Crystallography Open Database

Information card for entry 7221866

Preview

Coordinates	7221866.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	F6 O Pb2 V
Calculated formula	F6 O Pb2 V
Title of publication	Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V(iv) and V(v) containing Sr4V3O5F13, Pb7V4O8F18, Pb2VO2F5, and Pb2VOF6
Authors of publication	Yeon, Jeongho; Felder, Justin B.; Smith, Mark D.; Morrison, Gregory; zur Loye, Hans-Conrad
Journal of publication	CrystEngComm
Year of publication	2015
Journal volume	17
Journal issue	44
Pages of publication	8428
a	5.6675 ± 0.0004 Å
b	15.7931 ± 0.0012 Å
c	12.9995 ± 0.0009 Å
α	90°
β	92.019 ± 0.002°
γ	90°
Cell volume	1162.83 ± 0.15 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0293
Residual factor for significantly intense reflections	0.026
Weighted residual factors for significantly intense reflections	0.0564
Weighted residual factors for all reflections included in the refinement	0.0577
Goodness-of-fit parameter for all reflections included in the refinement	1.096
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
171047 (current)	2015-12-09	cif/ Updating files of 7221863, 7221864, 7221865, 7221866 Original log message: Adding full bibliography for 7221863--7221866.cif.	7221866.cif
153637	2015-08-25	cif/ Adding structures of 7221863, 7221864, 7221865, 7221866 via cif-deposit CGI script.	7221866.cif