
'Ishizaka, Shoji'
'Sasaki, Yoichi'
_publ_section_title
;
 A family of octahedral rhenium cluster complexes [Re6Q8(H2O)n(OH)6-n]n-4
 (Q=S, Se; n=0-6): structural and pH-dependent spectroscopic studies.
;
_journal_issue                   18
_journal_name_full               'Inorganic chemistry'
_journal_page_first              7414
_journal_page_last               7422
_journal_paper_doi               10.1021/ic7005265
_journal_volume                  46
_journal_year                    2007
_chemical_formula_moiety         '[Re6S8(H2O)6][Re6S6Br8].10H2O'
_chemical_formula_sum            'Br8 H32 O16 Re12 S14'
_chemical_formula_weight         3610.78
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                99.966(2)
_cell_angle_beta                 90.343(3)
_cell_angle_gamma                115.183(2)
_cell_formula_units_Z            1
_cell_length_a                   9.1109(8)
_cell_length_b                   9.2467(8)
_cell_length_c                   15.8877(15)
_cell_measurement_temperature    153(2)
_cell_volume                     1188.21(19)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      153(2)
_diffrn_measured_fraction_theta_full 0.935
_diffrn_measured_fraction_theta_max 0.935
_diffrn_measurement_device_type  'Bruker Nonius X8Apex CCD area-detector'
_diffrn_measurement_method       'φ scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0380
_diffrn_reflns_av_sigmaI/netI    0.0721
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       7
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            8570
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         1.31
_diffrn_source                   'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu    37.804
_exptl_absorpt_correction_T_max  0.7037
_exptl_absorpt_correction_T_min  0.0647
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    5.046
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1564
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.01
_refine_diff_density_max         3.839
_refine_diff_density_min         -4.591
_refine_diff_density_rms         0.640
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.002
_refine_ls_matrix_type           full
_refine_ls_number_parameters     230
_refine_ls_number_reflns         5085
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.002
_refine_ls_R_factor_all          0.0669
_refine_ls_R_factor_gt           0.0463
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0772P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1254
_refine_ls_wR_factor_ref         0.1346
_reflns_number_gt                3857
_reflns_number_total             5085
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic7005265-file003.cif
_cod_data_source_block           compound3
_cod_original_cell_volume        1188.21(18)
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'H32 Br8 O16 Re12 S14'
_cod_database_code               4338924
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Re1 Re 0.65071(7) 0.94887(8) -0.05596(4) 0.01200(16) Uani 1 1 d .
Re2 Re 0.61014(7) 1.02955(8) 0.10247(4) 0.01160(16) Uani 1 1 d .
Re3 Re 0.62068(7) 1.21355(8) -0.00401(4) 0.01239(16) Uani 1 1 d .
Re4 Re 0.51223(7) 0.31189(7) 0.44854(4) 0.00916(15) Uani 1 1 d .
Re5 Re 0.52984(7) 0.56972(8) 0.39716(4) 0.00963(15) Uani 1 1 d .
Re6 Re 0.27852(7) 0.40098(8) 0.47242(4) 0.00998(16) Uani 1 1 d .
Br5 Br 0.7484(4) 0.4813(4) 0.3800(2) 0.0191(11) Uani 0.187(12) 1 d P
Br6 Br 0.3025(3) 0.6511(4) 0.42460(19) 0.0189(10) Uani 0.312(12) 1 d P
Br7 Br 0.2673(3) 0.1553(3) 0.52440(17) 0.0166(9) Uani 0.373(12) 1 d P
Br8 Br 0.3320(4) 0.2965(4) 0.3296(2) 0.0182(12) Uani 0.125(11) 1 d P
Br4t Br 0.52046(19) 0.0469(2) 0.37988(11) 0.0165(4) Uani 1 1 d .
Br5t Br 0.5760(2) 0.6759(2) 0.25802(11) 0.0205(4) Uani 1 1 d .
Br6t Br -0.02571(19) 0.2605(2) 0.43410(12) 0.0219(4) Uani 1 1 d .
S1 S 0.6303(5) 0.7807(5) 0.0474(3) 0.0175(9) Uani 1 1 d .
S2 S 0.8550(5) 1.1790(5) 0.0390(3) 0.0171(9) Uani 1 1 d .
S3 S 0.6500(5) 1.1244(5) -0.1524(3) 0.0141(8) Uani 1 1 d .
