#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:07:58 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180004 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/98/7029812.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029812
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.203(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   21.9943(8)
_cell_length_b                   16.5773(6)
_cell_length_c                   25.5580(15)
_cell_measurement_reflns_used    11495
_cell_measurement_temperature    370.01(10)
_cell_measurement_theta_max      28.8640
_cell_measurement_theta_min      3.2020
_cell_volume                     8431.5(7)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      370.01(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.958
_diffrn_measured_fraction_theta_max 0.958
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0314
_diffrn_reflns_av_sigmaI/netI    0.0386
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            18204
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.07
_exptl_absorpt_coefficient_mu    2.145
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.48220
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.256
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.33
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.957
_refine_diff_density_min         -0.865
_refine_diff_density_rms         0.149
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.069
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7121
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.069
_refine_ls_R_factor_all          0.0590
_refine_ls_R_factor_gt           0.0461
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0727P)²+60.6942P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1293
_refine_ls_wR_factor_ref         0.1414
_reflns_number_gt                5704
_reflns_number_total             7121
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           B_370K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029812.cif.
;
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029812
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag -0.15573(3) 0.45714(4) -0.63270(3) 0.0489(2) Uani 1 1 d .
Ag2 Ag -0.17772(3) 0.75492(5) -0.13323(3) 0.0551(2) Uani 1 1 d .
C10 C 0.0978(3) 0.9708(4) -0.0004(3) 0.0278(14) Uani 1 1 d .
C17 C -0.2025(3) 0.5841(4) -0.4958(3) 0.0331(15) Uani 1 1 d .
H17A H -0.1803 0.5882 -0.4558 0.040 Uiso 1 1 calc R
C18 C 0.0034(3) 0.8846(4) -0.0048(3) 0.0341(16) Uani 1 1 d .
H18A H 0.0229 0.8834 0.0354 0.041 Uiso 1 1 calc R
C19 C 0.2773(4) 1.1378(5) 0.0086(3) 0.0395(17) Uani 1 1 d .
H19A H 0.2983 1.1338 0.0487 0.047 Uiso 1 1 calc R
C21 C 0.1817(3) 1.0522(4) 0.0057(3) 0.0302(15) Uani 1 1 d .
C22 C -0.2902(3) 0.7264(4) -0.4136(3) 0.0296(15) Uani 1 1 d .
C23 C -0.4402(3) 0.8014(4) -0.5317(3) 0.0301(15) Uani 1 1 d .
C24 C -0.4670(4) 0.8112(5) -0.5898(3) 0.0414(18) Uani 1 1 d .
H24A H -0.4454 0.7901 -0.6110 0.050 Uiso 1 1 calc R
C25 C -0.3767(3) 0.7563(4) -0.4991(3) 0.0280(14) Uani 1 1 d .
C26 C -0.0560(4) 0.8441(4) -0.0365(3) 0.0352(16) Uani 1 1 d .
H26A H -0.0758 0.8155 -0.0165 0.042 Uiso 1 1 calc R
C29 C 0.0331(3) 0.9272(4) -0.0346(3) 0.0293(14) Uani 1 1 d .
C30 C 0.2199(3) 1.1532(5) -0.1089(3) 0.0358(16) Uani 1 1 d .
H30A H 0.2002 1.1581 -0.1489 0.043 Uiso 1 1 calc R
C32 C 0.1791(4) 0.9563(5) 0.1800(3) 0.049(2) Uani 1 1 d .
H32A H 0.1350 0.9388 0.1599 0.058 Uiso 1 1 calc R
C33 C -0.2646(4) 0.5644(4) -0.6123(3) 0.0381(17) Uani 1 1 d .
H33A H -0.2862 0.5575 -0.6522 0.046 Uiso 1 1 calc R
C34 C -0.2568(3) 0.7369(4) -0.3495(3) 0.0324(15) Uani 1 1 d .
C35 C 0.1801(3) 1.0020(4) 0.0866(3) 0.0319(15) Uani 1 1 d .
C37 C 0.2149(3) 1.1013(4) -0.0232(3) 0.0289(15) Uani 1 1 d .
C39 C -0.2643(3) 0.6210(4) -0.5263(3) 0.0315(15) Uani 1 1 d .
C40 C -0.4744(4) 0.8356(5) -0.5020(3) 0.0405(18) Uani 1 1 d .
