Crystallography Open Database

Information card for entry 7121496

Preview

Coordinates	7121496.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50 H81 As N6 Si Zn
Calculated formula	C50 H81 As N6 Si Zn
Title of publication	From zinco(ii) arsaketenes to silylene-stabilised zinco arsinidene complexes.
Authors of publication	Ballestero-Martínez, Ernesto; Hadlington, Terrance J.; Szilvási, Tibor; Yao, Shenglai; Driess, Matthias
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	48
Pages of publication	6124 - 6127
a	13.577 ± 0.0006 Å
b	14.7552 ± 0.0005 Å
c	14.8121 ± 0.0005 Å
α	92.378 ± 0.003°
β	107.476 ± 0.004°
γ	112.237 ± 0.004°
Cell volume	2579.1 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0487
Residual factor for significantly intense reflections	0.0411
Weighted residual factors for significantly intense reflections	0.1109
Weighted residual factors for all reflections included in the refinement	0.1201
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
228358 (current)	2019-11-17	cif/ Updating files of 7121492, 7121493, 7121494, 7121495, 7121496 Original log message: Adding full bibliography for 7121492--7121496.cif.	7121496.cif
207347	2018-04-16	cif/ Adding structures of 7121492, 7121493, 7121494, 7121495, 7121496 via cif-deposit CGI script.	7121496.cif