Crystallography Open Database

Information card for entry 4333300

Preview

Coordinates	4333300.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C156 H206 As32 N46 O170 V54 Zn10
Calculated formula	C156 H198 As32 N46 O170 V54 Zn10
Title of publication	In situ ligand reactions under hydrothermal conditions afford a novel zinc-substituted polyoxovanadate dimer.
Authors of publication	Zheng, Shou-Tian; Wang, Ming-Hui; Yang, Guo-Yu
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	22
Pages of publication	9503 - 9508
a	28.3414 ± 0.0014 Å
b	27.9995 ± 0.0016 Å
c	41.5819 ± 0.0016 Å
α	90°
β	90°
γ	90°
Cell volume	32997 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	41
Hermann-Mauguin space group symbol	A b a 2
Hall space group symbol	A 2 -2ab
Residual factor for all reflections	0.075
Residual factor for significantly intense reflections	0.0644
Weighted residual factors for significantly intense reflections	0.1575
Weighted residual factors for all reflections included in the refinement	0.1692
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179436 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/33.	4333300.cif
116724	2014-06-13	cif/ Updating files of 4333300, 4333301 Original log message: Adding full bibliography for 4333300--4333301.cif.	4333300.cif
98915	2014-01-30	cif/ Adding structures of 4333300 via cif-deposit CGI script.	4333300.cif