S4 S 0.4249(5) 0.7244(5) -0.1447(3) 0.0138(8) Uani 1 1 d .
S5 S 0.7484(4) 0.4813(4) 0.3800(2) 0.0191(11) Uani 0.813(12) 1 d P
S6 S 0.3025(3) 0.6511(4) 0.42460(19) 0.0189(10) Uani 0.688(12) 1 d P
S7 S 0.2673(3) 0.1553(3) 0.52440(17) 0.0166(9) Uani 0.627(12) 1 d P
S8 S 0.3320(4) 0.2965(4) 0.3296(2) 0.0182(12) Uani 0.875(11) 1 d P
O1 O 0.8275(15) 0.8820(16) -0.1179(8) 0.024(3) Uani 1 1 d .
O2 O 0.7483(13) 1.0787(15) 0.2221(7) 0.019(3) Uani 1 1 d .
O3 O 0.7699(16) 1.4633(15) -0.0064(8) 0.026(3) Uani 1 1 d .
O1W O 0.112(3) 0.3658(18) -0.1467(13) 0.071(7) Uani 1 1 d .
O2W O 0.2372(14) 0.4237(15) 0.1481(9) 0.025(3) Uani 1 1 d .
O3W O 1.012(2) 0.477(3) 0.2428(12) 0.075(7) Uani 1 1 d .
O4W O -0.0249(14) -0.0438(15) 0.2263(9) 0.024(3) Uani 1 1 d .
O5W O 0.0961(18) -0.162(2) 0.3473(11) 0.050(4) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Re1 S2 92.8(4) . .
O1 Re1 S1 90.5(4) . .
S2 Re1 S1 89.94(15) . .
O1 Re1 S4 92.9(4) . .
S2 Re1 S4 174.31(14) . .
S1 Re1 S4 90.02(15) . .
O1 Re1 S3 95.4(4) . .
S2 Re1 S3 89.92(15) . .
S1 Re1 S3 174.09(14) . .
S4 Re1 S3 89.54(14) . .
O1 Re1 Re3 136.8(4) . .
S2 Re1 Re3 57.63(11) . .
S1 Re1 Re3 117.49(11) . .
S4 Re1 Re3 117.57(10) . .
S3 Re1 Re3 57.77(10) . .
O1 Re1 Re2 133.1(3) . .
S2 Re1 Re2 57.76(11) . .
S1 Re1 Re2 57.51(11) . .
S4 Re1 Re2 117.75(10) . .
S3 Re1 Re2 117.75(10) . .
Re3 Re1 Re2 60.01(3) . .
O1 Re1 Re3 133.3(4) . 2_675
S2 Re1 Re3 117.77(11) . 2_675
S1 Re1 Re3 57.71(10) . 2_675
S4 Re1 Re3 57.73(10) . 2_675
S3 Re1 Re3 117.39(9) . 2_675
Re3 Re1 Re3 89.89(3) . 2_675
Re2 Re1 Re3 60.05(2) . 2_675
O1 Re1 Re2 136.8(3) . 2_675
S2 Re1 Re2 117.61(11) . 2_675
S1 Re1 Re2 117.53(10) . 2_675
S4 Re1 Re2 57.60(10) . 2_675
S3 Re1 Re2 57.56(9) . 2_675
Re3 Re1 Re2 60.00(2) . 2_675
Re2 Re1 Re2 90.03(3) . 2_675
Re3 Re1 Re2 59.85(2) 2_675 2_675
O2 Re2 S1 95.0(4) . .
O2 Re2 S2 90.5(3) . .
S1 Re2 S2 89.89(15) . .
O2 Re2 S3 95.3(3) . 2_675
S1 Re2 S3 89.79(14) . 2_675
S2 Re2 S3 174.21(14) . 2_675
O2 Re2 S4 90.6(4) . 2_675
S1 Re2 S4 174.39(14) . 2_675
S2 Re2 S4 89.93(14) . 2_675
S3 Re2 S4 89.83(14) 2_675 2_675
O2 Re2 Re3 131.7(3) . .
S1 Re2 Re3 117.67(11) . .
S2 Re2 Re3 57.53(11) . .
S3 Re2 Re3 117.77(10) 2_675 .
S4 Re2 Re3 57.82(10) 2_675 .
O2 Re2 Re1 134.6(3) . .
S1 Re2 Re1 57.73(10) . .
S2 Re2 Re1 57.45(10) . .
