#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:07:58 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180004 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/98/7029806.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029806
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.311(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   22.0639(8)
_cell_length_b                   16.3382(4)
_cell_length_c                   25.6170(10)
_cell_measurement_reflns_used    15032
_cell_measurement_temperature    190.00(10)
_cell_measurement_theta_max      29.2530
_cell_measurement_theta_min      3.2280
_cell_volume                     8348.0(6)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      190.00(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.958
_diffrn_measured_fraction_theta_max 0.958
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0281
_diffrn_reflns_av_sigmaI/netI    0.0346
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            17987
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.07
_exptl_absorpt_coefficient_mu    2.166
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.59944
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.279
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.31
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.09
_refine_diff_density_max         1.845
_refine_diff_density_min         -1.464
_refine_diff_density_rms         0.132
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.057
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7055
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.057
_refine_ls_R_factor_all          0.0409
_refine_ls_R_factor_gt           0.0338
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0400P)²+55.7980P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0840
_refine_ls_wR_factor_ref         0.0898
_reflns_number_gt                6123
_reflns_number_total             7055
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           B_190K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029806.cif.
;
_cod_original_cell_volume        8348.0(5)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029806
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag -0.15593(2) 0.45744(3) -0.632172(17) 0.02545(12) Uani 1 1 d .
Ag2 Ag 0.32296(2) 0.25214(3) -0.132750(17) 0.02823(12) Uani 1 1 d .
Mo1 Mo 0.0000 0.46060(5) -0.7500 0.03375(19) Uani 1 2 d S
Mo2 Mo -0.00134(2) 0.58828(3) -0.639542(18) 0.01730(11) Uani 1 1 d .
Mo3 Mo -0.01051(2) 0.79168(3) -0.643672(19) 0.01779(11) Uani 1 1 d .
Mo4 Mo 0.0000 0.90534(5) -0.7500 0.02887(17) Uani 1 2 d S
Mo5 Mo -0.09146(2) 0.69332(3) -0.790980(19) 0.01683(11) Uani 1 1 d .
C16 C 0.1237(2) 0.2570(3) -0.4976(2) 0.0142(10) Uani 1 1 d .
C22 C 0.7780(3) 0.6377(3) 0.0092(2) 0.0211(11) Uani 1 1 d .
H22A H 0.7987 0.6341 0.0493 0.025 Uiso 1 1 calc R
C24 C 0.2351(3) 0.0650(3) -0.6117(2) 0.0201(11) Uani 1 1 d .
H24A H 0.2132 0.0583 -0.6515 0.024 Uiso 1 1 calc R
C25 C 0.5978(2) 0.4700(3) 0.0010(2) 0.0159(10) Uani 1 1 d .
C26 C 0.2981(2) 0.0842(3) -0.4951(2) 0.0173(11) Uani 1 1 d .
H26A H 0.3204 0.0886 -0.4551 0.021 Uiso 1 1 calc R
C28 C 0.0331(3) 0.3122(3) -0.5889(2) 0.0223(12) Uani 1 1 d .
H28A H 0.0545 0.2908 -0.6101 0.027 Uiso 1 1 calc R
C29 C 0.4437(3) 0.3430(3) -0.0351(2) 0.0214(11) Uani 1 1 d .
H29A H 0.4236 0.3148 -0.0152 0.026 Uiso 1 1 calc R
C30 C 0.5034(2) 0.3835(3) -0.0035(2) 0.0171(10) Uani 1 1 d .
H30A H 0.5230 0.3821 0.0367 0.021 Uiso 1 1 calc R
C32 C 0.0600(2) 0.3022(3) -0.5298(2) 0.0167(10) Uani 1 1 d .
C34 C 0.2099(2) 0.2269(3) -0.4123(2) 0.0179(11) Uani 1 1 d .
C35 C 0.6789(3) 0.4561(4) 0.1813(2) 0.0276(13) Uani 1 1 d .
H35A H 0.6348 0.4385 0.1614 0.033 Uiso 1 1 calc R
C36 C 0.7198(2) 0.6520(3) -0.1079(2) 0.0197(11) Uani 1 1 d .
H36A H 0.6998 0.6563 -0.1480 0.024 Uiso 1 1 calc R
C37 C 0.6825(2) 0.5518(3) 0.0068(2) 0.0166(10) Uani 1 1 d .
C38 C 0.5334(2) 0.4262(3) -0.0329(2) 0.0149(10) Uani 1 1 d .
