Crystallography Open Database

Information card for entry 7121495

Preview

Coordinates	7121495.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C55 H77 As N4 Si Zn
Calculated formula	C55 H77 As N4 Si Zn
Title of publication	From zinco(ii) arsaketenes to silylene-stabilised zinco arsinidene complexes.
Authors of publication	Ballestero-Martínez, Ernesto; Hadlington, Terrance J.; Szilvási, Tibor; Yao, Shenglai; Driess, Matthias
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	48
Pages of publication	6124 - 6127
a	14.0308 ± 0.0001 Å
b	13.9065 ± 0.0001 Å
c	26.737 ± 0.0002 Å
α	90°
β	90.031 ± 0.001°
γ	90°
Cell volume	5216.9 ± 0.07 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0454
Residual factor for significantly intense reflections	0.0372
Weighted residual factors for significantly intense reflections	0.0956
Weighted residual factors for all reflections included in the refinement	0.1018
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
228358 (current)	2019-11-17	cif/ Updating files of 7121492, 7121493, 7121494, 7121495, 7121496 Original log message: Adding full bibliography for 7121492--7121496.cif.	7121495.cif
207347	2018-04-16	cif/ Adding structures of 7121492, 7121493, 7121494, 7121495, 7121496 via cif-deposit CGI script.	7121495.cif