#------------------------------------------------------------------------------
#$Date: 2016-03-26 13:30:06 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180224 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/10/7111071.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_7111071
loop_
_publ_author_name
'Tao, Jun'
'Tong, Ming-Liang'
'Shi, Jian-Xin'
'Chen, Xiao-Ming'
'Ng, Seik Weng'
_publ_section_title
;
 Blue photoluminescent zinc coordination polymers with supertetranuclear
 cores
;
_journal_issue                   20
_journal_name_full               'Chemical Communications'
_journal_page_first              2043
_journal_paper_doi               10.1039/b005753n
_journal_year                    2000
_chemical_formula_sum            'C32 H24 N4 O14 Zn4'
_chemical_formula_weight         950.03
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yac'
_symmetry_space_group_name_H-M   'P 1 2/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 103.520(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.096(7)
_cell_length_b                   11.183(6)
_cell_length_c                   18.607(12)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      15
_cell_measurement_theta_min      7
_cell_volume                     3459(3)
_computing_cell_refinement       'SHELXTL-plus (Sheldrick, 1990)'
_computing_data_collection       'SHELXTL-plus (Sheldrick, 1990)'
_computing_data_reduction        'SHELXL-97  (Sheldrick, 1997)'
_computing_molecular_graphics    'SHELXL-97 (Sheldrick, 1997)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.861
_diffrn_measured_fraction_theta_max 0.861
_diffrn_measurement_device_type  'Siemens R3m'
_diffrn_measurement_method       ω-scans
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0287
_diffrn_reflns_av_sigmaI/netI    0.0328
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            7035
_diffrn_reflns_theta_full        26.93
_diffrn_reflns_theta_max         26.93
_diffrn_reflns_theta_min         2.14
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count 200
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    2.817
_exptl_absorpt_correction_T_max  0.5060
_exptl_absorpt_correction_T_min  0.3333
_exptl_absorpt_correction_type   \y-scan
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.824
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1904
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.48
_exptl_crystal_size_min          0.28
_refine_diff_density_max         0.444
_refine_diff_density_min         -0.629
_refine_diff_density_rms         0.103
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.026
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     487
_refine_ls_number_reflns         6801
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.026
_refine_ls_R_factor_all          0.0603
_refine_ls_R_factor_gt           0.0424
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0513P)²+8.0332P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0991
_refine_ls_wR_factor_ref         0.1104
_reflns_number_gt                5418
_reflns_number_total             6801
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b005753nsup1.cif
_cod_data_source_block           complex_2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0513P)^2^+8.0332P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.0513P)^2^+8.0332P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_sg_symbol_H-M      P2/n
_cod_database_code               7111071
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y, -z+1/2'
'-x, -y, -z'
'x-1/2, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
Zn1 Zn 0.58657(3) 0.06306(4) -0.00090(3) 0.02682(13) Uani 1 d .
Zn2 Zn 0.50043(3) 0.17578(4) 0.12963(3) 0.02893(13) Uani 1 d .
Zn3 Zn 0.92370(3) 0.41748(4) 0.02119(3) 0.02797(13) Uani 1 d .
Zn4 Zn 1.01780(3) 0.67075(4) 0.13106(3) 0.02971(13) Uani 1 d .
N1 N 0.1913(2) -0.0248(3) 0.4538(2) 0.0331(8) Uani 1 d .
N2 N 0.4392(2) 0.1291(3) 0.2082(2) 0.0307(8) Uani 1 d .
N3 N 0.8604(2) 0.3979(3) 0.1092(2) 0.0315(8) Uani 1 d .
N4 N 0.9172(2) 0.7089(3) 0.1682(2) 0.0353(9) Uani 1 d .
O1 O 0.5312(2) 0.1912(3) -0.10110(19) 0.0420(8) Uani 1 d .
O2 O 0.60413(19) 0.2479(3) 0.00713(18) 0.0365(7) Uani 1 d .
O3 O 0.6017(2) 0.6906(3) -0.0011(2) 0.0492(9) Uani 1 d .
O4 O 0.5209(2) 0.6520(3) -0.11240(18) 0.0429(8) Uani 1 d .
