Crystallography Open Database

Information card for entry 4329146

Preview

Coordinates	4329146.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	7
Formula	C27 H35 N Si
Calculated formula	C27 H35 N Si
Title of publication	Expanding the Steric Coverage Offered by Bis(amidosilyl) Chelates: Isolation of Low-Coordinate N-Heterocyclic Germylene Complexes
Authors of publication	Sean K. Liew; S. M. Ibrahim Al-Rafia; James T. Goettel; Paul A. Lummis; Sean M. McDonald; Leah J. Miedema; Michael J. Ferguson; Robert McDonald; Eric Rivard
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	5471 - 5480
a	15.0786 ± 0.0016 Å
b	6.8829 ± 0.0007 Å
c	23.297 ± 0.003 Å
α	90°
β	93.6135 ± 0.0014°
γ	90°
Cell volume	2413.1 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0559
Residual factor for significantly intense reflections	0.0371
Weighted residual factors for significantly intense reflections	0.0915
Weighted residual factors for all reflections included in the refinement	0.1018
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179394 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/91.	4329146.cif
78186	2013-04-01	cif/ Adding structures of 4329146 via cif-deposit CGI script.	4329146.cif