Crystallography Open Database

Information card for entry 4329147

Preview

Coordinates	4329147.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	12
Formula	C58 H78 Ge N2 Si4
Calculated formula	C58 H78 Ge N2 Si4
Title of publication	Expanding the Steric Coverage Offered by Bis(amidosilyl) Chelates: Isolation of Low-Coordinate N-Heterocyclic Germylene Complexes
Authors of publication	Sean K. Liew; S. M. Ibrahim Al-Rafia; James T. Goettel; Paul A. Lummis; Sean M. McDonald; Leah J. Miedema; Michael J. Ferguson; Robert McDonald; Eric Rivard
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	5471 - 5480
a	18.6549 ± 0.0005 Å
b	16.2623 ± 0.0004 Å
c	21.0055 ± 0.0005 Å
α	90°
β	116.425 ± 0.001°
γ	90°
Cell volume	5706.7 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0811
Residual factor for significantly intense reflections	0.0675
Weighted residual factors for significantly intense reflections	0.1791
Weighted residual factors for all reflections included in the refinement	0.1928
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179394 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/91.	4329147.cif
78187	2013-04-01	cif/ Adding structures of 4329147 via cif-deposit CGI script.	4329147.cif