Crystallography Open Database

Information card for entry 4333620

Preview

Coordinates	4333620.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Co2 H50 K12 O91 Si2 W18
Calculated formula	Co2 H10 K12 O91 Si2 W18
Title of publication	Di- and Tri-Cobalt Silicotungstates: Synthesis, Characterization, and Stability Studies
Authors of publication	Guibo Zhu; Yurii V. Geletii; Jie Song; Chongchao Zhao; Elliot N. Glass; John Bacsa; Craig L. Hill
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	1018 - 1024
a	12.2891 ± 0.0003 Å
b	23.5596 ± 0.0005 Å
c	30.7185 ± 0.0007 Å
α	90°
β	95.88 ± 0.001°
γ	90°
Cell volume	8847 ± 0.4 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0592
Residual factor for significantly intense reflections	0.0482
Weighted residual factors for significantly intense reflections	0.1104
Weighted residual factors for all reflections included in the refinement	0.1154
Goodness-of-fit parameter for all reflections included in the refinement	1.085
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179439 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/36.	4333620.cif
99416	2014-01-31	cif/ Adding structures of 4333620 via cif-deposit CGI script.	4333620.cif