Crystallography Open Database

Information card for entry 4339739

Preview

Coordinates	4339739.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H31 N4 O10 Pr
Calculated formula	C48 H31 N4 O10 Pr
Title of publication	Porphyrin framework solids. Synthesis and structure of hybrid coordination polymers of tetra(carboxyphenyl)porphyrins and lanthanide-bridging ions.
Authors of publication	Muniappan, Sankar; Lipstman, Sophia; George, Sumod; Goldberg, Israel
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	14
Pages of publication	5544 - 5554
a	9.6357 ± 0.0002 Å
b	13.9203 ± 0.0003 Å
c	17.2875 ± 0.0005 Å
α	98.1574 ± 0.0009°
β	89.7511 ± 0.0009°
γ	89.1062 ± 0.0016°
Cell volume	2295.01 ± 0.1 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0574
Residual factor for significantly intense reflections	0.0415
Weighted residual factors for significantly intense reflections	0.0938
Weighted residual factors for all reflections included in the refinement	0.0996
Goodness-of-fit parameter for all reflections included in the refinement	0.957
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179500 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/97.	4339739.cif
117510	2014-06-15	cif/ Adding structures of 4339737, 4339738, 4339739, 4339740, 4339741, 4339742, 4339743 via cif-deposit CGI script.	4339739.cif