Crystallography Open Database

Information card for entry 4334961

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Coordinates	4334961.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H25 Cu F12 Gd N2 O10
Calculated formula	C31 H25 Cu F12 Gd N2 O10
Title of publication	Syntheses, Structures, and Magnetic Properties of Acetato- and Diphenolato-Bridged 3d-4f Binuclear Complexes [M(3-MeOsaltn)(MeOH)x(ac)Ln(hfac)2] (M = ZnII, CuII, NiII, CoII; Ln = LaIII, GdIII, TbIII, DyIII; 3-MeOsaltn =N,N'-Bis(3-methoxy-2-oxybenzylidene)-1,3-propanediaminato; ac = Acetato; hfac = Hexafluoroacetylacetonato;x= 0 or 1)
Authors of publication	Masaaki Towatari; Koshiro Nishi; Takeshi Fujinami; Naohide Matsumoto; Yukinari Sunatsuki; Masaaki Kojima; Naotaka Mochida; Takayuki Ishida; Nazzareno Re; Jerzy Mrozinski
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	6160 - 6178
a	10.2246 ± 0.0003 Å
b	11.4639 ± 0.0003 Å
c	17.5688 ± 0.0005 Å
α	86.3787 ± 0.0009°
β	75.3313 ± 0.0008°
γ	66.2417 ± 0.0007°
Cell volume	1821.6 ± 0.09 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0407
Weighted residual factors for all reflections included in the refinement	0.1126
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179452 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/49.	4334961.cif
100847	2014-02-07	cif/ Adding structures of 4334961 via cif-deposit CGI script.	4334961.cif