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Information card for entry 4068105
Preview
| Coordinates | 4068105.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C44.5 H81 N4 Nd Si4 |
|---|---|
| Calculated formula | C44.5 H77 N4 Nd Si4 |
| Title of publication | Synthesis of Dianionic β-Diketiminate Lanthanide Amides L′LnN(SiMe3)2(THF) by Deprotonation of the β-Diketiminate Ligand L (L = {[(2,6-iPr2C6H3)NC(CH3)]2CH}−) and the Transformation with [HNEt3][BPh4] to the Cationic Samarium Amide [LSmN(SiMe3)2][BPh4] |
| Authors of publication | Liu, Peng; Zhang, Yong; Yao, Yingming; Shen, Qi |
| Journal of publication | Organometallics |
| Year of publication | 2012 |
| Journal volume | 31 |
| Journal issue | 3 |
| Pages of publication | 1017 |
| a | 11.7324 ± 0.0003 Å |
| b | 11.7814 ± 0.0002 Å |
| c | 20.5952 ± 0.0006 Å |
| α | 75.163 ± 0.003° |
| β | 79.407 ± 0.003° |
| γ | 68.293 ± 0.003° |
| Cell volume | 2544.08 ± 0.12 Å3 |
| Cell temperature | 223 ± 2 K |
| Ambient diffraction temperature | 223 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0337 |
| Residual factor for significantly intense reflections | 0.0303 |
| Weighted residual factors for significantly intense reflections | 0.0764 |
| Weighted residual factors for all reflections included in the refinement | 0.0793 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.064 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176467 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4068105.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4068105.cif |
| 38083 | 2012-03-04 | ../uploads/cif-deposit/cod/cif Adding structures of 4068101, 4068102, 4068103, 4068104, 4068105, 4068106, 4068107 via cif-deposit CGI script. |
4068105.cif |
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Users of the data should acknowledge the original authors of the
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