Crystallography Open Database

Information card for entry 7020800

7020799 << 7020800 >> 7020801

Preview

Coordinates	7020800.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H42 Ni O2 P2
Calculated formula	C19 H42 Ni O2 P2
SMILES	[Ni]1([P](C(C)C)(C(C)C)C(C)C)([P](C(C)C)(C(C)C)C(C)C)[O]=[C]1=O
Title of publication	Synthesis and chemistry of bis(triisopropylphosphine) nickel(i) and nickel(0) precursors.
Authors of publication	Beck, Robert; Shoshani, Manar; Krasinkiewicz, Jonathan; Hatnean, Jillian A.; Johnson, Samuel A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	5
Pages of publication	1461 - 1475
a	8.1143 ± 0.0003 Å
b	8.465 ± 0.0004 Å
c	18.9139 ± 0.0003 Å
α	89.338 ± 0.001°
β	77.635 ± 0.002°
γ	64.252 ± 0.001°
Cell volume	1138.11 ± 0.07 Å³
Cell temperature	173.15 K
Ambient diffraction temperature	173.15 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.06
Residual factor for significantly intense reflections	0.0488
Weighted residual factors for significantly intense reflections	0.093
Weighted residual factors for all reflections included in the refinement	0.0996
Goodness-of-fit parameter for all reflections included in the refinement	1.217
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179913 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/08.	7020800.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7020800.cif
73673	2013-02-21	cif/ Adding structures of 7020791, 7020792, 7020793, 7020794, 7020795, 7020796, 7020797, 7020798, 7020799, 7020800, 7020801, 7020802, 7020803, 7020804, 7020805 via cif-deposit CGI script.	7020800.cif