Crystallography Open Database

Information card for entry 1512677

Preview

Coordinates	1512677.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	{(hapto^6^-p-Cymene)[N-(8-methyl-5,11-dihydroindolo[3,2-c]quinolin-6- ylidene)-kappaN'-(1-kappaN-pyridin-2-yl-ethylidene)]azine chloridoosmium(II)}chloride hydrate diethyl ether solvate
Formula	C34 H38.25 Cl2 N5 O1.63 Os
Calculated formula	C34 H36.5 Cl2 N5 O1.625 Os
Title of publication	Ruthenium- and Osmium-Arene Complexes of 8-Substituted Indolo[3,2-c]quinolines: Synthesis,X-ray Diffraction Structures, Spectroscopic Properties, and Antiproli- ferative Activity
Authors of publication	Lukas K. Filak; Simone Goeschl; Stefanie Hackl; Michael A. Jakupec; Vladimir B. Arion
Journal of publication	Inorganica Chimica Acta
Year of publication	2012
Journal volume	393
Pages of publication	252 - 260
a	11.298 ± 0.0009 Å
b	14.494 ± 0.0012 Å
c	21.3506 ± 0.0018 Å
α	99.901 ± 0.005°
β	92.072 ± 0.004°
γ	98.838 ± 0.005°
Cell volume	3396.2 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0551
Residual factor for significantly intense reflections	0.0386
Weighted residual factors for significantly intense reflections	0.0933
Weighted residual factors for all reflections included in the refinement	0.0988
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1512677.cif
120071	2014-07-11	Adding DOIs to range 1 structures.	1512677.cif
90737	2013-11-18	cif/ Adding structures of 1512677 via cif-deposit CGI script.	1512677.cif