S3 Re2 Re1 117.80(10) 2_675 .
S4 Re2 Re1 117.77(10) 2_675 .
Re3 Re2 Re1 59.97(3) . .
O2 Re2 Re3 138.5(3) . 2_675
S1 Re2 Re3 57.77(10) . 2_675
S2 Re2 Re3 117.45(11) . 2_675
S3 Re2 Re3 57.79(10) 2_675 2_675
S4 Re2 Re3 117.59(10) 2_675 2_675
Re3 Re2 Re3 89.86(3) . 2_675
Re1 Re2 Re3 60.03(2) . 2_675
O2 Re2 Re1 135.2(3) . 2_675
S1 Re2 Re1 117.56(10) . 2_675
S2 Re2 Re1 117.47(11) . 2_675
S3 Re2 Re1 57.82(10) 2_675 2_675
S4 Re2 Re1 57.79(9) 2_675 2_675
Re3 Re2 Re1 59.97(2) . 2_675
Re1 Re2 Re1 89.97(3) . 2_675
Re3 Re2 Re1 59.82(3) 2_675 2_675
O3 Re3 S2 90.6(4) . .
O3 Re3 S1 95.2(4) . 2_675
S2 Re3 S1 174.20(15) . 2_675
O3 Re3 S3 93.1(4) . .
S2 Re3 S3 89.94(14) . .
S1 Re3 S3 89.49(14) 2_675 .
O3 Re3 S4 92.4(4) . 2_675
S2 Re3 S4 90.01(14) . 2_675
S1 Re3 S4 90.01(14) 2_675 2_675
S3 Re3 S4 174.50(14) . 2_675
O3 Re3 Re1 133.6(4) . .
S2 Re3 Re1 57.53(10) . .
S1 Re3 Re1 117.58(11) 2_675 .
S3 Re3 Re1 57.91(10) . .
S4 Re3 Re1 117.74(10) 2_675 .
O3 Re3 Re2 133.1(3) . .
S2 Re3 Re2 57.72(11) . .
S1 Re3 Re2 117.72(11) 2_675 .
S3 Re3 Re2 117.90(10) . .
S4 Re3 Re2 57.75(10) 2_675 .
Re1 Re3 Re2 60.01(3) . .
O3 Re3 Re1 136.3(4) . 2_675
S2 Re3 Re1 117.86(11) . 2_675
S1 Re3 Re1 57.58(11) 2_675 2_675
S3 Re3 Re1 117.56(10) . 2_675
S4 Re3 Re1 57.84(9) 2_675 2_675
Re1 Re3 Re1 90.11(3) . 2_675
Re2 Re3 Re1 60.17(2) . 2_675
O3 Re3 Re2 136.7(3) . 2_675
S2 Re3 Re2 117.68(11) . 2_675
S1 Re3 Re2 57.42(11) 2_675 2_675
S3 Re3 Re2 57.66(9) . 2_675
S4 Re3 Re2 117.73(10) 2_675 2_675
Re1 Re3 Re2 60.18(2) . 2_675
Re2 Re3 Re2 90.14(3) . 2_675
Re1 Re3 Re2 59.92(2) 2_675 2_675
Br8 Re4 Br5 89.75(12) . .
Br8 Re4 S6 175.50(11) . 2_666
Br5 Re4 S6 89.64(10) . 2_666
Br8 Re4 Br6 175.50(11) . 2_666
Br5 Re4 Br6 89.64(10) . 2_666
S6 Re4 Br6 0.00(16) 2_666 2_666
Br8 Re4 Br7 90.11(10) . .
Br5 Re4 Br7 175.93(10) . .
S6 Re4 Br7 90.19(9) 2_666 .
Br6 Re4 Br7 90.19(9) 2_666 .
Br8 Re4 Br4t 92.38(10) . .
Br5 Re4 Br4t 94.13(9) . .
S6 Re4 Br4t 92.11(8) 2_666 .
Br6 Re4 Br4t 92.11(8) 2_666 .
Br7 Re4 Br4t 89.94(7) . .
Br8 Re4 Re5 57.85(9) . .
Br5 Re4 Re5 58.10(8) . .
S6 Re4 Re5 118.25(7) 2_666 .
Br6 Re4 Re5 118.25(7) 2_666 .
Br7 Re4 Re5 118.60(6) . .
Br4t Re4 Re5 136.14(5) . .
Br8 Re4 Re6 57.94(9) . .
