#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:07:58 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180004 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/98/7029819.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029819
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.250(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   22.0267(7)
_cell_length_b                   16.6061(5)
_cell_length_c                   25.5742(12)
_cell_measurement_reflns_used    14276
_cell_measurement_temperature    370.00(10)
_cell_measurement_theta_max      28.7960
_cell_measurement_theta_min      3.2040
_cell_volume                     8460.7(6)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      370.00(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.972
_diffrn_measured_fraction_theta_max 0.972
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0278
_diffrn_reflns_av_sigmaI/netI    0.0310
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            19607
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.06
_exptl_absorpt_coefficient_mu    2.138
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.64946
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.249
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.33
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.10
_refine_diff_density_max         2.030
_refine_diff_density_min         -1.006
_refine_diff_density_rms         0.143
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.051
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7258
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.051
_refine_ls_R_factor_all          0.0546
_refine_ls_R_factor_gt           0.0447
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0765P)²+61.4138P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1285
_refine_ls_wR_factor_ref         0.1384
_reflns_number_gt                6085
_reflns_number_total             7258
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           A_370K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029819.cif.
;
_cod_original_cell_volume        8460.7(5)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029819
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Mo1 Mo 0.5000 -0.03524(6) 0.2500 0.0545(3) Uani 1 2 d S
Mo2 Mo 0.50128(3) 0.08977(3) 0.13917(2) 0.03282(16) Uani 1 1 d .
Mo3 Mo 0.50873(3) 0.29074(4) 0.14285(2) 0.03472(16) Uani 1 1 d .
Mo4 Mo 0.5000 0.40706(7) 0.2500 0.0519(3) Uani 1 2 d S
Mo5 Mo 0.59199(3) 0.19286(3) 0.29039(2) 0.03285(16) Uani 1 1 d .
O1 O 0.4377(6) -0.0984(6) 0.2073(6) 0.160(5) Uani 1 1 d .
O2 O 0.5338(3) 0.0152(3) 0.2058(2) 0.0594(14) Uani 1 1 d .
O3 O 0.4475(3) 0.0278(4) 0.0861(3) 0.0758(18) Uani 1 1 d .
O4 O 0.5728(3) 0.0824(4) 0.1305(3) 0.0688(17) Uani 1 1 d .
O5 O 0.4671(3) 0.1898(3) 0.1064(2) 0.0553(14) Uani 1 1 d .
O6 O 0.5511(3) 0.1860(3) 0.2144(2) 0.0639(16) Uani 1 1 d .
O7 O 0.5764(3) 0.1044(4) 0.3236(3) 0.0672(16) Uani 1 1 d .
O8 O 0.6761(3) 0.1969(3) 0.3167(3) 0.0655(17) Uani 1 1 d .
O9 O 0.5658(3) 0.2811(4) 0.3165(3) 0.0609(15) Uani 1 1 d .
O10 O 0.5783(3) 0.2876(4) 0.1297(3) 0.0751(18) Uani 1 1 d .
O11 O 0.4570(3) 0.3521(4) 0.0919(3) 0.079(2) Uani 1 1 d .
O12 O 0.5472(3) 0.3578(4) 0.2116(3) 0.0661(16) Uani 1 1 d .
O13 O 0.4420(4) 0.4668(5) 0.2015(3) 0.095(2) Uani 1 1 d .
Ag1 Ag 0.34424(3) -0.04292(4) -0.63274(2) 0.04982(18) Uani 1 1 d .
Ag2 Ag 0.32227(3) 0.25501(4) -0.13325(2) 0.0560(2) Uani 1 1 d .
C15 C 0.0327(3) 0.3107(4) -0.5904(3) 0.0409(16) Uani 1 1 d .
H15A H 0.0540 0.2897 -0.6120 0.049 Uiso 1 1 calc R
C17 C 0.1237(3) 0.2559(4) -0.4990(3) 0.0289(13) Uani 1 1 d .
C18 C 0.5978(3) 0.4713(4) -0.0005(3) 0.0301(13) Uani 1 1 d .
C19 C 0.0598(3) 0.3009(4) -0.5312(3) 0.0300(13) Uani 1 1 d .
C20 C 0.2977(3) 0.0835(4) -0.4957(3) 0.0322(13) Uani 1 1 d .
H20A H 0.3199 0.0872 -0.4556 0.039 Uiso 1 1 calc R
C21 C 0.5039(3) 0.3847(4) -0.0046(3) 0.0364(14) Uani 1 1 d .