C39 C 0.6805(2) 0.5021(3) 0.0883(2) 0.0166(10) Uani 1 1 d .
C40 C 0.2436(2) 0.2374(3) -0.3483(2) 0.0192(11) Uani 1 1 d .
C41 C 0.0261(3) 0.3356(3) -0.5000(2) 0.0214(11) Uani 1 1 d .
H41A H 0.0434 0.3309 -0.4601 0.026 Uiso 1 1 calc R
C42 C 0.7155(2) 0.6011(3) -0.0224(2) 0.0158(10) Uani 1 1 d .
C43 C 0.3259(2) 0.0409(3) -0.5259(2) 0.0189(11) Uani 1 1 d .
H43A H 0.3681 0.0177 -0.5057 0.023 Uiso 1 1 calc R
C44 C 0.6857(2) 0.6096(3) -0.0815(2) 0.0170(10) Uani 1 1 d .
H44A H 0.6436 0.5874 -0.1034 0.020 Uiso 1 1 calc R
C45 C 0.8085(3) 0.6797(3) -0.0206(2) 0.0232(12) Uani 1 1 d .
H45A H 0.8501 0.7036 0.0005 0.028 Uiso 1 1 calc R
C46 C -0.0265(2) 0.3547(3) -0.6159(2) 0.0222(12) Uani 1 1 d .
H46A H -0.0436 0.3629 -0.6555 0.027 Uiso 1 1 calc R
C47 C 0.2359(2) 0.1210(3) -0.5255(2) 0.0163(10) Uani 1 1 d .
C48 C -0.0332(3) 0.3754(4) -0.5304(2) 0.0253(12) Uani 1 1 d .
H48A H -0.0557 0.3973 -0.5101 0.030 Uiso 1 1 calc R
C49 C 0.2054(2) 0.1721(3) -0.4949(2) 0.0162(10) Uani 1 1 d .
C50 C 0.2039(2) 0.1101(3) -0.5848(2) 0.0184(11) Uani 1 1 d .
H50A H 0.1618 0.1329 -0.6061 0.022 Uiso 1 1 calc R
C51 C 0.8076(3) 0.5049(4) 0.2425(2) 0.0293(13) Uani 1 1 d .
H51A H 0.8519 0.5215 0.2632 0.035 Uiso 1 1 calc R
C52 C 0.5024(3) 0.4269(3) -0.0928(2) 0.0220(11) Uani 1 1 d .
H52A H 0.5205 0.4563 -0.1138 0.026 Uiso 1 1 calc R
C53 C 0.4438(3) 0.3830(3) -0.1204(2) 0.0230(12) Uani 1 1 d .
H53A H 0.4243 0.3815 -0.1605 0.028 Uiso 1 1 calc R
C54 C 0.2157(3) 0.2891(3) -0.3218(2) 0.0245(12) Uani 1 1 d .
H54A H 0.1775 0.3193 -0.3436 0.029 Uiso 1 1 calc R
C55 C 0.3023(3) 0.1975(3) -0.3151(2) 0.0248(12) Uani 1 1 d .
H55A H 0.3238 0.1650 -0.3319 0.030 Uiso 1 1 calc R
C56 C 0.3283(3) 0.2074(4) -0.2557(2) 0.0307(13) Uani 1 1 d .
H56A H 0.3678 0.1798 -0.2331 0.037 Uiso 1 1 calc R
C57 C 0.7123(2) 0.4924(3) 0.1520(2) 0.0204(11) Uani 1 1 d .
C58 C 0.7781(3) 0.5167(3) 0.1832(2) 0.0250(12) Uani 1 1 d .
H58A H 0.8021 0.5405 0.1648 0.030 Uiso 1 1 calc R
C59 C 0.7123(3) 0.4467(4) 0.2406(2) 0.0294(13) Uani 1 1 d .
H59A H 0.6896 0.4225 0.2600 0.035 Uiso 1 1 calc R
C60 C 0.2454(3) 0.2951(4) -0.2626(2) 0.0299(13) Uani 1 1 d .
H60A H 0.2261 0.3297 -0.2451 0.036 Uiso 1 1 calc R
N1 N -0.0607(2) 0.3847(3) -0.58778(18) 0.0202(9) Uani 1 1 d .
N2 N 0.2955(2) 0.0305(2) -0.58323(18) 0.0181(9) Uani 1 1 d .
N3 N 0.3008(2) 0.2536(3) -0.22886(19) 0.0275(11) Uani 1 1 d .
