Crystallography Open Database

Information card for entry 4334960

Preview

Coordinates	4334960.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H33 Dy F12 N2 Ni O12
Calculated formula	C33 H33 Dy F12 N2 Ni O12
Title of publication	Syntheses, Structures, and Magnetic Properties of Acetato- and Diphenolato-Bridged 3d-4f Binuclear Complexes [M(3-MeOsaltn)(MeOH)x(ac)Ln(hfac)2] (M = ZnII, CuII, NiII, CoII; Ln = LaIII, GdIII, TbIII, DyIII; 3-MeOsaltn =N,N'-Bis(3-methoxy-2-oxybenzylidene)-1,3-propanediaminato; ac = Acetato; hfac = Hexafluoroacetylacetonato;x= 0 or 1)
Authors of publication	Masaaki Towatari; Koshiro Nishi; Takeshi Fujinami; Naohide Matsumoto; Yukinari Sunatsuki; Masaaki Kojima; Naotaka Mochida; Takayuki Ishida; Nazzareno Re; Jerzy Mrozinski
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	6160 - 6178
a	17.1346 ± 0.0004 Å
b	12.6797 ± 0.0003 Å
c	19.4864 ± 0.0004 Å
α	90°
β	109.735 ± 0.0007°
γ	90°
Cell volume	3984.98 ± 0.16 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for significantly intense reflections	0.0405
Weighted residual factors for all reflections included in the refinement	0.1045
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179452 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/49.	4334960.cif
100846	2014-02-07	cif/ Adding structures of 4334960 via cif-deposit CGI script.	4334960.cif