Crystallography Open Database

Information card for entry 7020801

7020800 << 7020801 >> 7020802

Preview

Coordinates	7020801.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H42 Ni O2 P2
Calculated formula	C20 H42 Ni O2 P2
SMILES	C(#[O])[Ni](C#[O])([P](C(C)C)(C(C)C)C(C)C)[P](C(C)C)(C(C)C)C(C)C
Title of publication	Synthesis and chemistry of bis(triisopropylphosphine) nickel(i) and nickel(0) precursors.
Authors of publication	Beck, Robert; Shoshani, Manar; Krasinkiewicz, Jonathan; Hatnean, Jillian A.; Johnson, Samuel A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	5
Pages of publication	1461 - 1475
a	11.66 ± 0.002 Å
b	14.224 ± 0.003 Å
c	15.172 ± 0.003 Å
α	90°
β	111.17 ± 0.03°
γ	90°
Cell volume	2346.5 ± 0.9 Å³
Cell temperature	173.15 K
Ambient diffraction temperature	173.15 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0383
Residual factor for significantly intense reflections	0.0324
Weighted residual factors for significantly intense reflections	0.0749
Weighted residual factors for all reflections included in the refinement	0.0776
Goodness-of-fit parameter for all reflections included in the refinement	1.085
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179913 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/08.	7020801.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7020801.cif
73673	2013-02-21	cif/ Adding structures of 7020791, 7020792, 7020793, 7020794, 7020795, 7020796, 7020797, 7020798, 7020799, 7020800, 7020801, 7020802, 7020803, 7020804, 7020805 via cif-deposit CGI script.	7020801.cif