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Information card for entry 4318453
Preview
| Coordinates | 4318453.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | (trifluorovinyl)triphenylgermanium |
|---|---|
| Formula | C20 H15 F3 Ge |
| Calculated formula | C20 H15 F3 Ge |
| Title of publication | Spectroscopic and Structural Assignment of the Absolute Stereochemistry in a Series of 1,2-Difluorovinyl Organometalloids. The First Crystallographic Characterization and Structural Series of Group 14 Fluorovinyl Compounds |
| Authors of publication | Alan K. Brisdon; Ian R. Crossley; Robin G. Pritchard; John E. Warren |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2002 |
| Journal volume | 41 |
| Pages of publication | 4748 - 4755 |
| a | 10.087 ± 0.002 Å |
| b | 10.338 ± 0.005 Å |
| c | 18.704 ± 0.009 Å |
| α | 103.05 ± 0.04° |
| β | 95.43 ± 0.03° |
| γ | 108.91 ± 0.02° |
| Cell volume | 1767.5 ± 1.3 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1488 |
| Residual factor for significantly intense reflections | 0.0648 |
| Weighted residual factors for significantly intense reflections | 0.139 |
| Weighted residual factors for all reflections included in the refinement | 0.1716 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.003 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179264 (current) | 2016-03-23 | cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/84. |
4318453.cif |
| 131566 | 2015-02-08 | cif/ Changing empty string values "' '" into "." in range 4. In case of "_symmetry_cell_setting" tag values were added after consulting the original papers. |
4318453.cif |
| 120093 | 2014-07-12 | Adding DOIs to range 4/31 structures. | 4318453.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4318453.cif |
| 15167 | 2011-03-14 | ../uploads/cif-deposit/cod/cif Adding structures of 4318453 via cif-deposit CGI script. |
4318453.cif |
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