Crystallography Open Database

Information card for entry 4318454

Preview

Coordinates	4318454.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H15 F3 Sn
Calculated formula	C20 H15 F3 Sn
Title of publication	Spectroscopic and Structural Assignment of the Absolute Stereochemistry in a Series of 1,2-Difluorovinyl Organometalloids. The First Crystallographic Characterization and Structural Series of Group 14 Fluorovinyl Compounds
Authors of publication	Alan K. Brisdon; Ian R. Crossley; Robin G. Pritchard; John E. Warren
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	4748 - 4755
a	9.6807 ± 0.0006 Å
b	9.9819 ± 0.0008 Å
c	18.2114 ± 0.0014 Å
α	90.02 ± 0.004°
β	85.893 ± 0.004°
γ	87.843 ± 0.003°
Cell volume	1754 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1099
Residual factor for significantly intense reflections	0.087
Weighted residual factors for significantly intense reflections	0.2216
Weighted residual factors for all reflections included in the refinement	0.246
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4318454.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4318454.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4318454.cif
15168	2011-03-14	../uploads/cif-deposit/cod/cif Adding structures of 4318454 via cif-deposit CGI script.	4318454.cif