Crystallography Open Database

Information card for entry 4339740

Preview

Coordinates	4339740.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H28 Ca0.18 N4 O10 Sm
Calculated formula	C48 H28 Ca0.181 N4 O10 Sm
Title of publication	Porphyrin framework solids. Synthesis and structure of hybrid coordination polymers of tetra(carboxyphenyl)porphyrins and lanthanide-bridging ions.
Authors of publication	Muniappan, Sankar; Lipstman, Sophia; George, Sumod; Goldberg, Israel
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	14
Pages of publication	5544 - 5554
a	9.6187 ± 0.0003 Å
b	13.8934 ± 0.0006 Å
c	17.2345 ± 0.0007 Å
α	98.058 ± 0.002°
β	90.457 ± 0.002°
γ	90.599 ± 0.003°
Cell volume	2280.19 ± 0.15 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.067
Residual factor for significantly intense reflections	0.0497
Weighted residual factors for significantly intense reflections	0.1121
Weighted residual factors for all reflections included in the refinement	0.1178
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179500 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/97.	4339740.cif
117510	2014-06-15	cif/ Adding structures of 4339737, 4339738, 4339739, 4339740, 4339741, 4339742, 4339743 via cif-deposit CGI script.	4339740.cif