H40A H -0.4569 0.8319 -0.4619 0.049 Uiso 1 1 calc R
C42 C 0.2122(3) 0.9920(5) 0.1511(3) 0.0359(16) Uani 1 1 d .
C43 C 0.1859(3) 1.1107(4) -0.0827(3) 0.0324(15) Uani 1 1 d .
H43A H 0.1439 1.0886 -0.1050 0.039 Uiso 1 1 calc R
C44 C -0.2960(4) 0.6093(4) -0.5858(3) 0.0359(16) Uani 1 1 d .
H44A H -0.3381 0.6316 -0.6075 0.043 Uiso 1 1 calc R
C45 C 0.3073(4) 1.1805(5) -0.0215(3) 0.0423(18) Uani 1 1 d .
H45A H 0.3485 1.2054 -0.0004 0.051 Uiso 1 1 calc R
C46 C -0.2950(3) 0.6721(4) -0.4962(3) 0.0295(15) Uani 1 1 d .
C47 C -0.5268(4) 0.8529(5) -0.6173(3) 0.0408(18) Uani 1 1 d .
H47A H -0.5441 0.8604 -0.6571 0.049 Uiso 1 1 calc R
C48 C -0.1749(4) 0.5411(4) -0.5266(3) 0.0358(16) Uani 1 1 d .
H48A H -0.1328 0.5181 -0.5061 0.043 Uiso 1 1 calc R
C49 C -0.5332(4) 0.8742(5) -0.5322(3) 0.045(2) Uani 1 1 d .
H49A H -0.5556 0.8960 -0.5118 0.054 Uiso 1 1 calc R
C51 C 0.0020(4) 0.9276(5) -0.0941(3) 0.0401(17) Uani 1 1 d .
H51A H 0.0198 0.9570 -0.1153 0.048 Uiso 1 1 calc R
C52 C 0.3067(4) 1.0053(6) 0.2414(4) 0.053(2) Uani 1 1 d .
H52A H 0.3508 1.0225 0.2622 0.064 Uiso 1 1 calc R
C54 C -0.0560(4) 0.8837(5) -0.1214(3) 0.0433(18) Uani 1 1 d .
H54A H -0.0753 0.8819 -0.1616 0.052 Uiso 1 1 calc R
C55 C 0.2117(4) 0.9466(6) 0.2392(3) 0.055(2) Uani 1 1 d .
H55A H 0.1888 0.9219 0.2583 0.066 Uiso 1 1 calc R
C56 C -0.2851(4) 0.7882(5) -0.3229(3) 0.046(2) Uani 1 1 d .
H56A H -0.3237 0.8175 -0.3447 0.055 Uiso 1 1 calc R
C57 C -0.2546(4) 0.7946(5) -0.2636(3) 0.050(2) Uani 1 1 d .
H57A H -0.2737 0.8288 -0.2459 0.060 Uiso 1 1 calc R
C58 C 0.2776(4) 1.0163(5) 0.1818(3) 0.0443(19) Uani 1 1 d .
H58A H 0.3016 1.0395 0.1633 0.053 Uiso 1 1 calc R
C59 C -0.1717(4) 0.7089(6) -0.2567(4) 0.058(2) Uani 1 1 d .
H59A H -0.1322 0.6817 -0.2341 0.069 Uiso 1 1 calc R
C60 C -0.1978(4) 0.6994(5) -0.3159(4) 0.048(2) Uani 1 1 d .
H60A H -0.1757 0.6681 -0.3326 0.058 Uiso 1 1 calc R
N1 N -0.2044(3) 0.5304(3) -0.5833(3) 0.0350(14) Uani 1 1 d .
N2 N -0.5606(3) 0.8827(4) -0.5890(3) 0.0395(14) Uani 1 1 d .
N3 N -0.1992(3) 0.7543(5) -0.2303(3) 0.0502(18) Uani 1 1 d .
N4 N -0.2622(3) 0.6773(4) -0.4382(3) 0.0347(14) Uani 1 1 d .
N5 N -0.3522(3) 0.7100(4) -0.5288(2) 0.0331(13) Uani 1 1 d .
N6 N -0.3475(3) 0.7666(4) -0.4420(2) 0.0352(14) Uani 1 1 d .
N7 N -0.0865(3) 0.8436(4) -0.0941(3) 0.0374(14) Uani 1 1 d .
N8 N 0.2753(3) 0.9715(4) 0.2703(3) 0.0479(17) Uani 1 1 d .