Br5 Re4 Re6 118.12(8) . .
S6 Re4 Re6 118.66(7) 2_666 .
Br6 Re4 Re6 118.66(7) 2_666 .
Br7 Re4 Re6 58.58(6) . .
Br4t Re4 Re6 133.50(5) . .
Re5 Re4 Re6 60.04(2) . .
Br8 Re4 Re6 117.96(9) . 2_666
Br5 Re4 Re6 58.36(8) . 2_666
S6 Re4 Re6 58.12(7) 2_666 2_666
Br6 Re4 Re6 58.12(7) 2_666 2_666
Br7 Re4 Re6 118.31(7) . 2_666
Br4t Re4 Re6 136.46(4) . 2_666
Re5 Re4 Re6 60.13(2) . 2_666
Re6 Re4 Re6 90.00(3) . 2_666
Br8 Re5 Br5 89.80(12) . .
Br8 Re5 Br6 89.65(11) . .
Br5 Re5 Br6 175.71(11) . .
Br8 Re5 S7 176.34(11) . 2_666
Br5 Re5 S7 89.66(10) . 2_666
Br6 Re5 S7 90.61(9) . 2_666
Br8 Re5 Br7 176.34(11) . 2_666
Br5 Re5 Br7 89.66(10) . 2_666
Br6 Re5 Br7 90.61(9) . 2_666
S7 Re5 Br7 0.00(18) 2_666 2_666
Br8 Re5 Br5t 94.30(10) . .
Br5 Re5 Br5t 92.65(9) . .
Br6 Re5 Br5t 91.63(8) . .
S7 Re5 Br5t 89.34(8) 2_666 .
Br7 Re5 Br5t 89.34(8) 2_666 .
Br8 Re5 Re4 57.95(9) . .
Br5 Re5 Re4 58.09(8) . .
Br6 Re5 Re4 118.22(7) . .
S7 Re5 Re4 118.86(7) 2_666 .
Br7 Re5 Re4 118.86(7) 2_666 .
Br5t Re5 Re4 136.51(5) . .
Br8 Re5 Re6 57.99(9) . .
Br5 Re5 Re6 118.15(8) . .
Br6 Re5 Re6 58.16(7) . .
S7 Re5 Re6 119.28(7) 2_666 .
Br7 Re5 Re6 119.28(7) 2_666 .
Br5t Re5 Re6 135.94(5) . .
Re4 Re5 Re6 60.07(2) . .
Br8 Re5 Re6 118.03(9) . 2_666
Br5 Re5 Re6 58.34(8) . 2_666
Br6 Re5 Re6 118.38(8) . 2_666
S7 Re5 Re6 58.76(6) 2_666 2_666
Br7 Re5 Re6 58.76(6) 2_666 2_666
Br5t Re5 Re6 134.01(5) . 2_666
Re4 Re5 Re6 60.10(2) . 2_666
Re6 Re5 Re6 90.01(3) . 2_666
Br8 Re6 S5 174.78(11) . 2_666
Br8 Re6 Br5 174.78(11) . 2_666
S5 Re6 Br5 0.00(18) 2_666 2_666
Br8 Re6 Br6 90.06(11) . .
S5 Re6 Br6 89.79(11) 2_666 .
Br5 Re6 Br6 89.79(11) 2_666 .
Br8 Re6 Br7 90.55(11) . .
S5 Re6 Br7 89.36(10) 2_666 .
Br5 Re6 Br7 89.36(10) 2_666 .
Br6 Re6 Br7 177.33(9) . .
Br8 Re6 Br6t 92.15(10) . .
S5 Re6 Br6t 93.07(9) 2_666 .
Br5 Re6 Br6t 93.07(9) 2_666 .
Br6 Re6 Br6t 92.18(8) . .
Br7 Re6 Br6t 90.40(8) . .
Br8 Re6 Re5 57.76(8) . .
S5 Re6 Re5 117.96(8) 2_666 .
Br5 Re6 Re5 117.96(8) 2_666 .
Br6 Re6 Re5 59.04(7) . .
Br7 Re6 Re5 119.29(6) . .
Br6t Re6 Re5 135.20(5) . .
Br8 Re6 Re4 57.82(9) . .
S5 Re6 Re4 117.94(8) 2_666 .
Br5 Re6 Re4 117.94(8) 2_666 .
Br6 Re6 Re4 118.92(7) . .
