Crystallography Open Database

Information card for entry 1512676

Preview

Coordinates	1512676.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	{(hapto^6^-p-Cymene)[N-(8-bromo-5,11-dihydroindolo[3,2-c]quinolin-6- ylidene)-kappaN'-(1-kappaN-pyridin-2-yl-ethylidene)]azine chloridoosmium(II)}chloride hydrate
Formula	C32 H31.5 Br Cl2 N5 O0.75 Os
Calculated formula	C32 H31.5 Br Cl2 N5 O0.75 Os
Title of publication	Ruthenium- and Osmium-Arene Complexes of 8-Substituted Indolo[3,2-c]quinolines: Synthesis,X-ray Diffraction Structures, Spectroscopic Properties, and Antiproli- ferative Activity
Authors of publication	Lukas K. Filak; Simone Goeschl; Stefanie Hackl; Michael A. Jakupec; Vladimir B. Arion
Journal of publication	Inorganica Chimica Acta
Year of publication	2012
Journal volume	393
Pages of publication	252 - 260
a	12.3508 ± 0.0004 Å
b	13.3564 ± 0.0005 Å
c	20.584 ± 0.0008 Å
α	98.018 ± 0.002°
β	95.312 ± 0.002°
γ	112.859 ± 0.003°
Cell volume	3058 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0287
Residual factor for significantly intense reflections	0.0208
Weighted residual factors for significantly intense reflections	0.0482
Weighted residual factors for all reflections included in the refinement	0.0506
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176435 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries from ranges 1, 2.	1512676.cif
120071	2014-07-11	Adding DOIs to range 1 structures.	1512676.cif
90736	2013-11-18	cif/ Adding structures of 1512676 via cif-deposit CGI script.	1512676.cif