Crystallography Open Database

Information card for entry 7024295

Preview

Coordinates	7024295.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H41 F5 N2 O2 Pd
Calculated formula	C30 H41 F5 N2 O2 Pd
Title of publication	Synthesis and reactivity of palladium(II) fluoride complexes containing nitrogen-donor ligands.
Authors of publication	Ball, Nicholas D.; Kampf, Jeff W.; Sanford, Melanie S.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	2
Pages of publication	632 - 640
a	9.6894 ± 0.0007 Å
b	12.7681 ± 0.0009 Å
c	13.8914 ± 0.001 Å
α	73.672 ± 0.001°
β	77.18 ± 0.001°
γ	69.587 ± 0.001°
Cell volume	1530.97 ± 0.19 Å³
Cell temperature	85 ± 2 K
Ambient diffraction temperature	85 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0526
Residual factor for significantly intense reflections	0.0448
Weighted residual factors for significantly intense reflections	0.1019
Weighted residual factors for all reflections included in the refinement	0.1088
Goodness-of-fit parameter for all reflections included in the refinement	1.105
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179947 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/42.	7024295.cif
92361	2014-01-12	cif/ Adding structures of 7024293, 7024294, 7024295, 7024296, 7024297, 7024298, 7024299 via cif-deposit CGI script.	7024295.cif