N4 N 0.1531(2) 0.2682(3) -0.44072(17) 0.0180(9) Uani 1 1 d .
N5 N 0.1480(2) 0.2101(3) -0.52740(18) 0.0172(9) Uani 1 1 d .
N6 N 0.2383(2) 0.1778(3) -0.43694(18) 0.0180(9) Uani 1 1 d .
N7 N 0.4134(2) 0.3423(3) -0.09275(18) 0.0204(9) Uani 1 1 d .
N8 N 0.7802(2) 0.6870(2) -0.07837(18) 0.0194(9) Uani 1 1 d .
N9 N 0.7761(2) 0.4711(3) 0.27159(19) 0.0282(11) Uani 1 1 d .
N10 N 0.6228(2) 0.4627(3) 0.05881(18) 0.0190(9) Uani 1 1 d .
N11 N 0.62633(19) 0.5113(2) -0.02696(17) 0.0159(9) Uani 1 1 d .
N12 N 0.7115(2) 0.5497(3) 0.06481(18) 0.0202(9) Uani 1 1 d .
O1 O 0.0619(3) 0.3969(4) -0.7054(3) 0.096(3) Uani 1 1 d .
O2 O -0.0347(2) 0.5133(2) -0.70680(17) 0.0321(9) Uani 1 1 d .
O3 O -0.07359(19) 0.5828(3) -0.63085(17) 0.0342(10) Uani 1 1 d .
O4 O 0.0520(2) 0.5243(3) -0.58730(18) 0.0383(10) Uani 1 1 d .
O5 O 0.03301(19) 0.6898(2) -0.60673(17) 0.0303(9) Uani 1 1 d .
O6 O -0.0517(2) 0.6853(2) -0.71407(17) 0.0376(10) Uani 1 1 d .
O7 O -0.0753(2) 0.6039(3) -0.82271(18) 0.0369(10) Uani 1 1 d .
O8 O -0.17593(18) 0.6990(2) -0.81620(19) 0.0361(10) Uani 1 1 d .
O9 O -0.0792(2) 0.7871(3) -0.62944(19) 0.0372(10) Uani 1 1 d .
O10 O 0.0407(2) 0.8568(3) -0.59368(18) 0.0385(10) Uani 1 1 d .
O11 O -0.0495(2) 0.8587(2) -0.71240(17) 0.0333(10) Uani 1 1 d .
O12 O -0.06363(19) 0.7829(2) -0.81514(17) 0.0309(9) Uani 1 1 d .
O13 O 0.0569(2) 0.9672(3) -0.70007(19) 0.0457(11) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 Ag1 N9 129.53(16) . 1_454
N1 Ag1 N2 123.34(15) . 3_455
N9 Ag1 N2 107.10(16) 1_454 3_455
N8 Ag2 N3 135.54(16) 3_445 .
N8 Ag2 N7 122.09(15) 3_445 .
N3 Ag2 N7 102.36(16) . .
O1 Mo1 O1 105.0(6) 2_553 .
O1 Mo1 O2 107.9(2) 2_553 2_553
O1 Mo1 O2 105.8(2) . 2_553
O1 Mo1 O2 105.8(2) 2_553 .
O1 Mo1 O2 107.9(2) . .
O2 Mo1 O2 123.2(3) 2_553 .
O3 Mo2 O4 103.6(2) . .
O3 Mo2 O5 102.15(18) . .
O4 Mo2 O5 100.37(19) . .
O3 Mo2 O2 93.44(18) . .
O4 Mo2 O2 100.26(19) . .
O5 Mo2 O2 150.32(16) . .
O3 Mo2 O7 163.93(17) . 2_553
O4 Mo2 O7 90.75(17) . 2_553
O5 Mo2 O7 81.97(16) . 2_553
O2 Mo2 O7 76.66(16) . 2_553
O3 Mo2 O6 89.87(18) . .
O4 Mo2 O6 166.36(18) . .
O5 Mo2 O6 74.21(16) . .
O2 Mo2 O6 80.80(15) . .
O7 Mo2 O6 76.19(15) 2_553 .
O10 Mo3 O9 103.5(2) . .
O10 Mo3 O11 103.2(2) . .
O9 Mo3 O11 97.45(18) . .
O10 Mo3 O5 98.0(2) . .
O9 Mo3 O5 99.03(18) . .
O11 Mo3 O5 149.18(16) . .
