Crystallography Open Database

Information card for entry 7012475

Preview

Coordinates	7012475.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H22 Fe O12 Os3 P
Calculated formula	C32 H22 Fe O12 Os3 P
Title of publication	Reaction of metallophosphanide anions with MLnX (X = halide) species as a simple route to heterometallic transition metal complexes
Authors of publication	Birte Ahrens; Jacqueline M. Cole; Jonathan P. Hickey; James N. Martin; Martin J. Mays; Paul R. Raithby; Simon J. Teat; Anthony D. Woods
Journal of publication	Dalton Trans.
Year of publication	2003
Journal issue	7
Pages of publication	1389 - 1395
a	8.9577 ± 0.0019 Å
b	10.834 ± 0.002 Å
c	34.169 ± 0.007 Å
α	90°
β	94.537 ± 0.01°
γ	90°
Cell volume	3305.6 ± 1.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0786
Residual factor for significantly intense reflections	0.0559
Weighted residual factors for significantly intense reflections	0.0935
Weighted residual factors for all reflections included in the refinement	0.0973
Goodness-of-fit parameter for all reflections included in the refinement	1.178
Diffraction radiation wavelength	0.6923 Å
Diffraction radiation type	Synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
213973 (current)	2019-03-05	cod/ Removed potentially copyrighted or irrelevant data items from 1289 entries.	7012475.cif
179828	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/24.	7012475.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7012475.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7012475.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7012475.cif