O5 O 0.61032(19) 0.1370(3) 0.18271(18) 0.0440(8) Uani 1 d .
O6 O 0.6535(2) 0.0181(3) 0.10217(17) 0.0411(8) Uani 1 d .
O7 O 0.52839(17) -0.0908(2) -0.03568(15) 0.0277(6) Uani 1 d .
H7 H 0.5535 -0.1428 -0.0057 0.120 Uiso 1 d R
O8 O 1.1066(2) 0.6829(3) 0.21866(17) 0.0403(8) Uani 1 d .
O9 O 1.1016(2) 0.4849(3) 0.2233(2) 0.0652(13) Uani 1 d .
O10 O 1.3298(2) 0.4106(3) 0.4520(2) 0.0562(10) Uani 1 d .
O11 O 1.32811(19) 0.6073(3) 0.43789(17) 0.0387(8) Uani 1 d .
O12 O 1.01105(17) 0.5244(3) 0.07425(15) 0.0292(6) Uani 1 d .
H12 H 1.0444 0.4776 0.1016 0.120 Uiso 1 d R
O13 O 1.0246(2) 0.8150(3) 0.07509(17) 0.0444(9) Uani 1 d .
O14 O 1.0291(2) 0.7500(3) -0.03819(18) 0.0418(8) Uani 1 d .
C1 C 0.2272(3) -0.1093(4) 0.4207(3) 0.0391(11) Uani 1 d .
H1A H 0.2142 -0.1915 0.4271 0.080 Uiso 1 d R
C2 C 0.2813(3) -0.0838(4) 0.3782(3) 0.0396(11) Uani 1 d .
H2A H 0.3044 -0.1477 0.3555 0.080 Uiso 1 d R
C3 C 0.3025(3) 0.0353(4) 0.3675(2) 0.0289(9) Uani 1 d .
C4 C 0.2700(3) 0.1214(4) 0.4072(3) 0.0370(11) Uani 1 d .
H4A H 0.2857 0.2037 0.4057 0.080 Uiso 1 d R
C5 C 0.2159(3) 0.0884(4) 0.4484(3) 0.0371(11) Uani 1 d .
H5A H 0.1947 0.1495 0.4747 0.080 Uiso 1 d R
C6 C 0.3526(2) 0.0677(4) 0.3149(2) 0.0279(9) Uani 1 d .
C7 C 0.3836(3) -0.0198(4) 0.2751(3) 0.0366(11) Uani 1 d .
H7A H 0.3749 -0.1029 0.2835 0.080 Uiso 1 d R
C8 C 0.4263(3) 0.0135(4) 0.2237(3) 0.0375(11) Uani 1 d .
H8A H 0.4478 -0.0481 0.1979 0.080 Uiso 1 d R
C9 C 0.4105(3) 0.2135(4) 0.2463(3) 0.0382(11) Uani 1 d .
H9A H 0.4197 0.2958 0.2362 0.080 Uiso 1 d R
C10 C 0.3677(3) 0.1871(4) 0.2995(3) 0.0380(11) Uani 1 d .
H10A H 0.3487 0.2505 0.3258 0.080 Uiso 1 d R
C11 C 0.5620(3) 0.2720(4) -0.0564(3) 0.0315(10) Uani 1 d .
C12 C 0.5484(3) 0.4012(4) -0.0793(3) 0.0369(11) Uani 1 d .
H12A H 0.5166 0.4201 -0.1276 0.080 Uiso 1 d R
C13 C 0.5795(3) 0.4891(4) -0.0341(3) 0.0398(11) Uani 1 d .
H13A H 0.6125 0.4667 0.0132 0.080 Uiso 1 d R
C14 C 0.5678(3) 0.6212(4) -0.0500(3) 0.0371(11) Uani 1 d .
C15 C 0.6627(3) 0.0739(4) 0.1616(2) 0.0321(10) Uani 1 d .
C16 C 0.7446(3) 0.0703(4) 0.2138(2) 0.0390(11) Uani 1 d .
H16A H 0.7913 0.0680 0.1936 0.080 Uiso 1 d R
C17 C 0.7807(3) 0.3741(4) 0.0930(2) 0.0344(10) Uani 1 d .
