Crystallography Open Database

Information card for entry 4329148

Preview

Coordinates	4329148.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C148 H188 Ge2 N4 S2 Si6
Calculated formula	C136 H160 Ge2 N4 S2 Si6
Title of publication	Expanding the Steric Coverage Offered by Bis(amidosilyl) Chelates: Isolation of Low-Coordinate N-Heterocyclic Germylene Complexes
Authors of publication	Sean K. Liew; S. M. Ibrahim Al-Rafia; James T. Goettel; Paul A. Lummis; Sean M. McDonald; Leah J. Miedema; Michael J. Ferguson; Robert McDonald; Eric Rivard
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	5471 - 5480
a	15.3279 ± 0.0011 Å
b	16.5942 ± 0.0012 Å
c	16.8715 ± 0.0013 Å
α	62.851 ± 0.003°
β	66.564 ± 0.004°
γ	83.17 ± 0.004°
Cell volume	3493.2 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0956
Residual factor for significantly intense reflections	0.0722
Weighted residual factors for significantly intense reflections	0.2076
Weighted residual factors for all reflections included in the refinement	0.2328
Goodness-of-fit parameter for all reflections included in the refinement	1.102
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179394 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/91.	4329148.cif
78188	2013-04-01	cif/ Adding structures of 4329148 via cif-deposit CGI script.	4329148.cif