H21A H 0.5236 0.3833 0.0356 0.044 Uiso 1 1 calc R
C23 C 0.2095(3) 0.2261(4) -0.4136(3) 0.0306(13) Uani 1 1 d .
C24 C 0.7203(3) 0.6525(4) -0.1089(3) 0.0350(14) Uani 1 1 d .
H24A H 0.7006 0.6572 -0.1489 0.042 Uiso 1 1 calc R
C25 C 0.6820(3) 0.5522(4) 0.0056(3) 0.0302(13) Uani 1 1 d .
C26 C 0.7775(3) 0.6383(4) 0.0086(3) 0.0380(15) Uani 1 1 d .
H26A H 0.7984 0.6345 0.0487 0.046 Uiso 1 1 calc R
C27 C 0.5333(3) 0.4272(4) -0.0346(3) 0.0287(13) Uani 1 1 d .
C30 C 0.4441(3) 0.3444(4) -0.0366(3) 0.0387(15) Uani 1 1 d .
H30A H 0.4242 0.3164 -0.0165 0.046 Uiso 1 1 calc R
C31 C 0.2428(3) 0.2367(4) -0.3496(3) 0.0344(14) Uani 1 1 d .
C33 C 0.0260(3) 0.3343(5) -0.5014(3) 0.0401(16) Uani 1 1 d .
H33A H 0.0431 0.3297 -0.4614 0.048 Uiso 1 1 calc R
C36 C 0.2353(3) 0.0643(4) -0.6123(3) 0.0372(15) Uani 1 1 d .
H36A H 0.2135 0.0572 -0.6522 0.045 Uiso 1 1 calc R
C37 C 0.7148(3) 0.6017(4) -0.0235(3) 0.0308(13) Uani 1 1 d .
C39 C 0.2354(3) 0.1216(4) -0.5265(3) 0.0308(13) Uani 1 1 d .
C40 C -0.0330(3) 0.3742(5) -0.5321(3) 0.0464(18) Uani 1 1 d .
H40A H -0.0550 0.3968 -0.5117 0.056 Uiso 1 1 calc R
C41 C 0.6788(4) 0.4561(5) 0.1795(3) 0.0492(19) Uani 1 1 d .
H41A H 0.6348 0.4388 0.1592 0.059 Uiso 1 1 calc R
C42 C 0.2041(3) 0.1095(4) -0.5857(3) 0.0371(15) Uani 1 1 d .
H42A H 0.1620 0.1319 -0.6075 0.045 Uiso 1 1 calc R
C43 C 0.6802(3) 0.5021(4) 0.0869(3) 0.0327(14) Uani 1 1 d .
C44 C 0.7124(3) 0.4914(4) 0.1511(3) 0.0366(15) Uani 1 1 d .
C45 C 0.6865(3) 0.6099(4) -0.0827(3) 0.0331(14) Uani 1 1 d .
H45A H 0.6449 0.5869 -0.1051 0.040 Uiso 1 1 calc R
C46 C -0.0269(3) 0.3526(5) -0.6169(3) 0.0426(16) Uani 1 1 d .
H46A H -0.0444 0.3600 -0.6567 0.051 Uiso 1 1 calc R
C47 C 0.8073(3) 0.6801(4) -0.0213(3) 0.0433(17) Uani 1 1 d .
H47A H 0.8486 0.7046 -0.0001 0.052 Uiso 1 1 calc R
C48 C 0.2053(3) 0.1721(4) -0.4962(3) 0.0298(13) Uani 1 1 d .
C49 C 0.3248(3) 0.0404(4) -0.5269(3) 0.0373(15) Uani 1 1 d .
H49A H 0.3668 0.0171 -0.5065 0.045 Uiso 1 1 calc R
C50 C 0.5016(3) 0.4279(4) -0.0943(3) 0.0401(15) Uani 1 1 d .
H50A H 0.5191 0.4576 -0.1154 0.048 Uiso 1 1 calc R
C53 C 0.8066(4) 0.5049(5) 0.2413(3) 0.053(2) Uani 1 1 d .
H53A H 0.8506 0.5219 0.2624 0.063 Uiso 1 1 calc R
C54 C 0.7118(4) 0.4464(6) 0.2392(3) 0.056(2) Uani 1 1 d .
H54A H 0.6890 0.4222 0.2584 0.067 Uiso 1 1 calc R
C55 C 0.2449(4) 0.2951(5) -0.2641(3) 0.055(2) Uani 1 1 d .