N9 N 0.2797(3) 1.1871(4) -0.0787(3) 0.0361(14) Uani 1 1 d .
N10 N 0.1257(3) 1.0127(3) -0.0282(2) 0.0310(13) Uani 1 1 d .
N11 N 0.1229(3) 0.9632(4) 0.0577(2) 0.0343(13) Uani 1 1 d .
N12 N 0.2111(3) 1.0498(4) 0.0636(3) 0.0372(14) Uani 1 1 d .
Mo1 Mo 0.0000 0.46468(7) -0.7500 0.0535(3) Uani 1 2 d S
Mo2 Mo -0.00128(3) 0.58975(4) -0.63920(2) 0.03219(17) Uani 1 1 d .
Mo3 Mo -0.00875(3) 0.79075(4) -0.64289(3) 0.03417(18) Uani 1 1 d .
Mo4 Mo 0.0000 0.90713(7) -0.7500 0.0506(3) Uani 1 2 d S
Mo5 Mo -0.09193(3) 0.69287(4) -0.79041(3) 0.03198(17) Uani 1 1 d .
O1 O 0.0626(6) 0.4018(7) -0.7073(6) 0.163(6) Uani 1 1 d .
O2 O -0.0340(3) 0.5143(4) -0.7059(3) 0.0604(16) Uani 1 1 d .
O3 O 0.0527(3) 0.5278(5) -0.5860(3) 0.076(2) Uani 1 1 d .
O4 O -0.0729(3) 0.5819(4) -0.6305(3) 0.0664(18) Uani 1 1 d .
O5 O 0.0329(3) 0.6897(4) -0.6064(3) 0.0573(16) Uani 1 1 d .
O6 O -0.0513(4) 0.6865(4) -0.7143(3) 0.0645(17) Uani 1 1 d .
O7 O -0.0757(3) 0.6045(4) -0.8230(3) 0.0674(18) Uani 1 1 d .
O8 O -0.1761(3) 0.6971(4) -0.8168(3) 0.0650(18) Uani 1 1 d .
O9 O -0.0779(3) 0.7871(5) -0.6297(3) 0.0729(19) Uani 1 1 d .
O10 O 0.0430(4) 0.8522(5) -0.5920(3) 0.080(2) Uani 1 1 d .
O11 O -0.0476(3) 0.8583(4) -0.7116(3) 0.0657(17) Uani 1 1 d .
O12 O -0.0655(3) 0.7809(4) -0.8165(3) 0.0599(16) Uani 1 1 d .
O13 O 0.0579(4) 0.9664(5) -0.7016(3) 0.093(2) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Ag1 N8 129.2(2) 3_545 3_444
N2 Ag1 N1 124.0(2) 3_545 .
N8 Ag1 N1 106.7(2) 3_444 .
N9 Ag2 N3 134.6(2) 3_445 .
N9 Ag2 N7 123.3(2) 3_445 .
N3 Ag2 N7 102.0(2) . .
N10 C10 N11 125.1(6) . .
N10 C10 C29 119.0(6) . .
N11 C10 C29 115.8(6) . .
C48 C17 C39 118.1(7) . .
C26 C18 C29 118.3(6) . .
C45 C19 C37 118.3(7) . .
N12 C21 N10 125.4(6) . .
N12 C21 C37 117.2(6) . .
N10 C21 C37 117.4(6) . .
N4 C22 N6 124.6(6) . .
N4 C22 C34 118.7(6) . .
N6 C22 C34 116.7(6) . .
C24 C23 C40 117.6(6) . .
C24 C23 C25 122.8(6) . .
C40 C23 C25 119.7(6) . .
C23 C24 C47 119.6(7) . .
N6 C25 N5 124.7(6) . .
N6 C25 C23 116.7(6) . .
N5 C25 C23 118.6(6) . .
N7 C26 C18 123.8(6) . .
C51 C29 C18 118.6(6) . .
C51 C29 C10 122.8(6) . .
C18 C29 C10 118.5(6) . .
N9 C30 C43 122.3(7) . .
C55 C32 C42 119.7(7) . .
N1 C33 C44 122.9(7) . .
C60 C34 C56 118.4(7) . .
C60 C34 C22 122.0(6) . .
C56 C34 C22 119.6(6) . .
N11 C35 N12 125.7(6) . .
N11 C35 C42 116.9(6) . .
N12 C35 C42 117.4(6) . .
C43 C37 C19 117.9(6) . .
C43 C37 C21 121.0(6) . .
