#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:07:58 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180004 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/98/7029800.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029800
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.324(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   21.9362(7)
_cell_length_b                   16.7329(5)
_cell_length_c                   25.5715(11)
_cell_measurement_reflns_used    8995
_cell_measurement_temperature    440.01(10)
_cell_measurement_theta_max      28.7850
_cell_measurement_theta_min      3.1720
_cell_volume                     8484.2(6)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      440.01(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.972
_diffrn_measured_fraction_theta_max 0.972
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0292
_diffrn_reflns_av_sigmaI/netI    0.0325
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            19701
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.06
_exptl_absorpt_coefficient_mu    2.132
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.76672
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            crimson
_exptl_crystal_density_diffrn    2.242
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.33
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.857
_refine_diff_density_min         -1.010
_refine_diff_density_rms         0.142
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.071
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7274
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.071
_refine_ls_R_factor_all          0.0585
_refine_ls_R_factor_gt           0.0472
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0812P)²+43.3086P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1357
_refine_ls_wR_factor_ref         0.1465
_reflns_number_gt                5957
_reflns_number_total             7274
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           A_440K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029800.cif.
;
_cod_original_cell_volume        8484.2(5)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029800
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.34428(3) -0.04164(4) -0.63233(3) 0.0577(2) Uani 1 1 d .
Ag2 Ag 0.32166(3) 0.25405(5) -0.13281(3) 0.0658(2) Uani 1 1 d .
C9 C 0.5974(3) 0.4705(4) 0.0000(3) 0.0342(14) Uani 1 1 d .
C10 C 0.1235(3) 0.2563(4) -0.4990(3) 0.0340(14) Uani 1 1 d .
C15 C 0.0329(4) 0.3109(5) -0.5899(3) 0.0475(18) Uani 1 1 d .
H15A H 0.0541 0.2897 -0.6114 0.057 Uiso 1 1 calc R
C18 C 0.7201(3) 0.6503(4) -0.1083(3) 0.0417(15) Uani 1 1 d .
H18A H 0.7006 0.6540 -0.1485 0.050 Uiso 1 1 calc R
C19 C 0.0602(3) 0.3014(4) -0.5313(3) 0.0359(14) Uani 1 1 d .
C21 C 0.5027(3) 0.3844(4) -0.0047(3) 0.0404(15) Uani 1 1 d .
H21A H 0.5222 0.3837 0.0355 0.048 Uiso 1 1 calc R
C22 C 0.5327(3) 0.4261(4) -0.0341(3) 0.0340(13) Uani 1 1 d .
C23 C 0.2978(3) 0.0839(4) -0.4950(3) 0.0398(15) Uani 1 1 d .
H23A H 0.3199 0.0875 -0.4549 0.048 Uiso 1 1 calc R
C25 C 0.4435(3) 0.3438(4) -0.0358(3) 0.0432(16) Uani 1 1 d .
H25A H 0.4236 0.3163 -0.0155 0.052 Uiso 1 1 calc R
C26 C 0.6813(3) 0.5515(4) 0.0058(3) 0.0348(14) Uani 1 1 d .
C27 C 0.2097(3) 0.2253(4) -0.4134(3) 0.0362(14) Uani 1 1 d .
C28 C 0.7767(4) 0.6376(4) 0.0088(3) 0.0458(16) Uani 1 1 d .
H28A H 0.7975 0.6348 0.0489 0.055 Uiso 1 1 calc R
C32 C 0.2361(3) 0.0658(4) -0.6112(3) 0.0447(16) Uani 1 1 d .
H32A H 0.2145 0.0591 -0.6511 0.054 Uiso 1 1 calc R
C35 C 0.7113(3) 0.4929(4) 0.1511(3) 0.0414(15) Uani 1 1 d .
C36 C 0.2426(3) 0.2359(4) -0.3498(3) 0.0425(16) Uani 1 1 d .
C37 C 0.0256(3) 0.3347(5) -0.5018(3) 0.0482(18) Uani 1 1 d .
H37A H 0.0423 0.3295 -0.4619 0.058 Uiso 1 1 calc R
C38 C -0.0328(4) 0.3745(5) -0.5321(3) 0.0535(19) Uani 1 1 d .
H38A H -0.0547 0.3970 -0.5116 0.064 Uiso 1 1 calc R
C39 C 0.6792(3) 0.5017(4) 0.0868(3) 0.0386(15) Uani 1 1 d .