H17A H 0.7538 0.3618 0.0422 0.080 Uiso 1 d R
C18 C 0.7361(3) 0.3683(4) 0.1459(3) 0.0360(10) Uani 1 d .
H18A H 0.6798 0.3492 0.1318 0.080 Uiso 1 d R
C19 C 0.7730(3) 0.3889(4) 0.2204(2) 0.0291(9) Uani 1 d .
C20 C 0.8564(3) 0.4104(4) 0.2365(2) 0.0328(10) Uani 1 d .
H20A H 0.8855 0.4216 0.2868 0.080 Uiso 1 d R
C21 C 0.8963(3) 0.4146(4) 0.1807(2) 0.0333(10) Uani 1 d .
H21A H 0.9530 0.4308 0.1933 0.080 Uiso 1 d R
C22 C 0.8422(3) 0.6961(4) 0.1275(3) 0.0377(11) Uani 1 d .
H22A H 0.8344 0.6779 0.0759 0.080 Uiso 1 d R
C23 C 0.7747(3) 0.7078(4) 0.1571(3) 0.0408(11) Uani 1 d .
H23A H 0.7217 0.6981 0.1262 0.080 Uiso 1 d R
C24 C 0.7851(3) 0.7337(4) 0.2319(2) 0.0345(10) Uani 1 d .
C25 C 0.8633(3) 0.7522(4) 0.2733(3) 0.0402(11) Uani 1 d .
H25A H 0.8722 0.7744 0.3244 0.080 Uiso 1 d R
C26 C 0.9269(3) 0.7388(4) 0.2409(3) 0.0361(10) Uani 1 d .
H26A H 0.9805 0.7504 0.2704 0.080 Uiso 1 d R
C27 C 1.1308(3) 0.5814(4) 0.2481(2) 0.0320(10) Uani 1 d .
C28 C 1.1991(3) 0.5870(4) 0.3139(2) 0.0325(10) Uani 1 d .
H28A H 1.2224 0.6638 0.3289 0.080 Uiso 1 d R
C29 C 1.2301(3) 0.4943(4) 0.3540(3) 0.0382(11) Uani 1 d .
H29A H 1.2067 0.4172 0.3402 0.080 Uiso 1 d R
C30 C 1.3000(3) 0.5028(4) 0.4196(3) 0.0357(10) Uani 1 d .
C31 C 1.0223(3) 0.8303(4) 0.0072(2) 0.0323(10) Uani 1 d .
C32 C 1.0087(3) 0.9560(4) -0.0211(2) 0.0353(10) Uani 1 d .
H32A H 1.0126 0.9740 -0.0706 0.080 Uiso 1 d R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O7 Zn1 O6 102.49(13) . .
O7 Zn1 O2 156.77(12) . .
O6 Zn1 O2 97.82(13) . .
O7 Zn1 N1 95.50(13) . 4_655
O6 Zn1 N1 89.11(14) . 4_655
O2 Zn1 N1 95.97(13) . 4_655
O7 Zn1 O7 79.29(12) . 3_655
O6 Zn1 O7 94.98(12) . 3_655
O2 Zn1 O7 87.88(12) . 3_655
N1 Zn1 O7 173.96(12) 4_655 3_655
O7 Zn1 O1 100.80(12) . .
O6 Zn1 O1 156.52(12) . .
O2 Zn1 O1 58.77(12) . .
N1 Zn1 O1 91.55(13) 4_655 .
O7 Zn1 O1 86.46(12) 3_655 .
O7 Zn1 C11 129.05(14) . .
O6 Zn1 C11 127.27(14) . .
O2 Zn1 C11 29.46(13) . .
N1 Zn1 C11 95.46(14) 4_655 .
O7 Zn1 C11 85.61(12) 3_655 .
O1 Zn1 C11 29.36(13) . .
O7 Zn2 O5 110.88(13) 3_655 .
O7 Zn2 O4 109.39(13) 3_655 3_665
O5 Zn2 O4 114.69(15) . 3_665
O7 Zn2 N2 116.77(14) 3_655 .
O5 Zn2 N2 99.99(15) . .
O4 Zn2 N2 104.96(14) 3_665 .
