Crystallography Open Database

Information card for entry 4333619

Preview

Coordinates	4333619.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Co3 H62 K6 Na4 O97 Si2 W18
Calculated formula	Co3 K6 Na4 O89.8 Si2 W18
Title of publication	Di- and Tri-Cobalt Silicotungstates: Synthesis, Characterization, and Stability Studies
Authors of publication	Guibo Zhu; Yurii V. Geletii; Jie Song; Chongchao Zhao; Elliot N. Glass; John Bacsa; Craig L. Hill
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	1018 - 1024
a	13.3935 ± 0.0012 Å
b	16.1715 ± 0.0015 Å
c	20.3596 ± 0.0018 Å
α	90°
β	106.364 ± 0.001°
γ	90°
Cell volume	4231.1 ± 0.7 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0952
Residual factor for significantly intense reflections	0.0487
Weighted residual factors for significantly intense reflections	0.1025
Weighted residual factors for all reflections included in the refinement	0.1212
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179439 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/36.	4333619.cif
99415	2014-01-31	cif/ Adding structures of 4333619 via cif-deposit CGI script.	4333619.cif