H55A H 0.2260 0.3299 -0.2466 0.066 Uiso 1 1 calc R
C56 C 0.4438(3) 0.3840(5) -0.1218(3) 0.0451(17) Uani 1 1 d .
H56A H 0.4245 0.3824 -0.1620 0.054 Uiso 1 1 calc R
C57 C 0.2144(4) 0.2876(5) -0.3232(3) 0.0476(18) Uani 1 1 d .
H57A H 0.1754 0.3162 -0.3451 0.057 Uiso 1 1 calc R
C58 C 0.3280(4) 0.2086(6) -0.2570(3) 0.058(2) Uani 1 1 d .
H58A H 0.3672 0.1809 -0.2344 0.069 Uiso 1 1 calc R
C59 C 0.7780(4) 0.5166(5) 0.1822(3) 0.0473(18) Uani 1 1 d .
H59A H 0.8019 0.5406 0.1640 0.057 Uiso 1 1 calc R
C60 C 0.3022(4) 0.1993(5) -0.3161(3) 0.0494(19) Uani 1 1 d .
H60A H 0.3245 0.1684 -0.3328 0.059 Uiso 1 1 calc R
N1 N 0.2957(3) 0.0300(3) -0.5833(2) 0.0355(12) Uani 1 1 d .
N2 N -0.0608(3) 0.3829(4) -0.5892(2) 0.0389(13) Uani 1 1 d .
N3 N 0.3008(3) 0.2544(4) -0.2303(3) 0.0513(16) Uani 1 1 d .
N4 N 0.1477(3) 0.2104(3) -0.5286(2) 0.0332(12) Uani 1 1 d .
N5 N 0.1526(3) 0.2668(3) -0.4419(2) 0.0341(12) Uani 1 1 d .
N6 N 0.2379(3) 0.1775(3) -0.4383(2) 0.0336(12) Uani 1 1 d .
N7 N 0.7799(3) 0.6871(3) -0.0789(2) 0.0369(13) Uani 1 1 d .
N8 N 0.4135(3) 0.3432(3) -0.0941(2) 0.0387(13) Uani 1 1 d .
N9 N 0.7753(3) 0.4708(4) 0.2700(3) 0.0498(15) Uani 1 1 d .
N10 N 0.6259(2) 0.5127(3) -0.0279(2) 0.0323(11) Uani 1 1 d .
N11 N 0.6229(3) 0.4630(3) 0.0575(2) 0.0352(12) Uani 1 1 d .
N12 N 0.7110(3) 0.5491(3) 0.0635(2) 0.0359(12) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Mo1 O1 103.9(10) 2_655 .
O1 Mo1 O2 108.6(4) 2_655 2_655
O1 Mo1 O2 104.7(4) . 2_655
O1 Mo1 O2 104.7(4) 2_655 .
O1 Mo1 O2 108.6(4) . .
O2 Mo1 O2 124.7(4) 2_655 .
O3 Mo2 O4 102.8(3) . .
O3 Mo2 O5 99.7(3) . .
O4 Mo2 O5 103.0(3) . .
O3 Mo2 O2 100.4(3) . .
O4 Mo2 O2 93.0(3) . .
O5 Mo2 O2 150.7(2) . .
O3 Mo2 O7 90.4(3) . 2_655
O4 Mo2 O7 164.6(3) . 2_655
O5 Mo2 O7 82.1(2) . 2_655
O2 Mo2 O7 76.7(2) . 2_655
O3 Mo2 O6 165.7(3) . .
O4 Mo2 O6 91.2(3) . .
O5 Mo2 O6 74.0(2) . .
O2 Mo2 O6 81.5(2) . .
O7 Mo2 O6 76.2(2) 2_655 .
O10 Mo3 O11 103.7(3) . .
O10 Mo3 O5 99.1(3) . .
O11 Mo3 O5 97.3(3) . .
O10 Mo3 O12 96.5(3) . .
O11 Mo3 O12 104.3(3) . .
O5 Mo3 O12 149.4(2) . .
O10 Mo3 O9 164.9(3) . 2_655
O11 Mo3 O9 90.8(3) . 2_655
O5 Mo3 O9 82.8(2) . 2_655
O12 Mo3 O9 75.6(2) . 2_655
O10 Mo3 O6 92.2(3) . .
O11 Mo3 O6 162.3(3) . .
O5 Mo3 O6 72.1(2) . .
