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Information card for entry 4329144
Preview
| Coordinates | 4329144.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Common name | 4 |
|---|---|
| Formula | C67 H108 Ge2 N4 O S2 Si4 |
| Calculated formula | C67 H108 Ge2 N4 O S2 Si4 |
| Title of publication | Expanding the Steric Coverage Offered by Bis(amidosilyl) Chelates: Isolation of Low-Coordinate N-Heterocyclic Germylene Complexes |
| Authors of publication | Sean K. Liew; S. M. Ibrahim Al-Rafia; James T. Goettel; Paul A. Lummis; Sean M. McDonald; Leah J. Miedema; Michael J. Ferguson; Robert McDonald; Eric Rivard |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2012 |
| Journal volume | 51 |
| Pages of publication | 5471 - 5480 |
| a | 9.96 ± 0.002 Å |
| b | 14.101 ± 0.003 Å |
| c | 15.228 ± 0.003 Å |
| α | 102.871 ± 0.003° |
| β | 93.857 ± 0.003° |
| γ | 107.097 ± 0.002° |
| Cell volume | 1972.5 ± 0.7 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1149 |
| Residual factor for significantly intense reflections | 0.087 |
| Weighted residual factors for significantly intense reflections | 0.2477 |
| Weighted residual factors for all reflections included in the refinement | 0.2703 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.084 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301838 (current) | 2025-08-21 | Add cross-references to PubChem compounds in COD range 4/32/ Each referenced PubChem compound corresponds to the full crystal structure. |
4329144.cif |
| 179394 | 2016-03-23 | cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/91. |
4329144.cif |
| 78184 | 2013-04-01 | cif/ Adding structures of 4329144 via cif-deposit CGI script. |
4329144.cif |
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Users of the data should acknowledge the original authors of the
structural data.