C40 C 0.7144(3) 0.6006(4) -0.0233(3) 0.0359(14) Uani 1 1 d .
C41 C 0.2054(3) 0.1725(4) -0.4955(3) 0.0346(14) Uani 1 1 d .
C42 C 0.6782(4) 0.4572(5) 0.1798(3) 0.059(2) Uani 1 1 d .
H42A H 0.6342 0.4392 0.1596 0.070 Uiso 1 1 calc R
C43 C 0.2356(3) 0.1219(4) -0.5259(3) 0.0368(14) Uani 1 1 d .
C45 C 0.3254(3) 0.0410(4) -0.5257(3) 0.0403(15) Uani 1 1 d .
H45A H 0.3675 0.0177 -0.5052 0.048 Uiso 1 1 calc R
C47 C 0.6866(3) 0.6084(4) -0.0823(3) 0.0397(15) Uani 1 1 d .
H47A H 0.6450 0.5854 -0.1048 0.048 Uiso 1 1 calc R
C48 C -0.0268(3) 0.3524(5) -0.6166(3) 0.0502(18) Uani 1 1 d .
H48A H -0.0446 0.3592 -0.6565 0.060 Uiso 1 1 calc R
C49 C 0.2044(4) 0.1112(4) -0.5855(3) 0.0455(16) Uani 1 1 d .
H49A H 0.1626 0.1344 -0.6075 0.055 Uiso 1 1 calc R
C50 C 0.5016(3) 0.4254(5) -0.0934(3) 0.0469(17) Uani 1 1 d .
H50A H 0.5197 0.4539 -0.1146 0.056 Uiso 1 1 calc R
C51 C 0.8052(4) 0.5062(6) 0.2417(3) 0.061(2) Uani 1 1 d .
H51A H 0.8492 0.5238 0.2629 0.074 Uiso 1 1 calc R
C52 C 0.8065(4) 0.6790(5) -0.0219(3) 0.0503(18) Uani 1 1 d .
H52A H 0.8481 0.7032 -0.0009 0.060 Uiso 1 1 calc R
C53 C 0.7109(4) 0.4482(6) 0.2392(3) 0.064(2) Uani 1 1 d .
H53A H 0.6878 0.4244 0.2583 0.077 Uiso 1 1 calc R
C55 C 0.7771(4) 0.5176(5) 0.1826(3) 0.055(2) Uani 1 1 d .
H55A H 0.8016 0.5411 0.1647 0.066 Uiso 1 1 calc R
C56 C 0.4435(4) 0.3819(5) -0.1211(3) 0.0526(19) Uani 1 1 d .
H56A H 0.4240 0.3801 -0.1613 0.063 Uiso 1 1 calc R
C57 C 0.2150(4) 0.2868(5) -0.3233(3) 0.057(2) Uani 1 1 d .
H57A H 0.1764 0.3161 -0.3452 0.069 Uiso 1 1 calc R
C58 C 0.3011(4) 0.1965(5) -0.3157(3) 0.057(2) Uani 1 1 d .
H58A H 0.3229 0.1643 -0.3321 0.068 Uiso 1 1 calc R
C59 C 0.3267(4) 0.2057(6) -0.2569(4) 0.070(3) Uani 1 1 d .
H59A H 0.3659 0.1779 -0.2344 0.083 Uiso 1 1 calc R
C60 C 0.2453(5) 0.2935(6) -0.2639(3) 0.064(2) Uani 1 1 d .
H60A H 0.2271 0.3291 -0.2464 0.076 Uiso 1 1 calc R
N1 N 0.2958(3) 0.0308(3) -0.5827(2) 0.0409(13) Uani 1 1 d .
N2 N -0.0606(3) 0.3834(4) -0.5891(3) 0.0467(14) Uani 1 1 d .
N3 N 0.3002(3) 0.2509(4) -0.2298(3) 0.0593(18) Uani 1 1 d .
N4 N 0.1480(3) 0.2110(3) -0.5283(2) 0.0384(12) Uani 1 1 d .
N5 N 0.1527(3) 0.2669(3) -0.4418(2) 0.0408(13) Uani 1 1 d .
N6 N 0.2377(3) 0.1771(3) -0.4379(2) 0.0394(13) Uani 1 1 d .
N7 N 0.7794(3) 0.6857(3) -0.0784(3) 0.0433(14) Uani 1 1 d .
N8 N 0.4134(3) 0.3420(4) -0.0932(3) 0.0472(14) Uani 1 1 d .