O12 Zn3 O11 148.80(13) . 4_565
O12 Zn3 O14 104.62(13) . 3_765
O11 Zn3 O14 102.49(14) 4_565 3_765
O12 Zn3 N3 97.77(13) . .
O11 Zn3 N3 96.29(14) 4_565 .
O14 Zn3 N3 92.25(14) 3_765 .
O12 Zn3 O12 77.23(12) . 3_765
O11 Zn3 O12 84.29(12) 4_565 3_765
O14 Zn3 O12 97.37(12) 3_765 3_765
N3 Zn3 O12 170.01(12) . 3_765
O12 Zn4 O13 114.42(14) . .
O12 Zn4 O8 116.69(13) . .
O13 Zn4 O8 104.92(15) . .
O12 Zn4 N4 114.43(14) . .
O13 Zn4 N4 99.73(16) . .
O8 Zn4 N4 104.75(15) . .
C5 N1 C1 116.1(4) . .
C5 N1 Zn1 120.7(3) . 4_556
C1 N1 Zn1 122.6(3) . 4_556
C9 N2 C8 117.4(4) . .
C9 N2 Zn2 120.6(3) . .
C8 N2 Zn2 122.0(3) . .
C21 N3 C17 116.9(4) . .
C21 N3 Zn3 122.6(3) . .
C17 N3 Zn3 120.3(3) . .
C22 N4 C26 117.7(4) . .
C22 N4 Zn4 124.0(3) . .
C26 N4 Zn4 118.0(3) . .
C11 O1 Zn1 83.4(3) . .
C11 O2 Zn1 95.9(3) . .
C14 O4 Zn2 117.3(3) . 3_665
C15 O5 Zn2 129.0(3) . .
C15 O6 Zn1 129.3(3) . .
Zn2 O7 Zn1 134.91(15) 3_655 .
Zn2 O7 Zn1 106.47(13) 3_655 3_655
Zn1 O7 Zn1 100.71(12) . 3_655
Zn2 O7 O3 77.45(12) 3_655 1_545
Zn1 O7 O3 121.26(14) . 1_545
Zn1 O7 O3 115.73(14) 3_655 1_545
C27 O8 Zn4 113.8(3) . .
C27 O9 O12 107.8(3) . .
C30 O11 Zn3 105.6(3) . 4_666
Zn4 O12 Zn3 136.21(16) . .
Zn4 O12 Zn3 101.35(12) . 3_765
Zn3 O12 Zn3 102.77(12) . 3_765
Zn4 O12 O9 69.74(12) . .
Zn3 O12 O9 123.99(14) . .
Zn3 O12 O9 121.14(14) 3_765 .
C31 O13 Zn4 131.0(3) . .
C31 O14 Zn3 130.5(3) . 3_765
N1 C1 C2 123.7(4) . .
C1 C2 C3 120.4(4) . .
C4 C3 C2 115.4(4) . .
C4 C3 C6 122.5(4) . .
C2 C3 C6 122.0(4) . .
C5 C4 C3 120.4(4) . .
N1 C5 C4 123.7(4) . .
C10 C6 C7 116.5(4) . .
C10 C6 C3 121.9(4) . .
C7 C6 C3 121.6(4) . .
C8 C7 C6 120.2(4) . .
N2 C8 C7 122.9(4) . .
N2 C9 C10 123.1(4) . .
C9 C10 C6 119.9(4) . .
O1 C11 O2 121.7(4) . .
O1 C11 C12 119.2(4) . .
O2 C11 C12 119.1(4) . .
O1 C11 Zn1 67.2(2) . .
O2 C11 Zn1 54.6(2) . .
C12 C11 Zn1 172.7(3) . .
C13 C12 C11 121.3(4) . .
C12 C13 C14 126.0(5) . .
O3 C14 O4 125.5(4) . .
O3 C14 C13 116.9(5) . .
O4 C14 C13 117.5(4) . .
O6 C15 O5 126.9(4) . .
O6 C15 C16 117.6(4) . .
O5 C15 C16 115.5(4) . .
C16 C16 C15 123.2(6) 2_655 .
N3 C17 C18 123.1(4) . .
C17 C18 C19 120.1(4) . .
