Crystallography Open Database

Information card for entry 4311294

Preview

Coordinates	4311294.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H14 Cl2 N4 O Ru
Calculated formula	C18 H14 Cl2 N4 O Ru
Title of publication	cis-[Ru(2,2':6',2''-terpyridine)(DMSO)Cl2]: Useful Precursor for the Synthesis of Heteroleptic Terpyridine Complexes under Mild Conditions
Authors of publication	Raymond Ziessel; Vincent Grosshenny; Muriel Hissler; Christophe Stroh
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	4262 - 4271
a	8.7062 ± 0.0003 Å
b	10.3326 ± 0.0004 Å
c	10.8419 ± 0.0004 Å
α	99.214 ± 0.005°
β	101.015 ± 0.005°
γ	93.748 ± 0.005°
Cell volume	940.35 ± 0.06 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.035
Residual factor for significantly intense reflections	0.029
Weighted residual factors for all reflections	0.147
Weighted residual factors for all reflections included in the refinement	0.046
Goodness-of-fit parameter for all reflections	1.299
Goodness-of-fit parameter for all reflections included in the refinement	1.117
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	Mo-Kα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179151 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/12.	4311294.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4311294.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4311294.cif
2789	2010-11-12	../uploads/cif-deposit/cod/cif Adding structures of 4311294 via cif-deposit CGI script.	4311294.cif