O10 Mo3 O12 90.64(17) . 2_553
O9 Mo3 O12 165.29(18) . 2_553
O11 Mo3 O12 75.17(15) . 2_553
O5 Mo3 O12 82.56(15) . 2_553
O10 Mo3 O6 162.54(18) . .
O9 Mo3 O6 92.48(18) . .
O11 Mo3 O6 81.21(15) . .
O5 Mo3 O6 72.24(15) . .
O12 Mo3 O6 73.98(15) 2_553 .
O13 Mo4 O13 106.6(3) . 2_553
O13 Mo4 O11 102.8(2) . 2_553
O13 Mo4 O11 105.0(2) 2_553 2_553
O13 Mo4 O11 105.0(2) . .
O13 Mo4 O11 102.8(2) 2_553 .
O11 Mo4 O11 132.6(2) 2_553 .
O8 Mo5 O7 105.9(2) . .
O8 Mo5 O6 111.5(2) . .
O7 Mo5 O6 110.1(2) . .
O8 Mo5 O12 107.84(18) . .
O7 Mo5 O12 110.26(18) . .
O6 Mo5 O12 111.17(19) . .
N4 C16 N5 125.0(4) . .
N4 C16 C32 116.3(4) . .
N5 C16 C32 118.7(4) . .
C45 C22 C42 118.7(5) . .
N2 C24 C50 123.1(5) . .
N11 C25 N10 125.1(4) . .
N11 C25 C38 118.9(4) . .
N10 C25 C38 116.0(4) . .
C47 C26 C43 118.2(5) . .
C32 C28 C46 118.8(5) . .
N7 C29 C30 123.5(4) . .
C29 C30 C38 118.5(4) . .
C28 C32 C41 118.4(5) . .
C28 C32 C16 122.1(4) . .
C41 C32 C16 119.5(4) . .
N4 C34 N6 124.8(4) . .
N4 C34 C40 116.9(4) . .
N6 C34 C40 118.3(4) . .
C59 C35 C57 118.9(5) . .
N8 C36 C44 123.3(5) . .
N11 C37 N12 124.7(4) . .
N11 C37 C42 117.4(4) . .
N12 C37 C42 117.9(4) . .
C30 C38 C52 118.8(4) . .
C30 C38 C25 118.8(4) . .
C52 C38 C25 122.4(4) . .
N12 C39 N10 125.0(4) . .
N12 C39 C57 117.7(4) . .
N10 C39 C57 117.4(4) . .
C55 C40 C54 119.0(5) . .
C55 C40 C34 121.5(5) . .
C54 C40 C34 119.5(5) . .
C48 C41 C32 118.9(5) . .
C44 C42 C22 118.9(4) . .
C44 C42 C37 120.2(4) . .
C22 C42 C37 120.9(4) . .
N2 C43 C26 123.7(5) . .
C42 C44 C36 118.8(4) . .
N8 C45 C22 122.8(5) . .
N1 C46 C28 123.3(5) . .
C50 C47 C26 118.4(4) . .
C50 C47 C49 121.0(4) . .
C26 C47 C49 120.5(4) . .
N1 C48 C41 123.6(5) . .
N5 C49 N6 125.2(4) . .
N5 C49 C47 117.1(4) . .
N6 C49 C47 117.8(4) . .
C24 C50 C47 119.2(5) . .
N9 C51 C58 123.8(5) . .
C53 C52 C38 118.2(5) . .
N7 C53 C52 123.9(5) . .
C60 C54 C40 118.9(5) . .
C40 C55 C56 117.6(5) . .
N3 C56 C55 124.5(5) . .
C58 C57 C35 118.6(5) . .
C58 C57 C39 119.5(4) . .
C35 C57 C39 121.9(5) . .
C57 C58 C51 118.6(5) . .
N9 C59 C35 123.0(5) . .
N3 C60 C54 123.3(5) . .
C46 N1 C48 117.0(4) . .
C46 N1 Ag1 122.7(3) . .
C48 N1 Ag1 120.0(3) . .
C43 N2 C24 117.3(4) . .
C43 N2 Ag1 122.1(3) . 3_545
C24 N2 Ag1 120.6(3) . 3_545
C56 N3 C60 116.5(5) . .
C56 N3 Ag2 127.8(4) . .
C60 N3 Ag2 114.5(3) . .
C16 N4 C34 115.6(4) . .
C49 N5 C16 114.4(4) . .
C34 N6 C49 114.9(4) . .