N9 N 0.7746(3) 0.4725(4) 0.2704(3) 0.0563(17) Uani 1 1 d .
N10 N 0.6252(3) 0.5116(3) -0.0277(2) 0.0381(12) Uani 1 1 d .
N11 N 0.6224(3) 0.4626(3) 0.0578(2) 0.0397(13) Uani 1 1 d .
N12 N 0.7104(3) 0.5492(4) 0.0637(2) 0.0434(13) Uani 1 1 d .
Mo1 Mo 0.5000 -0.03266(7) -0.7500 0.0621(3) Uani 1 2 d S
Mo2 Mo 0.49853(3) 0.09036(4) -0.63926(2) 0.03877(17) Uani 1 1 d .
Mo3 Mo 0.49121(3) 0.28991(4) -0.64280(3) 0.04095(18) Uani 1 1 d .
Mo4 Mo 0.5000 0.40333(7) -0.7500 0.0579(3) Uani 1 2 d S
Mo5 Mo 0.40745(3) 0.19301(3) -0.79047(3) 0.03757(17) Uani 1 1 d .
O1 O 0.5634(7) -0.0939(7) -0.7072(7) 0.185(6) Uani 1 1 d .
O2 O 0.4659(3) 0.0164(4) -0.7056(3) 0.0657(15) Uani 1 1 d .
O3 O 0.4273(3) 0.0824(5) -0.6304(3) 0.0796(19) Uani 1 1 d .
O4 O 0.5534(3) 0.0300(5) -0.5861(3) 0.088(2) Uani 1 1 d .
O5 O 0.5330(3) 0.1903(4) -0.6066(2) 0.0631(15) Uani 1 1 d .
O6 O 0.4471(4) 0.1871(4) -0.7148(3) 0.0722(17) Uani 1 1 d .
O7 O 0.4241(3) 0.1056(4) -0.8225(3) 0.0769(18) Uani 1 1 d .
O8 O 0.3228(3) 0.1975(4) -0.8183(3) 0.0734(18) Uani 1 1 d .
O9 O 0.4219(3) 0.2876(5) -0.6291(3) 0.085(2) Uani 1 1 d .
O10 O 0.5433(3) 0.3511(5) -0.5924(3) 0.089(2) Uani 1 1 d .
O11 O 0.4528(3) 0.3572(4) -0.7111(3) 0.0725(17) Uani 1 1 d .
O12 O 0.4349(3) 0.2810(4) -0.8152(3) 0.0674(16) Uani 1 1 d .
O13 O 0.5587(4) 0.4632(5) -0.7013(3) 0.102(2) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Ag1 N9 128.9(2) 3_545 3_444
N2 Ag1 N1 124.3(2) 3_545 .
N9 Ag1 N1 106.8(2) 3_444 .
N7 Ag2 N3 133.8(2) 3_445 .
N7 Ag2 N8 123.2(2) 3_445 .
N3 Ag2 N8 102.8(2) . .
N10 C9 N11 125.4(6) . .
N10 C9 C22 119.3(6) . .
N11 C9 C22 115.3(6) . .
N4 C10 N5 125.0(6) . .
N4 C10 C19 119.0(5) . .
N5 C10 C19 116.0(6) . .
C19 C15 C48 118.8(6) . .
N7 C18 C47 122.7(6) . .
C15 C19 C37 117.5(6) . .
C15 C19 C10 122.5(6) . .
C37 C19 C10 120.0(6) . .
C25 C21 C22 119.2(6) . .
C50 C22 C21 118.0(6) . .
C50 C22 C9 123.0(6) . .
C21 C22 C9 119.1(6) . .
C45 C23 C43 118.1(6) . .
N8 C25 C21 123.3(6) . .
N10 C26 N12 124.5(6) . .
N10 C26 C40 117.8(6) . .
N12 C26 C40 117.7(6) . .
N6 C27 N5 125.1(6) . .
N6 C27 C36 119.1(6) . .
N5 C27 C36 115.9(6) . .
C52 C28 C40 117.6(7) . .
N1 C32 C49 124.2(7) . .
C42 C35 C55 118.5(7) . .
C42 C35 C39 121.6(6) . .
C55 C35 C39 119.8(6) . .
C58 C36 C57 118.2(7) . .
C58 C36 C27 121.6(6) . .
C57 C36 C27 120.2(6) . .
C38 C37 C19 119.2(6) . .
N2 C38 C37 124.1(7) . .
