Crystallography Open Database

Information card for entry 4069700

Preview

Coordinates	4069700.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H48 Cl N Nb P Rh
Calculated formula	C37 H48 Cl N Nb P Rh
Title of publication	Niobium/Rhodium Bimetallic Complexes: Synthesis, Structure, and Catalytic Hydrosilylation of Acetophenone and Benzaldehyde
Authors of publication	Leelasubcharoen, Somying; Zhizhko, Pavel A.; Kuzmina, Lyudmila G.; Churakov, Andrei V.; Howard, Judith A. K.; Nikonov, Georgii I.
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	15
Pages of publication	4500
a	9.1766 ± 0.0006 Å
b	18.6877 ± 0.0012 Å
c	20.1635 ± 0.0012 Å
α	90°
β	98.312 ± 0.003°
γ	90°
Cell volume	3421.5 ± 0.4 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.087
Residual factor for significantly intense reflections	0.0587
Weighted residual factors for significantly intense reflections	0.105
Weighted residual factors for all reflections included in the refinement	0.1113
Goodness-of-fit parameter for all reflections included in the refinement	1.164
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178586 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/97.	4069700.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4069700.cif
40398	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4069699, 4069700 via cif-deposit CGI script.	4069700.cif