Crystallography Open Database

Information card for entry 4078107

Preview

Coordinates	4078107.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H37 Cl2 P Ru2 S
Calculated formula	C22 H37 Cl2 P Ru2 S
Title of publication	Synthesis and Reactivity of Hybrid Phosphido- and Hydrosulfido-Bridged Diruthenium Complexes: Transformations into Diruthenium and Tetraruthenium Complexes Bridged by Phosphido and Sulfido Ligands
Authors of publication	Miyake, Yoshihiro; Moriyama, Taichi; Tanabe, Yoshiaki; Endo, Satoshi; Nishibayashi, Yoshiaki
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	8
Pages of publication	3292
a	16.5909 ± 0.0006 Å
b	8.5787 ± 0.0004 Å
c	18.0461 ± 0.0007 Å
α	90°
β	108.652 ± 0.0012°
γ	90°
Cell volume	2433.57 ± 0.17 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0175
Weighted residual factors for all reflections included in the refinement	0.0444
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178670 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/81.	4078107.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4078107.cif
57710	2012-05-18	cif/ Adding structures of 4078107, 4078108, 4078109, 4078110, 4078111, 4078112 via cif-deposit CGI script.	4078107.cif