C18 C19 C20 116.0(4) . .
C18 C19 C19 122.3(5) . 2_655
C20 C19 C19 121.6(5) . 2_655
C21 C20 C19 120.2(4) . .
N3 C21 C20 123.6(4) . .
N4 C22 C23 122.6(4) . .
C24 C23 C22 119.4(4) . .
C23 C24 C25 117.7(4) . .
C23 C24 C24 121.2(5) . 2_655
C25 C24 C24 120.9(5) . 2_655
C26 C25 C24 119.9(4) . .
N4 C26 C25 122.5(4) . .
O9 C27 O8 123.5(4) . .
O9 C27 C28 121.2(4) . .
O8 C27 C28 115.3(4) . .
C29 C28 C27 124.8(4) . .
C28 C29 C30 123.4(4) . .
O10 C30 O11 123.0(4) . .
O10 C30 C29 120.0(4) . .
O11 C30 C29 116.9(4) . .
O14 C31 O13 126.0(4) . .
O14 C31 C32 117.8(4) . .
O13 C31 C32 116.2(4) . .
C32 C32 C31 121.5(5) 3_775 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Zn1 O7 2.017(3) .
Zn1 O6 2.053(3) .
Zn1 O2 2.089(3) .
Zn1 N1 2.191(4) 4_655
Zn1 O7 2.247(3) 3_655
Zn1 O1 2.366(3) .
Zn1 C11 2.549(4) .
Zn2 O7 1.949(3) 3_655
Zn2 O5 1.956(3) .
Zn2 O4 1.972(3) 3_665
Zn2 N2 2.054(4) .
Zn3 O12 1.986(3) .
Zn3 O11 1.991(3) 4_565
Zn3 O14 2.035(3) 3_765
Zn3 N3 2.175(4) .
Zn3 O12 2.397(3) 3_765
Zn4 O12 1.937(3) .
Zn4 O13 1.939(3) .
Zn4 O8 1.955(3) .
Zn4 N4 2.043(4) .
N1 C5 1.345(6) .
N1 C1 1.352(6) .
N1 Zn1 2.191(4) 4_556
N2 C9 1.341(6) .
N2 C8 1.355(6) .
N3 C21 1.342(6) .
N3 C17 1.351(6) .
N4 C22 1.336(6) .
N4 C26 1.366(6) .
O1 C11 1.258(5) .
O2 C11 1.260(5) .
O3 C14 1.233(6) .
O4 C14 1.294(6) .
O4 Zn2 1.972(3) 3_665
O5 C15 1.272(5) .
O6 C15 1.247(5) .
O7 Zn2 1.949(3) 3_655
O7 Zn1 2.247(3) 3_655
O7 O3 2.754(4) 1_545
O8 C27 1.286(5) .
O9 C27 1.232(6) .
O9 O12 2.876(5) .
O10 C30 1.241(6) .
O11 C30 1.279(6) .
O11 Zn3 1.991(3) 4_666
O12 Zn3 2.397(3) 3_765
O13 C31 1.267(5) .
O14 C31 1.256(5) .
O14 Zn3 2.035(3) 3_765
C1 C2 1.380(7) .
C2 C3 1.406(6) .
C3 C4 1.404(6) .
C3 C6 1.489(6) .
C4 C5 1.383(6) .
C6 C10 1.402(6) .
C6 C7 1.403(6) .
C7 C8 1.383(6) .
C9 C10 1.393(6) .
C11 C12 1.509(6) .
C12 C13 1.322(7) .
C13 C14 1.511(6) .
C15 C16 1.507(6) .
C16 C16 1.316(9) 2_655
C17 C18 1.381(6) .
C18 C19 1.401(6) .
C19 C20 1.407(6) .
C19 C19 1.495(8) 2_655
C20 C21 1.370(6) .
C22 C23 1.395(7) .
C23 C24 1.391(6) .
C24 C25 1.393(7) .
C24 C24 1.508(9) 2_655
C25 C26 1.370(7) .
C27 C28 1.484(6) .
C28 C29 1.314(6) .
C29 C30 1.499(6) .
C31 C32 1.500(6) .
C32 C32 1.335(9) 3_775
