Crystallography Open Database

Information card for entry 4308276

Preview

Coordinates	4308276.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	DIPP-nacnac-Yb(OH)THF-dimer (toluene)0.5
Formula	C36.5 H54 N2 O2 Yb
Calculated formula	C36.5 H54 N2 O2 Yb
Title of publication	Syntheses and Structures of Ytterbium(II) Hydride and Hydroxide Complexes: Similarities and Differences with Their Calcium Analogues
Authors of publication	Christian Ruspic; Jan Spielmann; Sjoerd Harder
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	5320 - 5326
a	12.6955 ± 0.0015 Å
b	12.7651 ± 0.0015 Å
c	13.3877 ± 0.0014 Å
α	97.95 ± 0.007°
β	114.063 ± 0.007°
γ	111.239 ± 0.007°
Cell volume	1739.1 ± 0.4 Å³
Cell temperature	183 ± 2 K
Ambient diffraction temperature	183 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0525
Residual factor for significantly intense reflections	0.0475
Weighted residual factors for significantly intense reflections	0.1354
Weighted residual factors for all reflections included in the refinement	0.1455
Goodness-of-fit parameter for all reflections included in the refinement	1.106
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4308276.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4308276.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4308276.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4308276.cif