N11 C39 N12 125.9(6) . .
N11 C39 C35 117.2(6) . .
N12 C39 C35 116.9(6) . .
C47 C40 C28 117.7(6) . .
C47 C40 C26 121.4(6) . .
C28 C40 C26 120.9(6) . .
N6 C41 N4 125.1(6) . .
N6 C41 C43 117.9(5) . .
N4 C41 C43 117.0(6) . .
C35 C42 C53 119.4(7) . .
C49 C43 C23 117.7(6) . .
C49 C43 C41 121.8(6) . .
C23 C43 C41 120.4(6) . .
N1 C45 C23 124.3(6) . .
C40 C47 C18 120.3(6) . .
N2 C48 C15 124.2(7) . .
C32 C49 C43 118.9(6) . .
C56 C50 C22 119.3(7) . .
N9 C51 C55 125.1(7) . .
N7 C52 C28 124.0(7) . .
N9 C53 C42 122.7(8) . .
C51 C55 C35 117.7(7) . .
N8 C56 C50 123.3(7) . .
C36 C57 C60 119.0(7) . .
C59 C58 C36 118.4(7) . .
N3 C59 C58 125.2(8) . .
N3 C60 C57 123.1(7) . .
C45 N1 C32 116.7(6) . .
C45 N1 Ag1 123.0(4) . .
C32 N1 Ag1 120.4(5) . .
C48 N2 C38 116.2(6) . .
C48 N2 Ag1 124.1(5) . 3_455
C38 N2 Ag1 119.4(5) . 3_455
C59 N3 C60 115.8(7) . .
C59 N3 Ag2 130.0(6) . .
C60 N3 Ag2 113.3(5) . .
C10 N4 C41 114.7(5) . .
C10 N5 C27 115.1(6) . .
C27 N6 C41 115.1(5) . .
C52 N7 C18 117.8(6) . .
C52 N7 Ag2 127.2(5) . 3
C18 N7 Ag2 115.1(5) . 3
C25 N8 C56 116.9(6) . .
C25 N8 Ag2 115.0(5) . .
C56 N8 Ag2 127.6(5) . .
C51 N9 C53 116.6(7) . .
C51 N9 Ag1 112.6(5) . 3_556
C53 N9 Ag1 130.7(5) . 3_556
C9 N10 C26 115.5(6) . .
C39 N11 C9 114.3(6) . .
C39 N12 C26 114.3(6) . .
O1 Mo1 O1 105.7(11) 2_653 .
O1 Mo1 O2 108.4(5) 2_653 2_653
O1 Mo1 O2 103.6(4) . 2_653
O1 Mo1 O2 103.6(4) 2_653 .
O1 Mo1 O2 108.4(5) . .
O2 Mo1 O2 125.8(4) 2_653 .
O3 Mo2 O4 103.0(3) . .
O3 Mo2 O5 103.4(3) . .
O4 Mo2 O5 99.2(3) . .
O3 Mo2 O2 92.9(3) . .
O4 Mo2 O2 100.7(3) . .
O5 Mo2 O2 150.6(3) . .
O3 Mo2 O7 164.3(3) . 2_653
O4 Mo2 O7 90.4(3) . 2_653
O5 Mo2 O7 82.0(3) . 2_653
O2 Mo2 O7 76.5(2) . 2_653
O3 Mo2 O6 91.0(3) . .
O4 Mo2 O6 165.5(3) . .
O5 Mo2 O6 73.6(2) . .
O2 Mo2 O6 81.9(2) . .
O7 Mo2 O6 76.2(2) 2_653 .
O10 Mo3 O9 103.5(3) . .
O10 Mo3 O5 97.6(4) . .
O9 Mo3 O5 99.5(3) . .
O10 Mo3 O11 103.3(4) . .
O9 Mo3 O11 96.7(3) . .
O5 Mo3 O11 149.8(2) . .
O10 Mo3 O12 90.8(3) . 2_653
O9 Mo3 O12 164.8(3) . 2_653
O5 Mo3 O12 83.3(2) . 2_653
O11 Mo3 O12 74.9(2) . 2_653
O10 Mo3 O6 162.8(3) . .
O9 Mo3 O6 92.3(3) . .
O5 Mo3 O6 72.7(2) . .
O11 Mo3 O6 81.3(2) . .
O12 Mo3 O6 74.2(2) 2_653 .
O13 Mo4 O13 107.1(6) . 2_653
O13 Mo4 O11 105.8(4) . .
