Crystallography Open Database

Information card for entry 4317712

Preview

Coordinates	4317712.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H32 F12 N6 O6 P2 Ru2
Calculated formula	C16 H16 F6 N3 O3.5 P Ru
Title of publication	Homologous Series of Redox-Active, Dinuclear Cations [M2(O2CCH3)2(pynp)2]2+ (M = Mo, Ru, Rh) with the Bridging Ligand 2-(2-Pyridyl)-1,8-naphthyridine (pynp)
Authors of publication	Cristian Saul Campos-Fernández; Lisa M. Thomson; José Ramón Galán-Mascarós; Xiang Ouyang; Kim R. Dunbar
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	1523 - 1533
a	14.2228 ± 0.0007 Å
b	20.3204 ± 0.0009 Å
c	14.1022 ± 0.0007 Å
α	90°
β	95.144 ± 0.001°
γ	90°
Cell volume	4059.3 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0812
Residual factor for significantly intense reflections	0.0617
Weighted residual factors for significantly intense reflections	0.17
Weighted residual factors for all reflections included in the refinement	0.1798
Goodness-of-fit parameter for all reflections included in the refinement	1.078
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179257 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/77.	4317712.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4317712.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4317712.cif
13990	2011-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4317712 via cif-deposit CGI script.	4317712.cif