C19 C37 C21 121.1(6) . .
C17 C39 C44 117.9(6) . .
C17 C39 C46 120.8(6) . .
C44 C39 C46 121.3(6) . .
C49 C40 C23 119.2(7) . .
C58 C42 C32 119.0(7) . .
C58 C42 C35 119.0(6) . .
C32 C42 C35 121.9(6) . .
C37 C43 C30 119.7(6) . .
C33 C44 C39 119.5(7) . .
N9 C45 C19 123.1(7) . .
N5 C46 N4 125.3(6) . .
N5 C46 C39 117.4(6) . .
N4 C46 C39 117.3(6) . .
N2 C47 C24 122.6(7) . .
N1 C48 C17 124.4(7) . .
N2 C49 C40 123.7(7) . .
C54 C51 C29 118.5(7) . .
N8 C52 C58 123.9(7) . .
N7 C54 C51 124.3(7) . .
N8 C55 C32 122.3(7) . .
C57 C56 C34 118.4(7) . .
N3 C57 C56 123.5(7) . .
C42 C58 C52 118.1(7) . .
N3 C59 C60 124.0(8) . .
C34 C60 C59 118.6(7) . .
C48 N1 C33 117.2(6) . .
C48 N1 Ag1 122.9(5) . .
C33 N1 Ag1 119.9(5) . .
C49 N2 C47 117.2(6) . .
C49 N2 Ag1 119.5(5) . 3_455
C47 N2 Ag1 123.0(5) . 3_455
C59 N3 C57 116.9(7) . .
C59 N3 Ag2 128.5(6) . .
C57 N3 Ag2 113.5(5) . .
C22 N4 C46 114.9(6) . .
C46 N5 C25 114.5(6) . .
C25 N6 C22 116.0(6) . .
C26 N7 C54 116.5(6) . .
C26 N7 Ag2 114.4(4) . .
C54 N7 Ag2 128.3(5) . .
C52 N8 C55 117.1(7) . .
C52 N8 Ag1 112.4(5) . 3_556
C55 N8 Ag1 130.3(5) . 3_556
C45 N9 C30 118.6(6) . .
C45 N9 Ag2 126.9(5) . 3
C30 N9 Ag2 114.5(5) . 3
C10 N10 C21 115.0(6) . .
C35 N11 C10 114.5(6) . .
C35 N12 C21 114.1(6) . .
O1 Mo1 O1 104.4(10) 2_553 .
O1 Mo1 O2 104.2(4) 2_553 .
O1 Mo1 O2 108.5(5) . .
O1 Mo1 O2 108.5(5) 2_553 2_553
O1 Mo1 O2 104.2(4) . 2_553
O2 Mo1 O2 125.4(4) . 2_553
O4 Mo2 O3 102.6(3) . .
O4 Mo2 O5 103.3(3) . .
O3 Mo2 O5 99.5(3) . .
O4 Mo2 O2 92.7(3) . .
O3 Mo2 O2 100.4(3) . .
O5 Mo2 O2 151.0(3) . .
O4 Mo2 O7 164.3(3) . 2_553
O3 Mo2 O7 90.7(3) . 2_553
O5 Mo2 O7 82.3(3) . 2_553
O2 Mo2 O7 76.6(3) . 2_553
O4 Mo2 O6 91.2(3) . .
O3 Mo2 O6 165.8(3) . .
O5 Mo2 O6 73.9(2) . .
O2 Mo2 O6 81.8(2) . .
O7 Mo2 O6 76.1(2) 2_553 .
O10 Mo3 O9 103.8(3) . .
O10 Mo3 O5 97.3(4) . .
O9 Mo3 O5 98.9(3) . .
O10 Mo3 O11 104.2(4) . .
O9 Mo3 O11 96.5(3) . .
O5 Mo3 O11 149.7(3) . .
O10 Mo3 O12 90.9(3) . 2_553
O9 Mo3 O12 164.8(3) . 2_553
O5 Mo3 O12 82.8(2) . 2_553
O11 Mo3 O12 75.8(2) . 2_553
O10 Mo3 O6 162.5(3) . .
O9 Mo3 O6 91.9(3) . .
O5 Mo3 O6 72.3(2) . .
O11 Mo3 O6 81.3(2) . .
O12 Mo3 O6 74.1(2) 2_553 .