O13 Mo4 O11 102.4(3) 2_653 .
O13 Mo4 O11 102.4(3) . 2_653
O13 Mo4 O11 105.8(4) 2_653 2_653
O11 Mo4 O11 131.6(4) . 2_653
O8 Mo5 O6 114.0(3) . .
O8 Mo5 O7 104.4(3) . .
O6 Mo5 O7 111.0(3) . .
O8 Mo5 O12 106.8(3) . .
O6 Mo5 O12 110.5(3) . .
O7 Mo5 O12 110.0(3) . .
Mo1 O2 Mo2 137.1(3) . .
Mo2 O5 Mo3 122.4(3) . .
Mo5 O6 Mo3 130.8(3) . .
Mo5 O6 Mo2 140.1(3) . .
Mo3 O6 Mo2 88.3(2) . .
Mo5 O7 Mo2 128.1(3) . 2_653
Mo4 O11 Mo3 126.0(3) . .
Mo5 O12 Mo3 128.6(3) . 2_653
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N2 2.276(5) 3_545
Ag1 N9 2.307(6) 3_444
Ag1 N1 2.316(5) .
Ag2 N7 2.282(5) 3_445
Ag2 N3 2.318(6) .
Ag2 N8 2.344(6) .
C9 N10 1.310(8) .
C9 N11 1.347(8) .
C9 C22 1.504(9) .
C10 N4 1.331(8) .
C10 N5 1.335(8) .
C10 C19 1.483(9) .
C15 C19 1.365(10) .
C15 C48 1.378(10) .
C18 N7 1.333(9) .
C18 C47 1.376(9) .
C19 C37 1.394(9) .
C21 C25 1.378(9) .
C21 C22 1.382(9) .
C22 C50 1.373(9) .
C23 C45 1.381(9) .
C23 C43 1.403(9) .
C25 N8 1.328(9) .
C26 N10 1.337(8) .
C26 N12 1.340(8) .
C26 C40 1.490(9) .
C27 N6 1.321(8) .
C27 N5 1.340(8) .
C27 C36 1.482(9) .
C28 C52 1.398(10) .
C28 C40 1.403(9) .
C32 N1 1.331(9) .
C32 C49 1.375(10) .
C35 C42 1.371(10) .
C35 C55 1.381(10) .
C35 C39 1.494(9) .
C36 C58 1.373(10) .
C36 C57 1.380(10) .
C37 C38 1.354(10) .
C38 N2 1.326(9) .
C39 N11 1.318(8) .
C39 N12 1.339(8) .
C40 C47 1.369(9) .
C41 N6 1.336(9) .
C41 N4 1.343(8) .
C41 C43 1.484(9) .
C42 C53 1.382(11) .
C43 C49 1.388(10) .
C45 N1 1.329(9) .
C48 N2 1.327(9) .
C50 C56 1.372(10) .
C51 N9 1.316(10) .
C51 C55 1.379(11) .
C52 N7 1.312(10) .
C53 N9 1.342(10) .
C56 N8 1.341(9) .
C57 C60 1.378(11) .
C58 C59 1.369(11) .
C59 N3 1.318(11) .
C60 N3 1.349(11) .
N2 Ag1 2.276(5) 3_455
N7 Ag2 2.282(5) 3
N9 Ag1 2.307(6) 3_556
Mo1 O1 1.697(10) 2_653
Mo1 O1 1.697(10) .
Mo1 O2 1.801(6) 2_653
Mo1 O2 1.801(6) .
Mo2 O3 1.676(6) .
Mo2 O4 1.707(6) .
Mo2 O5 1.878(6) .
Mo2 O2 1.971(6) .
Mo2 O7 2.306(6) 2_653
Mo2 O6 2.400(6) .
Mo3 O10 1.661(6) .
Mo3 O9 1.699(6) .
Mo3 O5 1.936(6) .
Mo3 O11 1.942(6) .
Mo3 O12 2.300(6) 2_653
Mo3 O6 2.400(6) .
Mo4 O13 1.686(8) .
Mo4 O13 1.686(8) 2_653
Mo4 O11 1.881(6) .
Mo4 O11 1.881(6) 2_653
Mo5 O8 1.681(5) .
Mo5 O6 1.752(6) .
Mo5 O7 1.789(7) .
Mo5 O12 1.804(6) .
O7 Mo2 2.306(6) 2_653
O12 Mo3 2.300(6) 2_653
