Crystallography Open Database

Information card for entry 4333301

Preview

Coordinates	4333301.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H118 As16 N24 O87 V24 Zn8
Calculated formula	C32 H100 As16 N24 O87 V24 Zn8
Title of publication	In situ ligand reactions under hydrothermal conditions afford a novel zinc-substituted polyoxovanadate dimer.
Authors of publication	Zheng, Shou-Tian; Wang, Ming-Hui; Yang, Guo-Yu
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	22
Pages of publication	9503 - 9508
a	15.5635 ± 0.0003 Å
b	19.6903 ± 0.0004 Å
c	24.8067 ± 0.0004 Å
α	85.215 ± 0.005°
β	89.402 ± 0.004°
γ	82.088 ± 0.003°
Cell volume	7503.4 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1333
Residual factor for significantly intense reflections	0.0893
Weighted residual factors for significantly intense reflections	0.2164
Weighted residual factors for all reflections included in the refinement	0.2504
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179436 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/33.	4333301.cif
116724	2014-06-13	cif/ Updating files of 4333300, 4333301 Original log message: Adding full bibliography for 4333300--4333301.cif.	4333301.cif
98916	2014-01-30	cif/ Adding structures of 4333301 via cif-deposit CGI script.	4333301.cif