O13 Mo4 O13 107.8(6) . 2_553
O13 Mo4 O11 102.8(4) . 2_553
O13 Mo4 O11 106.4(4) 2_553 2_553
O13 Mo4 O11 106.4(4) . .
O13 Mo4 O11 102.8(4) 2_553 .
O11 Mo4 O11 129.4(4) 2_553 .
O8 Mo5 O6 113.5(3) . .
O8 Mo5 O7 104.5(3) . .
O6 Mo5 O7 110.8(3) . .
O8 Mo5 O12 106.9(3) . .
O6 Mo5 O12 111.4(3) . .
O7 Mo5 O12 109.3(3) . .
Mo1 O2 Mo2 137.1(4) . .
Mo2 O5 Mo3 122.2(3) . .
Mo5 O6 Mo2 140.5(3) . .
Mo5 O6 Mo3 130.3(3) . .
Mo2 O6 Mo3 88.6(2) . .
Mo5 O7 Mo2 127.7(3) . 2_553
Mo4 O11 Mo3 125.9(3) . .
Mo5 O12 Mo3 129.2(3) . 2_553
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N2 2.271(6) 3_545
Ag1 N8 2.302(6) 3_444
Ag1 N1 2.315(5) .
Ag2 N9 2.279(6) 3_445
Ag2 N3 2.318(6) .
Ag2 N7 2.340(6) .
C10 N10 1.315(8) .
C10 N11 1.352(9) .
C10 C29 1.501(9) .
C17 C48 1.378(9) .
C17 C39 1.389(9) .
C18 C26 1.383(10) .
C18 C29 1.389(9) .
C19 C45 1.399(10) .
C19 C37 1.401(10) .
C21 N12 1.339(9) .
C21 N10 1.337(9) .
C21 C37 1.484(9) .
C22 N4 1.330(9) .
C22 N6 1.334(9) .
C22 C34 1.492(9) .
C23 C24 1.354(10) .
C23 C40 1.396(9) .
C23 C25 1.487(9) .
C24 C47 1.383(10) .
C25 N6 1.331(9) .
C25 N5 1.343(8) .
C26 N7 1.332(9) .
C29 C51 1.376(10) .
C30 N9 1.334(9) .
C30 C43 1.390(9) .
C32 C55 1.380(11) .
C32 C42 1.374(10) .
C33 N1 1.337(9) .
C33 C44 1.374(10) .
C34 C60 1.362(10) .
C34 C56 1.390(10) .
C35 N11 1.323(9) .
C35 N12 1.336(9) .
C35 C42 1.499(10) .
C37 C43 1.383(9) .
C39 C44 1.390(10) .
C39 C46 1.486(9) .
C40 C49 1.352(10) .
C42 C58 1.372(10) .
C45 N9 1.327(10) .
C46 N5 1.334(9) .
C46 N4 1.347(9) .
C47 N2 1.332(9) .
C48 N1 1.325(9) .
C49 N2 1.322(9) .
C51 C54 1.373(10) .
C52 N8 1.333(10) .
C52 C58 1.390(11) .
C54 N7 1.335(9) .
C55 N8 1.347(10) .
C56 C57 1.375(11) .
C57 N3 1.331(11) .
C59 N3 1.319(11) .
C59 C60 1.381(11) .
N2 Ag1 2.271(6) 3_455
N8 Ag1 2.302(6) 3_556
N9 Ag2 2.279(6) 3
Mo1 O1 1.701(10) 2_553
Mo1 O1 1.701(10) .
Mo1 O2 1.796(6) .
Mo1 O2 1.796(6) 2_553
Mo2 O4 1.686(6) .
Mo2 O3 1.714(6) .
Mo2 O5 1.864(6) .
Mo2 O2 1.985(6) .
Mo2 O7 2.292(6) 2_553
Mo2 O6 2.381(6) .
Mo3 O10 1.663(6) .
Mo3 O9 1.694(6) .
Mo3 O5 1.946(6) .
Mo3 O11 1.947(7) .
Mo3 O12 2.284(6) 2_553
Mo3 O6 2.395(6) .
Mo4 O13 1.666(8) .
Mo4 O13 1.666(8) 2_553
Mo4 O11 1.894(6) 2_553
Mo4 O11 1.894(6) .
Mo5 O8 1.681(6) .
Mo5 O6 1.764(6) .
Mo5 O7 1.795(7) .
Mo5 O12 1.801(6) .
O7 Mo2 2.292(6) 2_553
O12 Mo3 2.284(6) 2_553
