Crystallography Open Database

Information card for entry 7020802

7020801 << 7020802 >> 7020803

Preview

Coordinates	7020802.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H42 Ni2 P2 S4
Calculated formula	C20 H42 Ni2 P2 S4
Title of publication	Synthesis and chemistry of bis(triisopropylphosphine) nickel(i) and nickel(0) precursors.
Authors of publication	Beck, Robert; Shoshani, Manar; Krasinkiewicz, Jonathan; Hatnean, Jillian A.; Johnson, Samuel A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	5
Pages of publication	1461 - 1475
a	7.6433 ± 0.0015 Å
b	11.11 ± 0.002 Å
c	17.163 ± 0.003 Å
α	87.22 ± 0.03°
β	79.83 ± 0.03°
γ	71.63 ± 0.02°
Cell volume	1361.4 ± 0.5 Å³
Cell temperature	173.15 K
Ambient diffraction temperature	173.15 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0999
Residual factor for significantly intense reflections	0.0579
Weighted residual factors for significantly intense reflections	0.0934
Weighted residual factors for all reflections included in the refinement	0.1091
Goodness-of-fit parameter for all reflections included in the refinement	0.981
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179913 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/08.	7020802.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7020802.cif
73673	2013-02-21	cif/ Adding structures of 7020791, 7020792, 7020793, 7020794, 7020795, 7020796, 7020797, 7020798, 7020799, 7020800, 7020801, 7020802, 7020803, 7020804, 7020805 via cif-deposit CGI script.	7020802.cif