Crystallography Open Database

Information card for entry 4311295

Preview

Coordinates	4311295.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H44 Cl10 N6 O4 Ru2 S2
Calculated formula	C37 H22 Cl10 N6 O4 Ru2 S2
Title of publication	cis-[Ru(2,2':6',2''-terpyridine)(DMSO)Cl2]: Useful Precursor for the Synthesis of Heteroleptic Terpyridine Complexes under Mild Conditions
Authors of publication	Raymond Ziessel; Vincent Grosshenny; Muriel Hissler; Christophe Stroh
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	4262 - 4271
a	10.9878 ± 0.0004 Å
b	29.844 ± 0.001 Å
c	8.6903 ± 0.0005 Å
α	90°
β	118.496 ± 0.005°
γ	90°
Cell volume	2504.5 ± 0.2 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	7
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.087
Residual factor for significantly intense reflections	0.055
Weighted residual factors for all reflections	0.134
Weighted residual factors for all reflections included in the refinement	0.072
Goodness-of-fit parameter for all reflections	1.953
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	Mo-Kα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179151 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/12.	4311295.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4311295.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4311295.cif
2790	2010-11-12	../uploads/cif-deposit/cod/cif Adding structures of 4311295 via cif-deposit CGI script.	4311295.cif