C29 N7 C53 116.9(4) . .
C29 N7 Ag2 114.8(3) . .
C53 N7 Ag2 127.4(3) . .
C45 N8 C36 117.6(4) . .
C45 N8 Ag2 127.1(3) . 3
C36 N8 Ag2 115.3(3) . 3
C51 N9 C59 117.1(5) . .
C51 N9 Ag1 112.6(4) . 1_656
C59 N9 Ag1 130.1(4) . 1_656
C39 N10 C25 115.0(4) . .
C25 N11 C37 115.1(4) . .
C39 N12 C37 114.8(4) . .
Mo1 O2 Mo2 136.7(2) . .
Mo2 O5 Mo3 121.2(2) . .
Mo5 O6 Mo2 141.3(2) . .
Mo5 O6 Mo3 128.9(2) . .
Mo2 O6 Mo3 88.99(13) . .
Mo5 O7 Mo2 127.7(2) . 2_553
Mo4 O11 Mo3 124.1(2) . .
Mo5 O12 Mo3 128.6(2) . 2_553
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N1 2.254(4) .
Ag1 N9 2.284(4) 1_454
Ag1 N2 2.300(4) 3_455
Ag2 N8 2.255(4) 3_445
Ag2 N3 2.296(4) .
Ag2 N7 2.336(4) .
Mo1 O1 1.709(6) 2_553
Mo1 O1 1.709(6) .
Mo1 O2 1.811(4) 2_553
Mo1 O2 1.811(4) .
Mo2 O3 1.704(4) .
Mo2 O4 1.710(4) .
Mo2 O5 1.868(4) .
Mo2 O2 1.981(4) .
Mo2 O7 2.292(4) 2_553
Mo2 O6 2.362(4) .
Mo3 O10 1.677(4) .
Mo3 O9 1.705(4) .
Mo3 O11 1.935(4) .
Mo3 O5 1.952(4) .
Mo3 O12 2.299(4) 2_553
Mo3 O6 2.387(4) .
Mo4 O13 1.691(5) .
Mo4 O13 1.691(5) 2_553
Mo4 O11 1.897(4) 2_553
Mo4 O11 1.897(4) .
Mo5 O8 1.694(4) .
Mo5 O7 1.781(4) .
Mo5 O6 1.786(4) .
Mo5 O12 1.797(4) .
C16 N4 1.331(6) .
C16 N5 1.345(6) .
C16 C32 1.486(7) .
C22 C45 1.394(7) .
C22 C42 1.399(7) .
C24 N2 1.341(6) .
C24 C50 1.378(7) .
C25 N11 1.323(6) .
C25 N10 1.346(6) .
C25 C38 1.494(7) .
C26 C47 1.392(7) .
C26 C43 1.384(7) .
C28 C32 1.378(7) .
C28 C46 1.382(7) .
C29 N7 1.335(7) .
C29 C30 1.385(7) .
C30 C38 1.385(7) .
C32 C41 1.389(7) .
C34 N4 1.332(6) .
C34 N6 1.332(6) .
C34 C40 1.493(7) .
C35 C59 1.386(8) .
C35 C57 1.391(7) .
C36 N8 1.348(6) .
C36 C44 1.391(7) .
C37 N11 1.344(6) .
C37 N12 1.345(6) .
C37 C42 1.484(7) .
C38 C52 1.388(7) .
C39 N12 1.337(6) .
C39 N10 1.335(6) .
C39 C57 1.483(7) .
C40 C55 1.372(7) .
C40 C54 1.383(7) .
C41 C48 1.368(7) .
C42 C44 1.376(7) .
C43 N2 1.338(6) .
C45 N8 1.344(7) .
C46 N1 1.338(6) .
C47 C50 1.385(7) .
C47 C49 1.489(7) .
C48 N1 1.337(7) .
C49 N5 1.333(6) .
C49 N6 1.349(6) .
C51 N9 1.338(7) .
C51 C58 1.385(8) .
C52 C53 1.379(7) .
C53 N7 1.342(7) .
C54 C60 1.374(8) .
C55 C56 1.388(8) .
C56 N3 1.330(7) .
C57 C58 1.383(7) .
C59 N9 1.347(7) .
C60 N3 1.340(7) .
N2 Ag1 2.300(4) 3_545
N8 Ag2 2.255(4) 3
N9 Ag1 2.284(4) 1_656
O7 Mo2 2.292(4) 2_553
O12 Mo3 2.299(4) 2_553
