Crystallography Open Database

Information card for entry 4317713

Preview

Coordinates	4317713.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H36 B2 F8 N6 O4 Rh2
Calculated formula	C37 H24 B2 F8 N6 O4 Rh2
Title of publication	Homologous Series of Redox-Active, Dinuclear Cations [M2(O2CCH3)2(pynp)2]2+ (M = Mo, Ru, Rh) with the Bridging Ligand 2-(2-Pyridyl)-1,8-naphthyridine (pynp)
Authors of publication	Cristian Saul Campos-Fernández; Lisa M. Thomson; José Ramón Galán-Mascarós; Xiang Ouyang; Kim R. Dunbar
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	1523 - 1533
a	13.4086 ± 0.0015 Å
b	21.67 ± 0.003 Å
c	13.7261 ± 0.0016 Å
α	90°
β	94.865 ± 0.002°
γ	90°
Cell volume	3973.9 ± 0.8 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1773
Residual factor for significantly intense reflections	0.1062
Weighted residual factors for significantly intense reflections	0.2365
Weighted residual factors for all reflections included in the refinement	0.2809
Goodness-of-fit parameter for all reflections included in the refinement	1.117
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179257 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/77.	4317713.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4317713.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4317713.cif
13991	2011-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4317713 via cif-deposit CGI script.	4317713.cif