Br7 Re6 Re4 59.41(6) . .
Br6t Re6 Re4 134.08(5) . .
Re5 Re6 Re4 59.89(2) . .
Br8 Re6 Re4 117.91(9) . 2_666
S5 Re6 Re4 57.81(8) 2_666 2_666
Br5 Re6 Re4 57.81(8) 2_666 2_666
Br6 Re6 Re4 58.91(7) . 2_666
Br7 Re6 Re4 118.57(7) . 2_666
Br6t Re6 Re4 135.93(5) . 2_666
Re5 Re6 Re4 60.18(2) . 2_666
Re4 Re6 Re4 90.00(3) . 2_666
Re4 Br5 Re5 63.81(9) . .
Re4 Br5 Re6 63.84(9) . 2_666
Re5 Br5 Re6 63.86(9) . 2_666
Re6 Br6 Re4 62.97(8) . 2_666
Re6 Br6 Re5 62.81(8) . .
Re4 Br6 Re5 62.77(8) 2_666 .
Re6 Br7 Re5 62.43(7) . 2_666
Re6 Br7 Re4 62.01(7) . .
Re5 Br7 Re4 62.22(7) 2_666 .
Re5 Br8 Re4 64.20(9) . .
Re5 Br8 Re6 64.25(10) . .
Re4 Br8 Re6 64.24(10) . .
Re2 S1 Re1 64.77(12) . .
Re2 S1 Re3 64.81(11) . 2_675
Re1 S1 Re3 64.72(11) . 2_675
Re1 S2 Re3 64.84(11) . .
Re1 S2 Re2 64.79(10) . .
Re3 S2 Re2 64.75(11) . .
Re2 S3 Re3 64.55(10) 2_675 .
Re2 S3 Re1 64.62(10) 2_675 .
Re3 S3 Re1 64.31(11) . .
Re2 S4 Re3 64.42(10) 2_675 2_675
Re2 S4 Re1 64.61(10) 2_675 .
Re3 S4 Re1 64.44(10) 2_675 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Re1 O1 2.145(12) .
Re1 S2 2.398(4) .
Re1 S1 2.406(4) .
Re1 S4 2.418(4) .
Re1 S3 2.419(4) .
Re1 Re3 2.5728(10) .
Re1 Re2 2.5739(9) .
Re1 Re3 2.5770(9) 2_675
Re1 Re2 2.5821(9) 2_675
Re2 O2 2.142(11) .
Re2 S1 2.400(4) .
Re2 S2 2.406(4) .
Re2 S3 2.412(4) 2_675
Re2 S4 2.413(4) 2_675
Re2 Re3 2.5739(9) .
Re2 Re3 2.5773(9) 2_675
Re2 Re1 2.5821(9) 2_675
Re3 O3 2.132(13) .
Re3 S2 2.401(4) .
Re3 S1 2.409(4) 2_675
Re3 S3 2.415(4) .
Re3 S4 2.415(4) 2_675
Re3 Re1 2.5770(9) 2_675
Re3 Re2 2.5773(9) 2_675
Re4 Br8 2.442(4) .
Re4 Br5 2.453(3) .
Re4 S6 2.501(3) 2_666
Re4 Br6 2.501(3) 2_666
Re4 Br7 2.533(3) .
Re4 Br4t 2.5359(18) .
Re4 Re5 2.5934(9) .
Re4 Re6 2.5982(9) .
Re4 Re6 2.6020(9) 2_666
Re5 Br8 2.439(4) .
Re5 Br5 2.454(3) .
Re5 Br6 2.504(3) .
Re5 S7 2.512(3) 2_666
Re5 Br7 2.512(3) 2_666
Re5 Br5t 2.5374(18) .
Re5 Re6 2.5972(8) .
Re5 Re6 2.6029(9) 2_666
Re6 Br8 2.445(4) .
Re6 S5 2.468(4) 2_666
Re6 Br5 2.468(4) 2_666
Re6 Br6 2.480(3) .
Re6 Br7 2.511(3) .
Re6 Br6t 2.5264(17) .
Re6 Re4 2.6020(9) 2_666
Br5 Re6 2.468(4) 2_666
Br6 Re4 2.501(3) 2_666
Br7 Re5 2.512(3) 2_666
S1 Re3 2.409(4) 2_675
S3 Re2 2.412(4) 2_675
S4 Re2 2.413(4) 2_675
S4 Re3 2.415(4) 2_675