O12 Mo3 O6 81.3(2) . .
O9 Mo3 O6 74.1(2) 2_655 .
O13 Mo4 O13 107.4(5) 2_655 .
O13 Mo4 O12 103.0(3) 2_655 .
O13 Mo4 O12 106.7(3) . .
O13 Mo4 O12 106.7(3) 2_655 2_655
O13 Mo4 O12 103.0(3) . 2_655
O12 Mo4 O12 128.8(4) . 2_655
O8 Mo5 O6 113.7(3) . .
O8 Mo5 O9 106.9(3) . .
O6 Mo5 O9 111.5(3) . .
O8 Mo5 O7 104.1(3) . .
O6 Mo5 O7 110.9(3) . .
O9 Mo5 O7 109.4(3) . .
Mo1 O2 Mo2 137.4(3) . .
Mo2 O5 Mo3 122.2(3) . .
Mo5 O6 Mo3 129.9(3) . .
Mo5 O6 Mo2 141.0(3) . .
Mo3 O6 Mo2 88.59(19) . .
Mo5 O7 Mo2 127.3(3) . 2_655
Mo5 O9 Mo3 128.9(3) . 2_655
Mo4 O12 Mo3 126.3(3) . .
N2 Ag1 N9 128.9(2) 3_545 3_444
N2 Ag1 N1 124.0(2) 3_545 .
N9 Ag1 N1 107.0(2) 3_444 .
N7 Ag2 N8 123.4(2) 3_445 .
N7 Ag2 N3 134.6(2) 3_445 .
N8 Ag2 N3 101.9(2) . .
C46 C15 C19 118.3(6) . .
N4 C17 N5 125.5(6) . .
N4 C17 C19 118.7(5) . .
N5 C17 C19 115.7(5) . .
N11 C18 N10 125.1(6) . .
N11 C18 C27 115.5(5) . .
N10 C18 C27 119.4(5) . .
C33 C19 C15 118.2(6) . .
C33 C19 C17 119.8(5) . .
C15 C19 C17 122.0(6) . .
C39 C20 C49 117.9(6) . .
C30 C21 C27 117.9(6) . .
N6 C23 N5 124.8(6) . .
N6 C23 C31 118.7(5) . .
N5 C23 C31 116.5(5) . .
N7 C24 C45 122.7(6) . .
N12 C25 N10 124.3(6) . .
N12 C25 C37 118.0(5) . .
N10 C25 C37 117.7(5) . .
C47 C26 C37 118.2(6) . .
C50 C27 C21 118.6(6) . .
C50 C27 C18 123.0(6) . .
C21 C27 C18 118.4(5) . .
N8 C30 C21 124.3(6) . .
C60 C31 C57 118.7(6) . .
C60 C31 C23 121.7(6) . .
C57 C31 C23 119.5(6) . .
C19 C33 C40 118.6(6) . .
C42 C36 N1 122.9(6) . .
C26 C37 C45 118.0(6) . .
C26 C37 C25 120.9(6) . .
C45 C37 C25 121.1(5) . .
C20 C39 C42 117.4(6) . .
C20 C39 C48 120.6(6) . .
C42 C39 C48 122.0(6) . .
N2 C40 C33 124.2(6) . .
C54 C41 C44 118.9(7) . .
C36 C42 C39 119.9(6) . .
N11 C43 N12 125.0(6) . .
N11 C43 C44 117.1(6) . .
N12 C43 C44 117.9(6) . .
C59 C44 C43 119.1(6) . .
C59 C44 C41 119.5(6) . .
C43 C44 C41 121.4(6) . .
C24 C45 C37 119.7(6) . .
C15 C46 N2 124.2(6) . .
C26 C47 N7 123.5(6) . .
N6 C48 N4 124.6(6) . .
N6 C48 C39 117.9(5) . .
N4 C48 C39 117.5(6) . .
N1 C49 C20 124.8(6) . .
C27 C50 C56 119.0(6) . .
N9 C53 C59 124.2(7) . .
C41 C54 N9 122.3(7) . .
C57 C55 N3 123.0(7) . .
N8 C56 C50 123.9(6) . .
C55 C57 C31 118.8(7) . .
N3 C58 C60 124.3(7) . .
C53 C59 C44 117.7(7) . .
C58 C60 C31 118.2(7) . .
C49 N1 C36 117.1(6) . .
C49 N1 Ag1 123.0(4) . .
C36 N1 Ag1 119.9(4) . .
