Crystallography Open Database

Information card for entry 7024294

Preview

Coordinates	7024294.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C57 H65 F4 N4 Pd2
Calculated formula	C57 H65 F4 N4 Pd2
Title of publication	Synthesis and reactivity of palladium(II) fluoride complexes containing nitrogen-donor ligands.
Authors of publication	Ball, Nicholas D.; Kampf, Jeff W.; Sanford, Melanie S.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	2
Pages of publication	632 - 640
a	17.9592 ± 0.0012 Å
b	17.5332 ± 0.0012 Å
c	20.295 ± 0.0014 Å
α	90°
β	95.135 ± 0.001°
γ	90°
Cell volume	6364.9 ± 0.8 Å³
Cell temperature	85 ± 2 K
Ambient diffraction temperature	85 ± 2 K
Number of distinct elements	5
Space group number	9
Hermann-Mauguin space group symbol	I 1 a 1
Hall space group symbol	I -2ya
Residual factor for all reflections	0.07
Residual factor for significantly intense reflections	0.0552
Weighted residual factors for significantly intense reflections	0.1553
Weighted residual factors for all reflections included in the refinement	0.1651
Goodness-of-fit parameter for all reflections included in the refinement	1.135
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179947 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/42.	7024294.cif
92361	2014-01-12	cif/ Adding structures of 7024293, 7024294, 7024295, 7024296, 7024297, 7024298, 7024299 via cif-deposit CGI script.	7024294.cif