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Information card for entry 4308275
Preview
| Coordinates | 4308275.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | (DIPP-nacnac)YbH.THF dimer |
|---|---|
| Formula | C22 H33.33 N1.33 O0.67 Yb0.67 |
| Calculated formula | C22 H33.3333 N1.33333 O0.666667 Yb0.666667 |
| Title of publication | Syntheses and Structures of Ytterbium(II) Hydride and Hydroxide Complexes: Similarities and Differences with Their Calcium Analogues |
| Authors of publication | Christian Ruspic; Jan Spielmann; Sjoerd Harder |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2007 |
| Journal volume | 46 |
| Pages of publication | 5320 - 5326 |
| a | 13.2493 ± 0.0005 Å |
| b | 14.5646 ± 0.0005 Å |
| c | 18.9955 ± 0.0007 Å |
| α | 90° |
| β | 93.654 ± 0.002° |
| γ | 90° |
| Cell volume | 3658.1 ± 0.2 Å3 |
| Cell temperature | 183 ± 2 K |
| Ambient diffraction temperature | 183 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0384 |
| Residual factor for significantly intense reflections | 0.0282 |
| Weighted residual factors for significantly intense reflections | 0.0671 |
| Weighted residual factors for all reflections included in the refinement | 0.0705 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.077 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179120 (current) | 2016-03-23 | cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/82. |
4308275.cif |
| 120081 | 2014-07-12 | Adding DOIs to range 4/30 structures. | 4308275.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4308275.cif |
| 17004 | 2011-03-31 | cif/ Commiting CIFs, that were updated with the 'cif_fix_values' script, using options '--fix-misspelled replacement_values.lst', '--fix-temperature' and '--fix-enums' with built-in table of enum values. The following cmd was used: > (set -x; find ? -name \*.cif | sort | xargs -i sh -c 'if !( > cif_fix_values --fix-misspelled ~/../inputs/replacament_values.lst {} | > cif_filter --add-cif-header {} | > sponge {} ) 2>&1 | grep NOTE; then svn revert {}; > fi' ) & |
4308275.cif |
| 1194 | 2010-06-06 | cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory. |
4308275.cif |
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