C46 N2 C40 116.4(6) . .
C46 N2 Ag1 123.7(4) . 3_455
C40 N2 Ag1 119.6(4) . 3_455
C58 N3 C55 116.7(6) . .
C58 N3 Ag2 128.6(5) . .
C55 N3 Ag2 113.4(5) . .
C17 N4 C48 114.7(5) . .
C17 N5 C23 115.2(5) . .
C23 N6 C48 115.1(5) . .
C24 N7 C47 117.9(6) . .
C24 N7 Ag2 114.9(4) . 3
C47 N7 Ag2 127.2(4) . 3
C30 N8 C56 116.3(6) . .
C30 N8 Ag2 114.9(4) . .
C56 N8 Ag2 128.2(5) . .
C53 N9 C54 117.5(6) . .
C53 N9 Ag1 112.3(5) . 3_556
C54 N9 Ag1 130.1(5) . 3_556
C18 N10 C25 115.8(5) . .
C18 N11 C43 114.6(5) . .
C25 N12 C43 115.1(5) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Mo1 O1 1.702(9) 2_655
Mo1 O1 1.702(9) .
Mo1 O2 1.804(6) 2_655
Mo1 O2 1.804(6) .
Mo2 O3 1.713(6) .
Mo2 O4 1.687(6) .
Mo2 O5 1.869(5) .
Mo2 O2 1.977(6) .
Mo2 O7 2.299(6) 2_655
Mo2 O6 2.379(6) .
Mo3 O10 1.703(6) .
Mo3 O11 1.665(6) .
Mo3 O5 1.946(6) .
Mo3 O12 1.943(6) .
Mo3 O9 2.293(5) 2_655
Mo3 O6 2.405(6) .
Mo4 O13 1.673(8) 2_655
Mo4 O13 1.673(7) .
Mo4 O12 1.894(6) .
Mo4 O12 1.894(6) 2_655
Mo5 O8 1.681(5) .
Mo5 O6 1.764(6) .
Mo5 O9 1.804(6) .
Mo5 O7 1.801(6) .
O7 Mo2 2.299(6) 2_655
O9 Mo3 2.293(5) 2_655
Ag1 N2 2.269(5) 3_545
Ag1 N9 2.307(6) 3_444
Ag1 N1 2.317(5) .
Ag2 N7 2.278(5) 3_445
Ag2 N8 2.338(5) .
Ag2 N3 2.320(6) .
C15 C46 1.380(10) .
C15 C19 1.380(9) .
C17 N4 1.328(8) .
C17 N5 1.333(8) .
C17 C19 1.492(8) .
C18 N11 1.351(8) .
C18 N10 1.308(8) .
C18 C27 1.502(8) .
C19 C33 1.390(9) .
C20 C39 1.407(9) .
C20 C49 1.383(9) .
C21 C30 1.390(9) .
C21 C27 1.390(9) .
C23 N6 1.333(8) .
C23 N5 1.334(8) .
C23 C31 1.490(9) .
C24 N7 1.335(8) .
C24 C45 1.388(9) .
C25 N12 1.340(8) .
C25 N10 1.338(8) .
C25 C37 1.487(8) .
C26 C47 1.387(9) .
C26 C37 1.408(9) .
C27 C50 1.381(9) .
C30 N8 1.332(9) .
C31 C60 1.369(10) .
C31 C57 1.388(9) .
C33 C40 1.369(9) .
C36 C42 1.378(9) .
C36 N1 1.343(8) .
C37 C45 1.377(9) .
C39 C42 1.384(9) .
C39 C48 1.478(9) .
C40 N2 1.329(9) .
C41 C54 1.393(10) .
C41 C44 1.369(10) .
C43 N11 1.331(8) .
C43 N12 1.333(8) .
C43 C44 1.496(9) .
C44 C59 1.382(10) .
C46 N2 1.329(9) .
C47 N7 1.337(9) .
C48 N6 1.345(8) .
C48 N4 1.343(8) .
C49 N1 1.316(8) .
C50 C56 1.372(10) .
C53 N9 1.328(10) .
C53 C59 1.381(10) .
C54 N9 1.342(10) .
C55 C57 1.373(10) .
C55 N3 1.347(10) .
C56 N8 1.347(9) .
C58 N3 1.325(10) .
C58 C60 1.378(11) .
N2 Ag1 2.269(5) 3_455
N7 Ag2 2.278(5) 3
N9 Ag1 2.307(6) 3_556
