Crystallography Open Database

Information card for entry 7703341

Preview

Coordinates	7703341.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H63 N4 O Sc Si2
Calculated formula	C43 H63 N4 O Sc Si2
Title of publication	Bis(alkyl) scandium and yttrium complexes coordinated by an amidopyridinate ligand: synthesis, characterization and catalytic performance in isoprene polymerization, hydroelementation and carbon dioxide hydrosilylation.
Authors of publication	Gurina, G. A.; Kissel, A. A.; Lyubov, D. M.; Luconi, L.; Rossin, A.; Tuci, G.; Cherkasov, A. V.; Lyssenko, K. A.; Shavyrin, A. S.; Ob'edkov, A. M.; Giambastiani, G.; Trifonov, A. A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	3
Pages of publication	638 - 650
a	19.191 ± 0.002 Å
b	16.3197 ± 0.0018 Å
c	14.8442 ± 0.0016 Å
α	90°
β	108.715 ± 0.003°
γ	90°
Cell volume	4403.3 ± 0.8 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0876
Residual factor for significantly intense reflections	0.0535
Weighted residual factors for significantly intense reflections	0.128
Weighted residual factors for all reflections included in the refinement	0.149
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
247075 (current)	2020-01-22	cif/ Adding structures of 7703341, 7703342, 7703343 via cif-deposit CGI script.	7703341.cif