Crystallography Open Database

Information card for entry 7221865

Preview

Coordinates	7221865.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	F5 O2 Pb2 V
Calculated formula	F5 O2 Pb2 V
Title of publication	Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V(iv) and V(v) containing Sr4V3O5F13, Pb7V4O8F18, Pb2VO2F5, and Pb2VOF6
Authors of publication	Yeon, Jeongho; Felder, Justin B.; Smith, Mark D.; Morrison, Gregory; zur Loye, Hans-Conrad
Journal of publication	CrystEngComm
Year of publication	2015
Journal volume	17
Journal issue	44
Pages of publication	8428
a	5.6675 ± 0.0005 Å
b	7.3492 ± 0.0006 Å
c	8.3152 ± 0.0007 Å
α	101.234 ± 0.0012°
β	108.995 ± 0.0013°
γ	110.625 ± 0.0012°
Cell volume	287.14 ± 0.04 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0322
Residual factor for significantly intense reflections	0.0305
Weighted residual factors for significantly intense reflections	0.0765
Weighted residual factors for all reflections included in the refinement	0.0771
Goodness-of-fit parameter for all reflections included in the refinement	1.27
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
171047 (current)	2015-12-09	cif/ Updating files of 7221863, 7221864, 7221865, 7221866 Original log message: Adding full bibliography for 7221863--7221866.cif.	7221865.cif
153637	2015-08-25	cif/ Adding structures of 7221863, 7221864, 7221865, 7221866 via cif-deposit CGI script.	7221865.cif