Crystallography Open Database

Information card for entry 4329143

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Coordinates	4329143.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	3
Formula	C28 H46 N2 Si2 Sn
Calculated formula	C28 H46 N2 Si2 Sn
SMILES	[Sn]1N([Si]([Si](N1c1c(cccc1C(C)C)C(C)C)(C)C)(C)C)c1c(cccc1C(C)C)C(C)C
Title of publication	Expanding the Steric Coverage Offered by Bis(amidosilyl) Chelates: Isolation of Low-Coordinate N-Heterocyclic Germylene Complexes
Authors of publication	Sean K. Liew; S. M. Ibrahim Al-Rafia; James T. Goettel; Paul A. Lummis; Sean M. McDonald; Leah J. Miedema; Michael J. Ferguson; Robert McDonald; Eric Rivard
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	5471 - 5480
a	9.1347 ± 0.0005 Å
b	10.0168 ± 0.0005 Å
c	19.1344 ± 0.001 Å
α	76.6557 ± 0.0005°
β	86.6259 ± 0.0005°
γ	66.6516 ± 0.0005°
Cell volume	1562.99 ± 0.14 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0199
Residual factor for significantly intense reflections	0.0186
Weighted residual factors for significantly intense reflections	0.0527
Weighted residual factors for all reflections included in the refinement	0.0586
Goodness-of-fit parameter for all reflections included in the refinement	1.129
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179394 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/91.	4329143.cif
78183	2013-04-01	cif/ Adding structures of 4329143 via cif-deposit CGI script.	4329143.cif